• Title/Summary/Keyword: specific surface

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Synthetic of Magnetic Fine Powder for Oil Suspending Magnetic Fluid (자성 유체용 미분 자성 분체의 제조)

  • 이경희;이병하;이재영
    • Journal of the Korean Ceramic Society
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    • v.28 no.2
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    • pp.146-152
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    • 1991
  • Ultra fine and homogeneous (Ni0.4Zn0.6)Fe2O4 ferrite powders were prepared by direct-wet, Hydrothermal and coprecipitation methods. In case that specific surface areas of Ni-Zn ferrite powders were over 220㎡/g, 100㎡/g, 30㎡/g individually direct-wet, hydrothermal and coprecipitation methods. The Ni-Zn ferrite magnetic fluids of which Solvents were benzene or kerosene was prepared by making cation surfactant adsorbed on the surface of the (Ni0.4Zn0.6)Fe2O4. The results that measured dispersion and viscosity by making cation surfactant adsorbed were as follows. 1. The adsorption amount of Oleric acid be proportioned the specific surface area of powders. 2. The maximum amount of Oleric acid was 36wt% of dried powders which has 220㎡/g of specific surface area. 3. The stability of fluid by direct-wet synthesis emthod in benzene or kerosene solvent excellent.

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Studies on Electrical Double Layer Capacitor Based on Mesoporous Activated Carbon

  • Meigen, Deng;Yihong, Feng;Bangchao, Yang
    • Carbon letters
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    • v.6 no.2
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    • pp.86-88
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    • 2005
  • Mesoporous activated carbon (AC) was prepared from aged petroleum coke through chemical activation. The AC has a specific surface area of 1733 $m^2/g$ and a mean pore diameter of 2.37 nm. The volume fraction of 2 to 4nm pores is 56.74%. At a current density of 10 mA/$cm^2$, a specific capacitance of 240 F/g is achieved representing the use factor of the surface area of 69.2%. And the electrical double layer capacitor (EDLC) based on the AC shows an excellent power performance. This result suggests that the presence of high fraction of mesopores can effectively increase the adsorption efficiency of the specific surface area of the AC and enhance the power performance of EDLC based on the efficient surface area of the AC.

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Characterization and Fabrication of Chemically Activated Carbon Fibers with Various Drying Temperatures using OXI-PAN Fibers

  • Moon, Sook-Young;Lee, Byung-Ha;Lim, Yun-Soo
    • Carbon letters
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    • v.8 no.1
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    • pp.30-36
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    • 2007
  • Oxidized PAN (OXI-PAN) fibers were used for the precursors of activated carbon fiber in study. How drying temperature affected the properties of carbon fibers on activating process of carbon fibers was investigated. The specific surface areas of activated carbon fibers have been determined on a series of chemically activated carbons with KOH and NaOH. The experimental data showed variations in specific surface area, iodine and silver adsorptions by the activated carbon fibers. The amount of iodine adsorption increases with increasing specific surface areas in both activation methods. This was because the ionic radius of iodine was smaller than the interior micropore size of activated carbon fibers. Silver adsorbed well in NaOH activated carbon fibers rather than KOH activated carbon fibers in this study.

Nano SPR Biosensor for Detecting Lung Cancer-Specific Biomarker (폐암 바이오마커 검출용 나노SPR 바이오센서)

  • Jang, Eun-Yoon;Yeom, Se-Hyuk;Eum, Nyeon-Sik;Han, Jung-Hyun;Kim, Hyung-Kyung;Shin, Yong-Beom;Kang, Shin-Won
    • Journal of Sensor Science and Technology
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    • v.22 no.2
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    • pp.144-149
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    • 2013
  • In this research, we developed a biosensor to detect lung cancer-specific biomarker using Anodic Aluminum Oxide (AAO) chip based on interference and nano surface plasmon resonance (nanoSPR). The nano-porous AAO chip was fabricated $2{\mu}m$ of pore-depth by two-step anodizing method for surface uniformity. NanoSPR has sensitivity to the refractive index (RI) of the surrounding medium and also provides simple and label-free detection when specific antibodies are immobilized to the Au-deposited surface of nano-porous AAO chip. To detect the lung cancer-specific biomarker, antibodies were immobilized on the surface of the chip by Self Assembled Monolayer (SAM) method. Since then lung cancer-specific biomarker was applied atop the antibodies immobilized layer. The specific reaction of the antigen-antibody contributed to the change in the refractive index that cause shift of resonance spectrum in the interference pattern. The Limit of Detection (LOD) was 1 fg/ml by using our nano-porous AAO biosensor chip.

Characteristics of methane sorption in surface modified activated carbon (표면개질 된 활성탄의 메탄흡장 특성)

  • Yun, Seok-Min;Kim, Ju-Wan;Jo, Won-Jun;Kim, Young-Ho;Lee, Young-Seak
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.73-76
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    • 2007
  • In this study, methane gas adsorption ability of activated carbon (AC) with surface functional group effect, adsorbed methane amount was evaluated after nitric acid and ureatreatment of AC surface. Specific surface area and pore distribution of AC were studied though nitrogen adsorption isotherm at 77 K. Micro pore volume was calculated through H-K method. Adsorbed methane amount was evaluated through volume method at room temperature by using auto adsorption apparatus. Adsorbed methane amount of AC was found to increase with to specific surface area increase.Correlation proposed between the methane adsorption amount and surface nature indicates that the surface nature plays an important role on the adsorption amount at a given temperature.

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Surface Modification by Heat-treatment of Propellant Waste Impregnated ACF

  • Yoon, Keun-Sig;Pyo, Dae-Ung;Lee, Young-Seak;Ryu, Seung-Kon;Yang, Xiao Ping
    • Carbon letters
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    • v.11 no.2
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    • pp.131-136
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    • 2010
  • Propellant waste was impregnated on the surface of activated carbon fiber and heat-treated at different temperature to introduce newly developed functional groups on the ACF surface. Functional groups of nitrogen and oxygen such as pyridine, pyridone, pyrrol, lacton and carboxyl were newly introduced on the surface of modified activated carbon fiber. The porosity, specific surface area, and morphology of those modified ACFs were changed as increasing the heat-treated temperature from 200 to $500^{\circ}C$. The optimum heat-treatment temperature was suggested to $500^{\circ}C$, because lower temperature given rise to the decrease of specific surface area and higher temperature resulted in the decrease of weight loss. Propellant waste can be used as an useful surface modifier to porous carbons.

Analysis of Specific Grinding Energy Characteristics Using Average Grain Model (평균입자모델을 이용한 비연삭에너지 특성평가)

  • 이영문;최원식;장승일;배대원;손정우;이현구
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2004.10a
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    • pp.16-21
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    • 2004
  • As a new approach to analyze grinding energy, this paper introduces a specific grinding energy model based on the average grain. Using this model, grinding characteristics such as radial and tangential forces, specific grinding energy of SM45C were investigated altering grinding variables such as workpiece velocity(v) and apparent depth of cut(Z) in down-surface grinding. From the experimental results, there is no significant difference between the radial, tangential forces and vertical. horizontal forces because of small contact angle between wheel and workpiece. The specific grinding energy decreases as the maximum undeformed chip thickness increases. But, there is much difference between the specific grinding energies of the existing and the proposed model.

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Characteristics of specific grinding energy depending on grain size (연삭입자크기에 따른 비연삭에너지 특성)

  • Lee H.G.;Lee Y.M.;Yang S.H.;Bae D.W.;Kim H.K.
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2005.05a
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    • pp.319-323
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    • 2005
  • As a new approach to analyze grinding energy, this paper introduces a specific grinding energy model based on the average grain. Using this model, grinding characteristics such as specific grinding energy of SM45C were investigated with changing variables such as grain size, workpiece velocity(v) and apparent depth of cut(Z) in down-surface grinding. From the experimental results, the specific grinding energy decreases as the maximum undeformed chip thickness increases. And also the specific grinding energy increases as the grit size increases.

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Analysis of specific grinding energy using average grain model (평균입자모델을 이용한 비연삭에너지 해석)

  • Lee Young Moon;Choi Won Sik;Chang Sung Il;Bae Dae Won;Son Jeong Woo;Lee Hyun Goo
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.14 no.4
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    • pp.61-68
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    • 2005
  • As a new approach to analyze grinding energy, this paper introduces a specific grinding energy model based on the average grain. Using this model, grinding characteristics such as radial and tangential forces, specific grinding energy of SM45C were investigated with changing grinding variables such as workpiece velocity(v) and apparent depth of cut(Z) in down-surface grinding. From the experimental results, the specific grinding energy decreases as the maximum undeformed chip thickness increases. And there is no significant difference between the specific grinding energies of the existing and the proposed model.

Adsorption Behaviors of Noxious Gases on Chemically Surface-treated Activated Carbons

  • Park, Soo-Jin;Shin, Jun-Sik
    • Carbon letters
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    • v.4 no.1
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    • pp.31-35
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    • 2003
  • The specific adsorption behaviors of activated carbons (ACs) treated with 30 wt% $H_3PO_4$ or NaOH were investigated in the removals of NO or $NH_3$. The acid and base values were determined by Boehm's titration method. And, the surface properties of ACs were studied by FT-IR and XPS analyses. Also, $N_2/77K$ adsorption isotherm characteristics, including the specific surface area and micropore volume were studied by BET and t-plot methods, respectively. From the adsorption tests of NO and $NH_3$, it was revealed in the case of acidic treatment on ACs that the $NH_3$ removal was more effective due to the increase of acidic functional groups in carbon surfaces. Also, the NO removal was increased, in the case of basic treatment, due to the improvement of basic functional groups, in spite of significant decreases of BET's specific surface area and total pore volume. It was found that the adsorption capacity of ACs was not only determined by the textural characteristics but also correlated with the surface functional groups in the acid-base intermolecular interactions.

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