• Title/Summary/Keyword: spectral ratio method

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Isolation of Berberine from the Rhizome of $Coptis$ $chinensis$ by Centrifugal Partition Chromatography (향류분배 크로마토그라피법에 의한 황련($Coptis$ $chinensis$) 뿌리로 부터 Berberine의 분리)

  • Kim, Jung-Bae
    • The Korean Journal of Food And Nutrition
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    • v.24 no.4
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    • pp.617-621
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    • 2011
  • $Coptis$ $chinensis$ Franch rhizome is one of the important traditional Korea medicines with anti-inflammatory, anti-bacterial, anti-hypertensive and anti-cancer properties. The methanol extract of rhizome from the $Coptis$ $chinensis$ rhizome was purified by using preparative centrifugal partition chromatography (CPC) and HPLC method. The optimum two-phase CPC solvent system was composed of n-butanol:acetic acid:water at a ratio of 4:1:5. Berberine (16.8 mg) was successfully isolated by CPC and HPLC. The chemical structure of the compound was identified by (1 H)$^1H$, $^{13}C$-NMR and ESI-MS spectral data analysis.

Analysis of Seismic Response due to the Dynamic Coupling Between a Primary Structure and Secondary System (구조물과 부계통간의 연계방법에 따른 지진응답 분석)

  • Jung, Kwangsub;Kwag, Shinyoung;Choi, In-Kil;Eem, Seunghyun
    • Journal of the Earthquake Engineering Society of Korea
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    • v.24 no.2
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    • pp.87-93
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    • 2020
  • Seismic responses due to the dynamic coupling between a primary structure and secondary system connected to a structure are analyzed in this study. The seismic responses are compared based on dynamic coupling criteria and according to the error level in the natural frequency, with the recent criteria being reliant on the error level in the spectral displacement response. The acceleration responses and relative displacement responses of a primary structure and a secondary system for a coupled model and two different decoupled models of two degrees-of-freedom system are calculated by means of the time integration method. Errors in seismic responses of the uncoupled models are reduced with the recent criteria. As the natural frequency of the secondary system increases, error in the natural frequency decreases, but seismic responses of uncoupled models can be underestimated compared to that of coupled model. Results in this paper can help determine dynamic coupling and predict uncoupled models' response conservatism.

Chemical Composition of RM_1-390 - Large Magellanic Cloud Red Supergiant

  • Yushchenko, Alexander V.;Jeong, Yeuncheol;Gopka, Vira F.;Vasil'eva, Svetlana V.;Andrievsky, Sergey M.;Yushchenko, Volodymyr O.
    • Journal of Astronomy and Space Sciences
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    • v.34 no.3
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    • pp.199-205
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    • 2017
  • A high resolution spectroscopic observation of the red supergiant star RM_1-390 in the Large Magellanic Cloud was made from a 3.6 m telescope at the European Southern Observatory. Spectral resolving power was R=20,000, with a signal-to-noise ratio S/N > 100. We found the atmospheric parameters of RM_1-390 to be as follows: the effective temperature $T_{eff}=4,250{\pm}50K$, the surface gravity ${\log}\;g=0.16{\pm}0.1$, the microturbulent velocity $v_{micro}=2.5km/s$, the macroturbulence velocity $v_{macro}=9km/s$ and the iron abundance $[Fe/H]=-0.73{\pm}0.11$. The abundances of 18 chemical elements from silicon to thorium in the atmosphere of RM_1-390 were found using the spectrum synthesis method. The relative deficiencies of all elements are close to that of iron. The fit of abundance pattern by the solar system distribution of r- and s-element isotopes shows the importance of the s-process. The plot of relative abundances as a function of second ionization potentials of corresponding chemical elements allows us to find a possibility of convective energy transport in the photosphere of RM_1-390.

Microwave Sol-Gel Derived Ho3+/Yb3+ Co-Doped NaCaGd(MoO4)3 Phosphors and their Upconversion Photoluminescence

  • Lim, Chang Sung
    • Journal of the Korean Ceramic Society
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    • v.53 no.4
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    • pp.456-462
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    • 2016
  • $NaCaGd(MoO_4)_3:Ho^{3+}/Yb^{3+}$ ternary molybdates were successfully synthesized by microwave sol-gel method for the first time. Well-crystallized particles formed after heat-treatment at $900^{\circ}C$ for 16 h showed a fine and homogeneous morphology with particle sizes of $3-5{\mu}m$. Under excitation at 980 nm, the UC intensities of the doped samples exhibited strong yellow emissions based on the combination of strong emission bands at the 520-nm and 630-nm emission bands in the green and red spectral regions, respectively. The strong 520-nm emission band in the green region corresponds to the $^5S_2/^5F_4{\rightarrow}^5I_8$ transition of $Ho^{3+}$ ions, while the strong 630-nm emission band in the red region appears to be due to the $^5F_5{\rightarrow}^5I_8$ transition of the $Ho^{3+}$ ions. The optimal $Yb^{3+}:Ho^{3+}$ ratio was found at 9:1, as indicated by the composition-dependent quenching effect of $Ho^{3+}$ ions. The pump power dependence of the upconversion emission intensity and the Commission Internationale de L'Eclairage chromaticity coordinates of the phosphors were evaluated in detail.

The Chemical Composition of V1719 Cyg: δ Scuti Type Star without the Accretion of Interstellar Matter

  • Yushchenko, Alexander V.;Kim, Chulhee;Jeong, Yeuncheol;Doikov, Dmytry N.;Yushchenko, Volodymyr A.;Khrapatyi, Sergii V.;Demessinova, Aizat
    • Journal of Astronomy and Space Sciences
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    • v.37 no.3
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    • pp.157-163
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    • 2020
  • High resolution spectroscopic observation of V1719 Cyg were made at 1.8 meter telescope of Bohyunsan Optical Astronomy observatory in Korea. Spectral resolving power was R=45,000, signal to noise ratio S/N>100. The abundances of 28 chemical elements from carbon to dysprosium were found with the spectrum synthesis method. The abundances of oxygen, titanium, vanadium and elements with Z>30 are overabundant by 0.2-0.9 dex with respect to the solar values. Correlations of derived abundances with condensation temperatures and second ionization potentials of these elements are discussed. The possible influence of accretion from interstellar environment is not so strong as for ρ Pup and other stars with similar temperatures. The signs of accretion are absent. The comparison of chemical composition with solar system r- & s-process abundance patterns shows the enhancement of the photosphere by s-process elements.

Seismic performances of three- and four-sided box culverts: A comparative study

  • Sun, Qiangqiang;Peng, Da;Dias, Daniel
    • Geomechanics and Engineering
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    • v.22 no.1
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    • pp.49-63
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    • 2020
  • Studying the critical response characteristics of box culverts with diverse geometrical configurations under seismic excitations is a necessary step to develop a reasonable design method. In this work, a numerical parametric study is conducted on various soil-culvert systems, aiming to highlight the critical difference in the seismic performances between three- and four-sided culverts. Two-dimensional numerical models consider a variety of burial depths, flexibility ratios and foundation widths, assuming a visco-elastic soil condition, which permits to compare with the analytical solutions and previous studies. The results show that flexible three-sided culverts at a shallow depth considerably amplify the spectral acceleration and Arias intensity. Larger racking deformation and rocking rotation are also predicted for the three-sided culverts, but the bottom slab influence decreases with increasing burial depth and foundation width. The bottom slab combined with the burial depth and structural stiffness also significantly influences the magnitude and distribution of the dynamic earth pressure. The findings of this work shed light on the critical role of the bottom slab in the seismic responses of box culverts and may have a certain reference value for the preliminary seismic design using R-F relation.

Spectral Domain Analysis of Input Impedance and Radiation Pattern in Rectangular Microstrip Patch Antenna on Anisotropy Substrates with Airgap (공기 갭을 갖는 이방성 매질 위의 사각 마이크로스트립 패치 안테나의 입력 임피던스와 방사패턴에 대한파수 영역 해석)

  • 윤중한;곽경섭
    • Journal of the Institute of Electronics Engineers of Korea TC
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    • v.40 no.5
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    • pp.187-196
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    • 2003
  • Effects of Airgap and anisotropy substrate on input impedance and radiation pattern of rectangular microstrip patch antenna are studied in terms of an integral equation formulation. The input impedance and radiation pattern of microstrip patch antenna is investigated by using Galerkin's moment method in solving the integral equation. Sinusoidal functions are selected as basis functions, which resemble in the actual standing wave on the Patch. From the numerical results, the variation of input impedance and radiation patterns in the variation of air gap thickness, anisotropy ratio of substrate, and relative permittivity of anisotropy substrate are presented.

A Study on an Improved MVE for Estimating the Direction of Arrival of Multiple Sources (다중 신호원의 도래방향 추정을 위한 개선된 MVE에 관한 연구)

  • 정용민;신준호;김용득
    • Proceedings of the IEEK Conference
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    • 1999.06a
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    • pp.687-690
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    • 1999
  • Many high-resolution algorithms based on the eigen-decomposition analysis of observed covariance matrix, such as MVE, MUSIC, and EVM, have been proposed. However, the resolution of spectral estimates for these algorithms is severely degraded when Signal-to-Noise Ratio (SNR) is low and arrival angles of signal are close to each other. And EVM and MUSIC is powerful for the characteristic of SNR. But have the limitation that the number of signals presented is known. While MVE is bad the characteristic of SNR. In this study, we propose a modified MVE to enhance the resolution for Direction-Of-Arrival (DOA) estimation of underwater acoustic signal. This is to remove the limitation that existing algorithms should know the information for the number of signals. Because the algorithms founded on the eigen value estimate DOA with only the noise subspace, they have the high-resolution characteristic. And then, with the method reducing the effect of the signal subspace, we are to reduce the degradation because of complementary relationship between the signal subspace and the noise subspace. This paper, with using the simulation data, we have estimated the proposed algorithms, compared it with other high-resolution algorithms. The simulation results show that the modified MVE proposed is accurate and has a better resolution even though SNR is low, under the same condition.

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Design and Fabrication of Miniaturized Optical Chopper Operated by Electromagnetic Actuation

  • Kim, Ho Won;Min, Seong Ki;Choi, Young Chan;Kong, Seong Ho
    • Journal of Sensor Science and Technology
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    • v.23 no.3
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    • pp.165-169
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    • 2014
  • An existing infrared (IR) analysis system is generally composed of infrared source, IR focusing lenses, IR detector, and optical chopper. An optical chopper is widely used in combination with lock-in amplifier to improve the signal-to-noise ratio by periodically interrupting incident light beam. During recent years, a few researches on miniaturized optical chopper have been reported to apply to micro-scaled optical systems. In this paper, a micro optical chopper operated by electromagnetic actuation is proposed and applied to a miniaturized micro-scaled optical system operating in IR spectral range. Additionally, the fabrication method of the proposed micro chopper is demonstrated. The proposed micro optical chopper is composed of the polydimethylsiloxane (PDMS) membrane, solenoid, and permanent magnet. The permanent magnet is bonded on the PDMS membrane using an ultraviolet-activated adhesive. The operation of the chopper is based on the attractive and repulsive forces between permanent magnet and solenoid induced by an electrical current flowing through the solenoid. The fabricated micro optical chopper could operate up to 200 Hz of frequency. The maximum operating distance of the chopper with 7mm diameter membrane was $750{\mu}m$ at 100 Hz of frequency.

Detrended fluctuation analysis of magnetic parameters of solar active regions

  • Lee, Eo-Jin;Moon, Yong-Jae
    • The Bulletin of The Korean Astronomical Society
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    • v.41 no.1
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    • pp.81.2-81.2
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    • 2016
  • Many signals in the nature have power-law behaviors, namely they are "scale-free". The method of detrended fluctuation analysis (DFA), as one of the popular methods (e.g., Rescaled range analysis and Spectral analysis) for determining scale-free nature of time series, has a very important advantage that the DFA can be applied to both stationary and non-stationary signals. The analysis of time series using the DFA has been broadly used in physiology, finance, hydrology, meteorology, geology, and so on. We performed the DFA of 16 Spaceweather HMI Active Region Patch (SHARP) parameters for 38 HMI Active Region Patches (HARPs) obtained by Solar Dynamics Observatory (SDO) from May 2010 to June 2014. The main results from this study are as follows. (1) The most of the time series data are non-stationary. (2) The DFA scaling exponents of "mean vertical current density" for 38 HARPs have a negative correlation coefficient (-0.41) with flare index. (3) The DFA scaling exponents of parameters such as "Sum of the absolute value of net currents per polarity", "Absolute value of the net current helicity", and "Mean photospheric excess magnetic energy density" for the most active HARPs having more than 10 major flares, have positive correlation coefficients (0.64, 0.59, and 0.53, respectively) with the ratio of "the number of CMEs associated with major flares" to "the number of major flares". Physical interpretations on our results will be discussed.

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