• Title/Summary/Keyword: spectrophotometer

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Effect of CAD/CAM ceramic thickness on shade (CAD/CAM 세라믹의 두께가 색조에 미치는 영향)

  • Kang, Wol;Han, Man-So;Kim, Ji-Hwan
    • Journal of Korean society of Dental Hygiene
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    • v.16 no.5
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    • pp.695-700
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    • 2016
  • Objectives: The purpose of the study was to investigate the effect of CAD/CAM ceramic thickness on shade. Methods: 24 disk-shaped ceramic specimens (E.Max CAD & Empress CAD, $12mm{\times}12mm$) were prepared and divided into 4 groups (n=6). Ceramic specimens in 2 thicknesses (0.8 mm, 1.0 mm) were made low translucency(LT) shade A2. All specimens were measured as L*, a*, b* using spectrophotometer. The color differences(${\Delta}E$ values) between the specimen and a control target block ($12{\times}12{\times}1.2mm$) were calculated. Two-way ANOVA performed between 2 groups(material and thickness). Results: As the thickness increased, the $L^*$ (for all groups) and $b^*$ value (for all groups) increased and the $a^*$ value(for LR group) decreased. The mean color differences caused by thickness was acceptible (${\Delta}E$ > 2) for group LD1. But the mean color differences by thickness were not selected (${\Delta}E$ < 2) for group LD2, LR1, LR2. Conclusions: The different thickness can influence the final color of CAD/CAM ceramic.

Effects of Ascorbic acid on the Phototoxicity of Phenothiazines (Phenothiazines의 광독성에 미치는 Ascorbic acid의 영향)

  • 김봉희;박영아
    • Journal of Food Hygiene and Safety
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    • v.7 no.4
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    • pp.143-147
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    • 1992
  • This study was conducted to investigate the effects of ascorbic add on their phototoxicity of four phenothiazine derivatives such as chloropromazine, perphenazine, trifluoperazine and thioridazine. Effects of the test compounds on RBes were monitored with a spectrophotometer by the method of Kahan et al. The extent of photohemolysis by chlorpromazine, perphenazine and thioridazine were decreased with the use of ascorbic acid. It was observed that toxic photoproducts were formed by chlorpromazine and thioridazine with preirtadiated. Although red blood cell hemolysis by preirradiated chlorpromazine was decreased with the use of ascorbic acid but thioridazine was not changed.

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Pigmentation of Diketopyrrolopyrroles Compound through Solvent Thermal-treatment and Its Property (용매 열처리법을 통한 diketopyrrolopyrroles 화합물의 안료화 및 그 특성)

  • Kim, Jae Hwan;Yang, Seok Won;Kim, Dae-Sung;Wu, Guan Zhu;Lee, Gun-Dae;Park, Seong Soo
    • Applied Chemistry for Engineering
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    • v.25 no.4
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    • pp.357-362
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    • 2014
  • To prepare diketopyrrolopyrrole (DPP) red 254 pigment with high shield and bright color, DPP red 254 crude previously synthesized was treated at various thermal-treat temperature, addition derivative and ball-milling. The properties of samples were measured by the means of FT-IR, UV-Vis spectroscopy, TEM, PSA, BET surface area analyzer, viscometer and spectrophotometer. It was found that solvent thermal-treatment of the sample prepared after ball-milling as nano-scale was very effective method in pigmentation process.

Study of the most frequent natural tooth colors in the Spanish population using spectrophotometry

  • Gomez-Polo, Cristina;Gomez-Polo, Miguel;Martinez Vazquez de Parga, Juan Antonio;Celemin Vinuela, Alicia
    • The Journal of Advanced Prosthodontics
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    • v.7 no.6
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    • pp.413-422
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    • 2015
  • PURPOSE. To identify the most frequent natural tooth colors using the Easyshade Compact (Vita -Zahnfabrik) spectrophotometer on a sample of the Spanish population according to the 3D Master System. MATERIALS AND METHODS. The middle third of the facial surface of natural maxillary central incisors was measured with an Easyshade Compact spectrophotometer (Vita Zahnfabrik) in 1361 Caucasian Spanish participants aged between 16 and 89 years. Natural tooth color was recorded using the 3D Master System nomenclature. The program used for the present descriptive statistical analysis of the results was SAS 9.1.3. RESULTS. The results show that the most frequent dental color in the total sample studied is 3M1 (7.05%), followed by the intermediate shade 1M1.5 (6.91%) and 2L1.5 (6.02%). CONCLUSION. According to the research methodology used, and taking into account the limitations of this study, it can be proposed that the most frequent color among the Spanish population is 3M1; the most common lightness group is 2; the most frequent hue group according to the 3D Master System is M and the most frequent chroma group is 1.5.

Composition of Mineral Components of Ginseng on Age and Cultivated Area (인삼의 년근별, 산지별 무기물의 분포에 관한 연구)

  • 전병선;양재원;박채규;고성룡;굴야준랑(掘野俊郞);손종록;박원종
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.22 no.5
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    • pp.592-595
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    • 1993
  • Mineral compositions in various ginseng, which was grown in different region, different age, were analyzed by atomic absorption spectrophotometer. $Mn^{++}$ content in ginseng of five years old was four times higher than that of two years old, suggesting that the amount of $Mn^{++}$ would be increased as they are cultivated. The content of phosphate in the various ginseng did not show much difference, whereas that of $Ca^{++},\;Mn^{++}$ did. Korean red ginseng revealed much higher in $Mn^{++}$ content than that of others investigated. When the amount N was compared, San Chi, Chinese ginseng was significantly lowered. Korean red ginseng of 100g contains highest phosphate ion of 328.3mg.

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Analysis and Measurement of the Spectrum of Whole Blood (전혈의 SPECTRUM 측정과 분석)

  • Kim, Y.J.;Kim, H.S.;Kim, J.W.;Yoon, K.W.;Kim, W.K.
    • Proceedings of the KOSOMBE Conference
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    • v.1996 no.05
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    • pp.52-55
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    • 1996
  • The spectra of whole blood EDTA samples from two people were generated using a CARY 5E (UV-VIS-NIR) spectrophotometer from 400 to 1000nm which contain visible and NIR region. Only the data between 400 and 800nm were used to analyze the components of blood. Using the same spectrophotometer, the spectra of Water, normal saline, plasma were generated These spectra were subtracted from each blood sample, and then the first derivative of each of the subtracted data was taken to minimize baseline variations and indicated the wavelength-shift of peak and valley. Normalization and division between two blood samples were used to correlate the quantity ratio of specific components with feature of spectra. Samples were controlled at $30^{\circ}C,\;37^{\circ}C$, ambient temperature.

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Hair Bleaching and Degree of Damage by Thermal Treatment (열처리에 의한 모발의 퇴색 및 손상도 연구)

  • Seong, Yu Rim;Kang, Eun Ju;Lim, Sun Nye
    • Textile Coloration and Finishing
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    • v.31 no.3
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    • pp.155-164
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    • 2019
  • This study comparatively analyzed hair bleaching and degree of damage by the temperature of a heating tool after coloring hair with a permanent, semi-permanent or plant hair dye. According to analysis by spectrophotometer, 'semi-permanent hair dye' was the highest, followed by 'permanent hair dye' and 'plant hair dye' in terms of changes in $L^*$ values. In terms of changes in hair shape when analyzed using FE-SEM, 'semi-permanent hair dye($150^{\circ}C$ or lower)' was the greatest, followed by 'plant hair dye($180^{\circ}C$ or lower)' and 'permanent hair dye($200^{\circ}C$ or lower)'. Therefore, it is reasonable to flat iron hair at low temperature. According to the test, amino acid values gradually decreased in both bleached and colored hair. The results obtained through TGA-based thermal analysis confirmed that as brightness increases, hair moisture contents decrease. This study aimed to protect hair by suggesting a correct use of a flat iron by the hair dye type during hair coloring. It appears that the study results would help hairdressers minimize hair damage by using a hair dye at proper temperature.

Effect of translucency on CAD/CAM ceramic according to different core/veneer thickness (캐드캠 세라믹의 코어와 베니어의 서로 다른 두께가 반투명도에 미치는 영향)

  • Kang, Wol;Kim, Ji-Hwan
    • Journal of Korean society of Dental Hygiene
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    • v.18 no.6
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    • pp.1037-1045
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    • 2018
  • Objectives: The purpose of this study was to evaluation the effect of translucency on CAD/CAM ceramic according to different core/veneer thicknesses. Methods: A total of 42 samples from 2 groups of 7 ceramic cores, each with 3 thickness values (0.8, 1.0, 1.2 mm) were manufactured. The veneers were also manufactured in 3 thicknesses (0.3, 0.5, 0.7 mm). The group names were based on the name of the ceramic core (IPS e.Max CAD; LD, and IPS Empress CAD; LR). The associated number was determined by the combined thickness of the core and veneer: 1 = (0.8 + 0.7); 2 = (1.0 + 0.5); 3 = (1.2 + 0.3). The translucency was measured using a spectrophotometer and defined via the contrast ratio (CR) and translucency parameter (TP). Two-way ANOVA was performed to compare the 2 groups (material and thickness). Results: As the core thickness increased, the TP value also increased, and the CR value (for LR group) decreased. The results of 2-way ANOVA demonstrated that the thicknesses of different core/veneer combinations significantly affected the translucency (p<0.05). Conclusions: The different core and veneer thicknesses affected the translucency of CAD/CAM ceramic.

Sodium titanate as an infrared reflective material for cool roof application

  • Ullah, Mahboob;Kim, Hee Jung;Heo, Jae Gu;Roh, Dong Kyu;Kim, Dae-Sung
    • Journal of Ceramic Processing Research
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    • v.20 no.spc1
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    • pp.86-91
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    • 2019
  • A solid-state route was used to prepare sodium titanium oxide (NTO, Na2Ti3O7) as a solar heat protecting material with an impressive solar reflectance (TSR = 94.3%) using a high refractive index rutile TiO2. The solar reflectance of the synthesized NTO was measured using UV-Vis-NIR spectrophotometer. Solar reflectance property of the synthesized compound depends on the calcination temperature. The solar reflectance property of the synthesized NTO powder was compared with commercial rutile TiO2. The compound synthesized at 900 ℃ for 24 hrs had remarkable solar reflectance 94.3% than that calcined below 900 ℃. Crystalline nature, structural property, morphology and optical properties of NTO powders were characterized and analyzed using XRD, FE-SEM, EDS and UV-Vis-NIR spectrophotometer. From the results, we guessed that NTO would be a suitable "solar heat protecting candidate" for energy-saving applications in coating industries.

Difference in color and translucency according to dental zirconia A3 colorant (치과용 지르코니아 A3 착색제에 따른 색상 및 반투명도 차이)

  • Joo-Hee Lee;Jin-Young Park
    • Journal of Technologic Dentistry
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    • v.44 no.4
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    • pp.118-125
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    • 2022
  • Purpose: The color of dental zirconia is very important in terms of aesthetics. To reproduce the color tone, a colorant is applied to zirconia to express the color tone. I would like to point out that the color, brightness, and saturation of the colorant used to express the color A3 may vary depending on the manufacturer. Methods: Each zirconia block received a total of 25 circular specimens for the experiment. The zirconia specimen was then deposited by colorant type to reproduce the color tone. Color differences and translucency were measured using a spectrophotometer. To compare and analyze the zirconia color according to the type of colorant, one-way ANOVA was used. Results: For each type of zirconia colorant, there was no statistically significant difference in translucency or b* (p>0.05). There was a statistical difference in L* and a* (p<0.05). Conclusion: The ΔE*ab (D65) value is less than 5.5 or less, and the color difference is within an acceptable range.