• 제목/요약/키워드: solution-deposition

검색결과 862건 처리시간 0.035초

전기도금법으로 제조한 Ni-Fe 나노박막의 스트레스와 자기적 특성에 미치는 용액의 조건 및 전류밀도의 영향 (Effect of Bath Conditions and Current Density on Stress and Magnetic Properties of Ni-Fe Nano Thin Films Synthesized by Electrodeposition Methods)

  • 구본급
    • 한국표면공학회지
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    • 제44권4호
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    • pp.137-143
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    • 2011
  • The internal stress and magnetic properties (coercivity and squareness) of Ni-Fe nano thin film synthesized by electrodeposition method were studied as a function of acidic chloride bath conditions (composition and temperature) and current density. Fe deposition patterns were different depending on the temperature of the solution, the stress of film decreased with increasing the solution temperature, and the depending on the amount of Fe deposition showed a parabolic shape. The grain size of film was inversely proportional to stress of thin film. The internal stress of thin film and magnetic properties were deeply relevant, and the stress of thin film had a relationship with bath conditions and grain size of the thin film surface.

분무 열분해법에 의해 증착된 $SnO_2$ 박막의 광전기 화학 변환 특성 (Photoelectrochemical Conversion of $SnO_2$ Films Deosited by Spray Pyrolysis)

  • 김태희;박경봉;윤기현
    • 한국세라믹학회지
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    • 제28권3호
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    • pp.197-204
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    • 1991
  • The photoelectrochemical conversion in SnO2 films deposited by spray pyrolysis using SnCl4-alcohol solution and N2 gas has been studied. The photocurrent increases with increasing deposition temperature up to 40$0^{\circ}C$ and then decreases, and the electron affinity decreases as the deposition temperature increases to 40$0^{\circ}C$. As the concentration of the spray solution increases, the photocurrent reaches a maximum value at the concentration of 0.05M, and the electron affinity is consistent. As the thickness of the film increases, the photocurrent increases with a maximum value at the thickness of 4600$\AA$, and electron affinity does not change.

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Preparation of Crack-free YBCO Films by EPD on Silver

  • Soh, Dea-wha;Li, Young-mae;Korobova N.;Park, Sung-Jai
    • Journal of information and communication convergence engineering
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    • 제1권1호
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    • pp.27-30
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    • 2003
  • Electrophoretic deposition (EPD) of alcohol YBCO suspensions on the Ag wire electrode is studied. Poly(ethylene glycol) was coordinated to a structure formed by the EPD process with YBCO particles. The suspension is characterized in terms of zeta potential and conductivity. The d.c electric fields of 200-300 V/cm are applied for 1-10 min. The optimal condition for the EPD allows modifying the properties and microstructure of the deposited films. Superconducting coatings with nanometer-sized pores and a preferred orientation along the c-axis were prepared from the result with chemically modified precursor solution. In contrast, YBCO coatings of submicrometer-sized pores and randomly orientated grains were prepared from the solution without PEG.

Preparation of Non-cracking YBCO Films Using Eelectrophoretic Deposition

  • Soh, Deawha;Korobova, Natalya
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2004년도 SMICS 2004 International Symposium on Maritime and Communication Sciences
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    • pp.117-122
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    • 2004
  • Electrophoretic deposition (EPD) of alcohol YBCO suspensions on the Ag wire electrode was studied. Poly(ethylene glycol) was coordinated to a structure formed by the EPD process with YBCO particles. The suspension is characterized in terms of zeta potential and conductivity. The d.c electric fields of 200-300V/cm are applied for 1-10 min. The optimal condition for the EPD allows modifying the properties and microstructure of the deposited films. Superconducting coatings with nanometer-sized pores and a preferred orientation along the c-axis were prepared from the result with chemically modified precursor solution. In contrast, YBCO coatings of sub-micrometer sized pores and randomly orientated grains were prepared from the solution without PEG

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무전해 니켈 도금용액에 사용되는 안정제의 도금피막 특성에 미치는 영향 (The Effect of Stabilizers on the Characteristics of Deposit in the Electroless Nikel Plating)

  • 이홍기;손성호;전준미;구석본;허진영
    • 한국표면공학회지
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    • 제37권6호
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    • pp.335-343
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    • 2004
  • Bath stabilizers in the electroless nickel(EN) plating solution are known to prevent sudden bath decomposition and extend its lifetime. Further, every stabilizer has a different role and function in EN solution and it influences the surface structure. In this study, the effects of various stabilizers on the deposition rate, surface morphology, deposition content of phosphor and hardness were investigated.

전기영동 초전도 선재의 크랙발생 억제 (Control of Cracking on Superconducting Wire by Electrophoresis)

  • 소대화;이영매;조용준;김태완;박정철;코로보바나탈리아
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.270-273
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    • 2000
  • For the well-preparation of the superconducting wire by electrophoresis, the control of the cracking on the YBCO, BSCCO superconductor deposited on Ag wire in acetone and buthanol solution with PEG(poly-ethylenglycol) was investigated with XRD and SEM analysis. After deposition, drying and heat treatment process, the cracks on the deposited surface of YBCO and BSCCO samples was clearly removed and decreased, which was perpared in suspension with addition of PEG from 1 to 3ml. However, in the case of the addition rate of PEG in acetone suspension was exceeded in 3ml, BSCCO superconductor deposited on Ag wire was slightly melted at 90$0^{\circ}C$ which was the same heat treatment condition of other samples with different additin rate of PEG. In the process of electrophoretic deposition, drying and heat treatment, PEG added into the suspension solution as a binder was very useful to prepare the crack-free thick film-wire of YBCO and BSCCO.

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무전해 니켈도금에 의한 도전성 실리콘고무 시트의 제조 (Preparation of Conductive Silicone Rubber Sheets by Electroless Nickel Plating)

  • 이병우;이진희
    • 한국표면공학회지
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    • 제47권5호
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    • pp.269-274
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    • 2014
  • Electroless plating process as a solution deposition method is a viable means of preparing conductive metal films on non-conducting substrates through chemical reactions. In the present study, the preparation and properties of electroless Ni-plating on flexible silicone rubber are described. The process has been performed using a conventional Ni(P) chemical bath. Additives and complexing agents such as ammonium chloride and glycine were added and the reaction pH was controlled by NaOH aqueous solution. Ni deposition rate and crystallinity have been found to vary with pH and temperature of the plating bath. It was shown that Ni-films having the high crystallinity, enhanced adhesion and optimum electric conductivity were formed uniformly on silicone rubber substrates under pH 7 at $70^{\circ}C$. The conductive Ni-plated silicone rubber showed a high electromagnetic interference shielding effect in the 400 MHz-1 GHz range.

The effect of various parameters for few-layered graphene synthesis using methane and acetylene

  • Kim, Jungrok;Seo, Jihoon;Jung, Hyun Kyung;Kim, Soo H.;Lee, Hyung Woo
    • Journal of Ceramic Processing Research
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    • 제13권spc1호
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    • pp.42-46
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    • 2012
  • The effect of the parameters for few-layered graphene growth by thermal CVD on nickel substrate was investigated. Graphene can be synthesized by using different strategies. Chemical vapor deposition (CVD) has known as one of the most attractive methods to produce graphene due to its good film uniformity, compatibility and large scale production. The control of parameters such as temperature, growth time and pressure in CVD process has been widely recognized as the most important process in graphene growth. Different carbon precursors, methane and acetylene, were introduced in the quartz tube with a variety of growth conditions. Raman spectroscopy was used to confirm the presence of a few- or multi-layered graphene.

섬유질 필터내의 다분산 에어로졸 입자의 확산 침착에 관한 해석적 해 (Analytic Solutions to Diffusional Deposition of Polydisperse Aerosols in Fibrous Filters)

  • Gwon Sun-Park;Kim Hyeon-Tae;Lee Gyu-Won
    • 한국대기환경학회:학술대회논문집
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    • 한국대기환경학회 2001년도 추계학술대회 논문집
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    • pp.389-390
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    • 2001
  • Deposition of polydisperse aerosols by Brownian diffusion was studied analytically using the penetration efficiency of monodisperse aerosols combined with the correlations among the moments of lognormal distribution functions. The analytic solutions so obtained were validated using the exact solution were applied to recalculate the filtration efficiencies of the existing experimental data for various filtration conditions. (omitted)

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