• 제목/요약/키워드: solution coating method

검색결과 544건 처리시간 0.024초

Synthesis of $SiO_2$ nanoparticles self-assembled thin film by organic.inorganic hybrid method

  • Hu, Yi;Lyu, Jhong-Ming;Liu, Tung-Cheng;Liu, Jiun-Shing
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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    • pp.1538-1541
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    • 2009
  • Amphiphobic thin films for touched panel application was prepared by $SiO_2$ nanoparticles self-assembled nanostructure. Silicon dioxide nano spheres were prepared by sol-gel method and well dispersed in a solution with surfacants of low surface energy. Nanostrcture thin films were obtained by spin coating technologies.

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Self-patterning 기술을 이용한 강유전체 메모리 전극용La0.5Sr0.5CoO3박막의 제조에 관한 연구 (A Study on Fabrication of La0.5Sr0.5CoO3Thin Films as an Electrode for Ferroelectric Memory by Self-patterning Technique)

  • 손현수;김병호
    • 한국세라믹학회지
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    • 제40권2호
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    • pp.153-158
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    • 2003
  • Photosensitive sol solution을 이용한 self pattern된 박막은 photoresist/dry etching process에 비해 박막의 제조과정이 간단하다는 장점을 가지고 있다. 이 연구에서는 강유전성 메모리소자의 산화물 전극재료로 사용되고 있는 La$_{0.5}$Sr$_{0.5}$CoO$_3$(LSCO)극 photosensitive sol solution을 이용하여 spin coating법으로 제조하였으며 출발원료는 La-2methoxyethoxide, Sr-ethoxide, Co-2methoxyethoxide를 사용하였다. LSCO gel 박막에 UV 노광시간을 증가시킴에 따라 M(metal)-O-M 결합이 생성되면서 metal $\beta$-diketonate의 UV 흡수 피크 강도는 감소되었고 LSCO gel 박막에 UV조사에 따른 용해도 차이가 생기면서 fine patterning 을 얻을 수 있었다. 68$0^{\circ}C$ 이상의 온도로 대기 중에서 열처리된 LSCO 박막은 perovskite 상을 나타내었고 74$0^{\circ}C$에서 가장 낮은 비저항값(4$\times$10 ̄$^3$Ωcm)을 얻을 수 있었다.

Comparison between Basic and Inverse Dual Drug and Peptide-coated Stents in a Porcine Restenosis Model

  • Jang, Eun-Jae;Lee, So-Youn;Bae, In-Ho;Park, Dae Sung;Jeong, Myung Ho;Park, Jun-Kyu
    • 공업화학
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    • 제31권5호
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    • pp.502-508
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    • 2020
  • Dual drug-eluting stents (DES) is a primary treatment method for coronary arterial diseases in current interventional cardiology practice. However, their pathological results according to the sequence of coating of drugs have not been reported yet. The peptide-dopamine dissolved in acetonitrile was coated onto the Chonnam National University Hospital (CNUH) stent using an electrospinning coating machine. For secondary coating (e.g., sirolimus coating, designated as SPS), sirolimus (SRL) and poly lactic-glycolic acid (PLGA) were mixed in tetrahydrofuran (THF), and the solution was then coated on the CNUH stent that had underwent the primary peptide coating using an electrospinning and spray technique. Next, the peptide-dopamine was coated on the SRL-PLGA coated stent (PSS). In this study, it was confirmed that endothelialization was promoted without being significantly affected by the coating order (SPS or PSS). The sequence of drug and peptide coating may affect the development of restenosis and PSS was effective in the prevention of restenosis compared to that of using SPS.

자체-감지능 및 광투과도를 지닌 CNT 및 ITO/PET 다기능성 나노복합소재의 계면 조절 연구 (Interfacial Control of Multi-functional CNT and ITO/PET Nanocomposites having Self-Sensing and Transparency)

  • 왕작가;권동준;구가영;박종만
    • Composites Research
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    • 제24권1호
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    • pp.45-50
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    • 2011
  • 자체-감지능 있는 다기능성 나노복합소재를 위해, 투명하고 전도성 있는 카본나노튜브 (CNT)로 코팅된 폴리에틸렌 테레프탈레이트(PET)를 함침 방법으로 제조하였다. CNT 코팅의 전기적 광학적 특정의 변화는 함침 횟수와 CNT용액의 농도에 주로 의존하였다. 결과적으로, CNT 코팅의 표면저항과 투과도는 제조공정의 변수들에 따라 예민하게 조절되었다. CNT 코팅의 표면저항은 4점법과 이중 배열법에 의해 측정되었으며, 광학적 투과도는 UV 스펙트럼을 사용하여 평가하였다. CNT 코팅의 표면특성을 측정한 정적 및 동적 접촉각은 상호 일치함을 보여주었다. 함침 코팅수가 증가함에 따라, CNT코팅한 PET의 표면저항은 현저하게 저하했으나, 투명도는 CNT 네트워크의 특성으로 거의 감소하지 않았다. CNT와 인듐틴옥사이드 (ITO)의 계면 및 전기적 특성들은 피로 시험을 통하여 비교하였다. CNT는 2000회 반복 후에도 표면저항의 변화가 없는 반면에, ITO는 1000회 반복까지 표면저항의 급격한 증가를 보여주었다가 안정화하였다. 이는 형상비가 큰 CNT는 전기 접촉점을 계속 유지하는 반면에, 취성이 있는 ITO는 미세 균열이 발생하여 전지 접촉점을 많이 상실하기 때문이다.

평면형 마이크로 가스센서 (Planar-Type Micro Gas Sensor)

  • 이상윤;정완영;이덕동
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 추계학술대회 논문집
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    • pp.101-104
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    • 1998
  • A new planar-type micro gas sensor was designed and fabricated on silicon substrate and the operating characteristics of the sensor were investigated. The thin sensitive film of the sensor was fabricated by spin-coating of the SnO$_2$ sol solution which was synthesized by hydrothermal method. The spin-coating method for preparation of sensing layer was adopted to improve the long-term stability of the fabricated sensing film instead of physical methods such as rf sputtering and thermal evaporation. The fabricated microsensor showed a fairly good sensing performance for CO gas in air at 250$^{\circ}C$ The sensitivity(S=Ra/Rg) was shown to be about 5 to 2000ppm CO with heating power of 50mW.

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PEDOT:PSS Thin Films with Different Pattern Structures Prepared Using Colloidal Template

  • Yu, Jung-Hoon;Lee, Jin-Su;Nam, Sang-Hun;Boo, Jin-Hyo
    • Applied Science and Convergence Technology
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    • 제23권5호
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    • pp.254-260
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    • 2014
  • Organic solar cells have attracted extensive attention as a promising approach for cost-effective photovoltaic devices. However, organic solar cell has disadvantage of low power conversion efficiency in comparison with other type of solar cell, due to the recombination ratio of hole and electron is too large in the active layer. Thus we have change the surface structure of PEDOT:PSS layers to improve the current density by colloidal lithography method using various-size of polystyrene sphere. The two types of coating method were applied to fabricate the different pattern shape and height, such as spin coating and drop casting. Using the organic solvent, we easily eliminate the PS sphere and could make the varied pattern shapes by controlling the wet etching time. Also we have measured the electrical properties of patterned PEDOT:PSS film to check whether it is suitable for organic photovoltaics.

MOD 공정으로 제조된 고임계전류 YBCO 후막 (High-Ic YBCO thick film fabricated by the MOD process)

  • 신거명;송규정;문승현;유상임
    • 한국초전도ㆍ저온공학회논문지
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    • 제10권1호
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    • pp.6-9
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    • 2008
  • We have investigated the MOD process successfully for the fabrication of the YBCO thick film on the $LaAlO_3$(001) single crystalline substrate. The cracking problem in YBCO thick film, a serious problem in the conventional TFA-MOD method, could be overcome with a careful control of precursor materials. Thus coating solution was prepared for the YBCO thick film by using fluorine-free precursor material. The precursor solutions were coated on the LAO(001) single crystalline substrate using the dip coating method, calcined at the temperature up to $500^{\circ}C$, and fired at various high temperatures for 2 h in a reduced oxygen atmosphere. Optimally processed YBCO thick film exhibited high critical current($I_c$) over 200 A/cm-width at 77K in self-field.

다중 졸-겔 방법에 의해 증착된 ZnO 막의 형태적 및 구조적 특성평가 (Morphological and Structural Characterization of ZnO Films Deposited by Multiple Sol-Gel Methods)

  • 사키브 무하마드;김우영
    • 한국응용과학기술학회지
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    • 제40권5호
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    • pp.1116-1125
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    • 2023
  • 산화아연 막은 투명한 전도성 물질로써 다양한 분야의 광전자소자에 이용되고 있다. 그러므로 산화아연 막의 특성을 규명하는 것은 광전자소자의 성능을 높이는데 매우 중요한 역할을 할 것이다. 본 논문에서는 이러한 산화아연 막을 용액공정 기반으로 제작하여 형태적, 구조적 특성을 평가하고자 한다. 구체적으로는 졸-겔 방법을 반복적으로 시행하여, 시행 횟수에 따른 산화아연 막의 물성의 변화를 관찰할 것이다. 일정한 용액 조건하에서, 5회의 반복적인 졸-겔 방법을 시행한 결과 결정화가 진행되는 것을 확인하였다. 7회 이상에서는 원소 구성 및 결정화도가 특정 값에 수렴하는 경향을 보였다. 최종적인 산화아연 막의 평균결정의 크기는 약 10.7 nm 정도로 계산되었다. 본 연구를 통해 최적의 결정화를 보이는 공정횟수는 7회였다. 본 연구 결과 및 방법론은 다양한 용액공정 변수를 가변시키면서 적용할 수가 있고 최적의 공정조건을 확립하는데 기여할 것으로 기대한다.

Structural and Electrical Features of Solution-Processed Li-doped ZnO Thin Film Transistor Post-Treated by Ambient Conditions

  • Kang, Tae-Sung;Koo, Jay-Hyun;Kim, Tae-Yoon;Hong, Jin-Pyo
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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    • pp.242-242
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    • 2012
  • Transparent oxide semiconductors are increasingly becoming one of good candidates for high efficient channel materials of thin film transistors (TFTs) in large-area display industries. Compare to the conventional hydrogenated amorphous silicon channel layers, solution processed ZnO-TFTs can be simply fabricated at low temperature by just using a spin coating method without vacuum deposition, thus providing low manufacturing cost. Furthermore, solution based oxide TFT exhibits excellent transparency and enables to apply flexible devices. For this reason, this process has been attracting much attention as one fabrication method for oxide channel layer in thin-film transistors (TFTs). But, poor electrical characteristic of these solution based oxide materials still remains one of issuable problems due to oxygen vacancy formed by breaking weak chemical bonds during fabrication. These electrical properties are expected due to the generation of a large number of conducting carriers, resulting in huge electron scattering effect. Therefore, we study a novel technique to effectively improve the electron mobility by applying environmental annealing treatments with various gases to the solution based Li-doped ZnO TFTs. This technique was systematically designed to vary a different lithium ratio in order to confirm the electrical tendency of Li-doped ZnO TFTs. The observations of Scanning Electron Microscopy, Atomic Force Microscopy, and X-ray Photoelectron Spectroscopy were performed to investigate structural properties and elemental composition of our samples. In addition, I-V characteristics were carried out by using Keithley 4,200-Semiconductor Characterization System (4,200-SCS) with 4-probe system.

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정량 주입(Pre-metered) 코팅 방식을 이용한 유기 트랜지스터 반도체 박막 제작 연구 (Organic Semiconducting Thin Films Fabricated by Using a Pre-metered Coating Method for Organic Thin Film Transistors)

  • 조찬연;전홍구;최진성;김윤기;임종선;정준영;조성윤;이창진;박병주
    • 한국전기전자재료학회논문지
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    • 제25권7호
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    • pp.531-536
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    • 2012
  • We herein present results of flat and uniform polymer-blended small molecular semiconductor thin films. Which were produced for organic thin film transistors (OTFTs), using a simple pre-metered horizontal dipping process. The organic semiconducting thin films were composed of 6,13-bis(triisopropylsilylethynyl)-pentacene (TIPS-PEN) composite blended with a polymer binder of poly(${\alpha}$-methylstyrene) (PaMS). We show that the pre-metered horizontal-dip-coating(H-dip-coating) process allowed the critical control of the thickness of the blended TIPS-PEN:PaMs thin film. The fabricated OTFTs using the TIPS-PEN:PaMs films exhibited maximum field-effect mobility of $0.22\;cm^2\;V^{-1}\;s^{-1}$. These results demonstrated that H-dip-coated TIPS-PEN:PaMS films show considerable promise for the production of reliable, reproducible, and high-performance OTFTs.