• Title/Summary/Keyword: solution coating method

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Indium Sulfide and Indium Oxide Thin Films Spin-Coated from Triethylammonium Indium Thioacetate Precursor for n-Channel Thin Film Transistor

  • Dao, Tung Duy;Jeong, Hyun-Dam
    • Bulletin of the Korean Chemical Society
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    • v.35 no.11
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    • pp.3299-3302
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    • 2014
  • The In2S3 thin films of tetragonal structure and In2O3 films of cubic structure were synthesized by a spin coating method from the organometallic compound precursor triethylammonium indium thioacetate ($[(Et)_3NH]^+[In(SCOCH_3)_4]^-$; TEA-InTAA). In order to determine the electron mobility of the spin-coated TEA-InTAA films, thin film transistors (TFTs) with an inverted structure using a gate dielectric of thermal oxide ($SiO_2$) was fabricated. These devices exhibited n-channel TFT characteristics with a field-effect electron mobility of $10.1cm^2V^{-1}s^{-1}$ at a curing temperature of $500^{\circ}C$, indicating that the semiconducting thin film material is applicable for use in low-cost, solution-processed printable electronics.

Preparation of Highly Oriented ZnO Thin Films Prepared by Sol-Gel Method

  • Cheol Jeong;Hwang, Kyu-Seog;Moon, Jong-Ha;Kim, Byung-Hoon
    • The Korean Journal of Ceramics
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    • v.3 no.4
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    • pp.249-252
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    • 1997
  • Highly oriented ZnO thin films were fabricated by dip-coating technique using zinc acetate 2-methoxyethanol 2-aminoethanol solution as starting materials, and effects of substrates on the film's orientation were investigated. Product films were obtained by prefiring at 300, 400, 500 and 550℃ for 10 min, followed by final heat-treatment at the same temperatures as prefiring for 1h. c-axis oriented films on glass substrates were prepared by heat treatment of prefiring films at 300-550℃, while films on alumina showed polycrystalline structure. Films with c-axis orientation exhibited lower specific resistivities than those of polycrystalline films with partial crack and pore.

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Fabrication of a Polymeric Film with Nanofiber-based Porous Window and Its Application to Co-culture (섬유 기반의 다공성 윈도우를 가지는 박막 제작 및 공배양에의 활용)

  • Jeong, Young Hun;Lee, Jongwan;Jin, Songwan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.13 no.2
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    • pp.21-27
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    • 2014
  • Recently, various biochip environments have been presented. In this study, a novel transparent film with porous membrane windows, which is an essential component in a co-cultured biochip environment, is fabricated using spin-coating, 3D printing, and electrospinning processes. In detail, a transparent polystyrene film was fabricated by means of the spin-coating process followed bywindow cutting, after which apolycaprolactone-chloroform solution was deposited along the window edge to introduce an adhesion layer between the PS film and the PCL nanofibers. Nanofibers were electrospun into the window region using a direct-write electrospinning method. Consequently, it was demonstrated that the fabricated window film could be used in a co-culture biochip environment.

Preparation of $PbTiO_3$ Thin Films using Metal Alkoxide and Diethanolamine Complexing Agent (금속알콕사이드와 Diethanolamine 착체를 이용한 $PbTiO_3$ 박막 제조)

  • 김승현;한현규;오영제;김창은
    • Journal of the Korean Ceramic Society
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    • v.31 no.5
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    • pp.499-504
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    • 1994
  • PbTiO3 thin films were prepared by sol-gel spin coating method using metal alkoxide and diethanolamine (DEA). The precipitation of the PbTiO3 sol occurred at pH 7.3 with HNO3 addition, regardless of the amount of DEA. The gelation time of the PbTiO3 sol was reduced with increasing amount of HNO3 and/or water. When the PbTiO3 films prepared by 0.2 molar coating solution were annealed at $650^{\circ}C$ for 30 min, dense and single phase perovskite films were obtained. Dielectric constant and loss tangent of the film were 239 and 0.01 at 1 kHz, respectively.

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The application of hydrated fine MgO particles for flux pinning center in the HTS-BSCCO system

  • 김성환;김철진;정준기;박성창;유재무
    • Progress in Superconductivity
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    • v.3 no.2
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    • pp.188-192
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    • 2002
  • To introduce flux pinning center in HTS-BSCCO system, nano-size MgO particles were uniformly distributed within the Bi-2223 grain by partial hydration of MgO. The existing method MgO doped Bi-2223 used nato-size MgO powders, which resulted in agglomeration during mixing or grain growth during heat-treatment due to the high surface energy of the fine particles. By hydration of the MgO surface, the agglomeration of the MgO powders was avoided and the size of remaining MgO core was controlled by changing hydration medium and time. The thin film obtained by spin coating of (Bi_$1.8/Pb_{0.4}$)$Sr_2$$_{Ca}$$2.2/Cu_3$ $O_{y}$ nitrate solution mixed with hydrated MgO showed the even distribution of nano-size MgO particles in the Bi-2212 grains.s.s.

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PVP-assisted Synthesis of TiO2 Nanospheres and their Application to the Preparation of Superhydrophobic Surfaces

  • Munkhbaatar, Naranchimeg;Ryu, Ilhwan;Park, Dasom;Yim, Sanggyu
    • Applied Science and Convergence Technology
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    • v.24 no.6
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    • pp.219-223
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    • 2015
  • Enhancement of the surface hydrophobicity of polydimethylsiloxane (PDMS) thin films deposited on substrates covered with titanium dioxide ($TiO_2$) nanospheres was studied. First, a low-temperature solution-phase method using polyvinylpyrrolidone (PVP) as a surface capping agent and a water/dimethylformamide (DMF) mixture as the reaction medium was used to synthesize monodisperse $TiO_2$ nanospheres. It was possible to easily control hydrolysis rate of the Ti-precursors and the size of the synthesized nanospheres by varying the amount of PVP and the volume ratio of the solvent mixture. Spray coating of the synthesized $TiO_2$ nanospheres under the PDMS film increased the water contact angle of the film surface to $150.3^{\circ}$. This simple treatment can modify the surface morphology at a nanometer scale without any long or complicated nanoprocess; hence, the surface enters the superhydrophobic Cassie-Baxter regime.

Heat-resistant Enamel Varinish (내열성 에나멜 바니쉬)

  • Kim, Yang-Kook;Bae, Hun-Jai
    • Applied Chemistry for Engineering
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    • v.4 no.2
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    • pp.264-272
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    • 1993
  • Current research aimed at investigating of heat-resistance of magnet wire to endow miniaturizing electronic equipment with a high efficiency or reliability. Thermal stability of magnet wire has a close relationship with physical properties of polymeric coating that is formed from enamel varnish. Design of heat-resistant enamel varnish and coating technology of varnish solution were briefly described. Some factors which have a thermal effect on wire were discussed through the evaluation method of the wire properties.

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Fractal Analysis of the Surface in Thin Film Capacitors

  • Hong, Kyung-Jin;Min, Yong-Ki;Cho, Jae-Cheol
    • KIEE International Transactions on Electrophysics and Applications
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    • v.11C no.2
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    • pp.18-22
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    • 2001
  • The thin films of high permitivity in ferroelectric materials using a capacitor are applied to DRAMs and FRAMs. (Ba, Sr)TiO$_3$ thin as ferroelectric materials were prepared by the sol-gel method and made by spin-coating on the Pt/Sio$_2$/Si substrate at 4,000 [rpm] for 10 seconds. The structural characteristics of the surface were analyzed by fractal dimension. The thickness of BST ceramics thin films was about 260∼280 [nm]. The property of the leakage current was stable with 10-9∼10-11[A] when the applied voltage was 0∼3[V]. BST thin films ha low leakage current properties when fractal dimension was low and a coating area was high.

Solution-processible corrugated structure and scattering layer for enhanced light extraction from organic light-emitting diodes

  • Hyun, Woo Jin;Im, Sang Hyuk;Park, O Ok;Chin, Byung Doo
    • Journal of Information Display
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    • v.13 no.4
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    • pp.151-157
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    • 2012
  • A simple method of fabricating out-coupling structures was demonstrated via solution-processing to enhance light extraction from organic light-emitting diodes (OLEDs). Scattering layers were easily obtained by spin-coating an $SiO_2$ sol solution that contained $TiO_2$ particles. By introducing the scattering layer and the solution-processible corrugated structure as internal and external extraction layers, the OLEDs showed increased external quantum efficiency without a change in the electroluminescence spectrum compared to conventional devices. Using these solution-processible out-coupling structures, nearly all-solution-processed OLEDs with enhanced light extraction could be fabricated. The light extraction enhancement is attributed to the suppression by the out-coupling structures of the light-trapping that arose at the interface of the glass substrate and the air.

Development of Spray Thin Film Coating Method using an Air Pressure and Electrostatic Force (공압과 정전기력을 이용한 스프레이 박막 코팅 기술 개발)

  • Kim, Jung Su;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.6
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    • pp.567-572
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    • 2013
  • In many electro-devices, the vacuum process is used as the manufacturing process. However, the vacuum process has a problem, it is difficult to apply to a continuous process such as a R2R(roll to roll) printing process. In this paper, we propose an ESD (electro static deposition) printing process has been used to apply an organic solar cell of thin film forming. ESD is a method of liquid atomization by electrical forces, an electrostatic atomizer sprays micro-drops from the solution injected into the capillary with electrostatic force generated by electric potential of about several tens kV. The organic solar cell based on a P3HT/PCBM active layer and a PEDOT:PSS electron blocking layer prepared from ESD method shows solar-to-electrical conversion efficiency of 1.42% at AM 1.5G 1sun light illumination, while 1.86% efficiency is observed when the ESD deposition of P3HT/PCBM is performed on a spin-coated PEDOT:PSS layer.