• Title/Summary/Keyword: solution casting

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Research on the Adhesion of Flexible Copper Clad Laminates According to Species of Polyimide (폴리이미드 종류에 따른 연성 동박 적층판의 부착력 연구)

  • Lee Jae Won;Kim Sang Ho
    • Journal of Surface Science and Engineering
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    • v.38 no.2
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    • pp.49-54
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    • 2005
  • Flexible copper clad laminates (FCCL) fabricated by sputtering has advantages in fine pitch etching and dimensional accuracy than previous casting or laminating type FCCL, But its lower adhesion is inevitable technical challenge to solve for commercializing it. Chromium (Cr) which strongly reacts with O moiety was used as tie-coating layer in order to improve low adhesion between copper (Cu) and polyimide (PI). Sputtering raw polyimide (SRPI) and casting raw polyimide (CRPI) were used as substrates at this research. PI was pretreated by plasma before sputtering, and each sample was varied with RF power and Cr thickness on sputtering. Peel strength of the FCCL on SRPI was higher than that on CRPI. Adhesion had maximum value when 10 nm of Cr was deposited on SRPI by RF power of 50 W. It seems to be by the formation of Cu-Cr-O solid solution at the metal-PI interface.

Study on the Microstructural Changes with Modification and Cast-forging in Eutectic Al-Si Alloys (공정 Al-Si 합금의 개량처리와 주단조에 의한 조직변화에 관한 연구)

  • Yoon, Ji-Hyun;Seol, Eun-Cheol;Park, Seung-Min;Lee, Kwang-Hak
    • Journal of Korea Foundry Society
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    • v.22 no.1
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    • pp.17-25
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    • 2002
  • Recently, many studies have been carried out to process on the purpose of lightness in a transport parts because of the saving energy, the environmental problem. The cast-forging process can be expected to lower costs without decreasing the mechanical properties. So, the finest microstructure is needed to get for applying the cast-forging process with Al-Si alloy because the microstructure affects to the cast-forging process. For refinement treatment of eutectic Si and Al solid-solution phase, Sr and TiB were added in Al-Si alloys. The finest microstructure could be observed when 0.075 wt.%Sr and 0.1 wt.%TiB were added respectively. In this case, tensile strength and elongation much more increased than as casting. After high temperature deformation simulation test with grain refinement specimens was carried out, about 70N per unit $area(mm^2)$ of specimen was confirmed. After hot forging, tensile strength and elongation were increased. It was considered because casting defect was removed by compressive working.

Morphology and Swelling Behaviors of PVA/Gelatin Blend Membranes Prepared Under High Electric Field (고전장하에서 제조된 PVA/Gelatin 블렌드막의 구조와 팽윤거동)

  • Huh, Yang-Il;Yun, Hyung-Ku
    • Polymer(Korea)
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    • v.30 no.6
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    • pp.563-567
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    • 2006
  • Poly(vinyl alcohol) (PVA) and gelatin (GEL) blend membranes were prepared by solution casting method under a high electric field. SEM observation of the membrane showed that gelatin rich domains were elongated and oriented to the direction of the applied electric field in PVA matrix. This can be attributed to the electrostatic emulsifying effects due to a reduction in interfacial tension. In addition, it was observed through WAXD and swelling measurements that the degree of crystallinity of membranes increased with applied electric field strength. This may be interpreted to be caused by the orientation effect of GEL domains in the blend membrane, and the self-annealing effect due to some heat generated from high electric field during casting.

Lot Planning & Scheduling in the Integrated Steelmaking Process

  • Park Hyungwoo;Hong Yushin
    • Proceedings of the Korean Operations and Management Science Society Conference
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    • 2002.05a
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    • pp.109-113
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    • 2002
  • Steel industry is the most capital intensive and the largest energy consuming industry, which operate huge and complex facilities to supply various steel products as the primary materials to almost every manufacturing industry Major steel products are hot-rolled and cold-rolled coils, plates, and wires that are produced through molten iron making, molten steel making, casting, and rolling. Each process runs in batch between setups and the specifications or bach are different with each other High energy consuming and heavy material handling require careful synchronization or processes, as well. Considering the synchronization or processes, the lot planning and scheduling problem in the integrated steelmaking process rovers the roll grouping with given casts. the sequencing or rolls over time, and the machine assignment and time scheduling or charges and casts. The problem is investigated by dividing it into two cases whether single or parallel machines at the molten steel making and the continuous casting processes. Problem descriptions and solution approaches or each instance are introduced. To test their performance and conformity, implementation or the algorithms and numerical experiments are carried out with real world and constructed data sets.

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Effect of Heat Treatment on the Mechanical Properties of Investment Casting Turbo Charger Wheel using A356 Alloy (A356합금을 이용한 정밀주조 Turbo Charger Wheel의 기계적 특성에 미치는 열처리의 영향)

  • Kim, Sang-Mi;Woo, Kee-Do;Kim, Ji-Young;Kim, Sang-Hyuk;Park, Sang-Hoon;Kang, Hwang-Jin;Park, Chan-Sung
    • Journal of Korea Foundry Society
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    • v.31 no.5
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    • pp.262-266
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    • 2011
  • The aim of this study is to investigate aging behavior of A356 alloy for turbo charger part. The specimen was fabricated by investment casting. Solution heat treatment was performed at $525^{\circ}C$ for 8h and followed by aging treated at $160^{\circ}C$, $170^{\circ}C$ for 0.5~20h. And their microstructures and mechanical properties of the aged specimens were analyzed by scanning electron microscope and hardness tester, respectively. All the cast A356 alloy included eutectic Si particles. In the cast A356 alloy, eutectic Si phase mainly was formed along Chinese script phase. Vickers hardness of the cast was improved by aging treatment due to formation of ${\beta}$" phase and ${\beta}$' phase.

Dielectric properties of P(VDF/TrFE) copolymers thin films prepared by Casting method (Casting 법으로 제조된 P(VDF/TrFE) 공중합체 박막의 유전 특성)

  • Yoon, J.H.;Chung, M.Y.;Lee, S.W.;Park, S.H.;Kim, J.T.;Kim, B.S.;Lee, D.C.;Lim, E.C.;Choi, C.S.
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.1631-1633
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    • 2000
  • A study was carried out on the effect of VDF mol%, on the phase transition presented by P(VDF/TrFE) copolymer cast from dimethylformamide(DMF) solution with molar ratios 70/30 and 80/20. The results from dielectric spectrum and differential scanning calorimetry(DSC) showed that the phase transitions from ferroelectric to paraelectric phase(Curie transition) were observed The Curie point slightly has shifted to high temperature with increasing in VDF mol%, however, the melting point has shifted to low temperature.

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Fabration of PLC susbstrate by slurry filling and sandblasting Method (Tape casting법과 Sandblasting법을 이용한 광소자용 기판 제조 (1))

  • 조윤희;김응석;이용호
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.341-345
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    • 2001
  • In this study, nano-sized powders of SiO$_2$-0∼15mo1%B$_2$O$_3$ composition were prepared by sol-gel processing method using TEOS(Tetra ethyl ortho silicate) and H$_3$BO$_3$ solution. The powders were tape-cast on High silicate glass sheet(HSG) substrate and sintered to form a layer of undercladding for the planar light wave module. During the sol-gel processing, H$_2$O/Si mole ratio were varied to modify the size of the powders in a range from 600 to 75nm. The dispersion of the powder was modified by changing the pH of the slurry. Sintering temperature of the tape was observed to decrease with the size of the powder and the B$_2$O$_3$ content in the powder. When the silica powders of 75∼125nm in diameter containing 15mo1% B$_2$O$_3$ were used, 98 TD% was obtained at 1250$^{\circ}C$, which is approximately 300$^{\circ}C$ reduction in sintering temperature compared with micrometer-sized powders.

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Effect of Cu on Hot Ductility Behavior of Low Carbon Steel (저탄소강의 열간 연성 거동에 미치는 Cu의 영향)

  • Son, Kwang Suk;Park, Tae Eun;Park, Byung-Ho;Kim, Donggyu
    • Korean Journal of Metals and Materials
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    • v.47 no.4
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    • pp.217-222
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    • 2009
  • Cu as a tramp element has been reported to encourage transverse cracking upon straightening operation during continuous casting or mini-mill processing. Therefore, the hot workability of steels containing Cu should be investigated. The purpose of the present study was to examine the effect of Cu contents on the hot ductility of low carbon steels by using hot compression test. Hot compression test was carried out using a Gleeble. The specimens were heated to $1300^{\circ}C$ for solution treatment and then held for 300s before cooling at a rate of $1^{\circ}C/s$ to test temperatures in the range of $650{\sim}1150^{\circ}C$ ($50^{\circ}C$ intervals) with strain rate of $5{\times}10^{-3}/s$. In Cu containing steels, the hot ductility was decreased with increasing Cu content at high temperature region which is to be attributed to copper enriched phase formed at scale/steel interface, and low hot ductility with increasing Cu content at low temperature region is attributable to the strengthening of matrix by the formation of ${\varepsilon}-Cu$. The width of ductility trough region was decreased with increasing Cu content.

Effect of Austenitizing Ratio on the Delta Ferrite Volume Fraction and Corrosion Resistance of Shell Mold Cast SSC13 Elbow Fitting (셀 몰드 주조한 SSC13 엘보우 피팅 주강의 고용화율에 따른 델타 페라이트 분율 변화와 내부식특성)

  • Kim, Kuk-Jin;Lim, Su-Gun;Ju, Heong-kyu;Pak, Sung-Joon
    • Journal of Korea Foundry Society
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    • v.35 no.5
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    • pp.109-113
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    • 2015
  • In this study, the measurement of FN (ferrite volume fraction) and the solution annealing ratio at a temperature of $1130^{\circ}C$ were determined with 15A elbow fittings of shell cast SSC13, and the corrosion resistance with and without austenitizing solution annealing were investigated in comparison with AISI304. The delta ferrite phase was observed in the material due to the slow cooling effect of the shell mold casting. However, the delta ferrite phase decreased gradually with the solution annealing at a temperature of $1130^{\circ}C$. The hardness generally decreased with a heat treatment; however, its corrosion resistance was improved with the heat treatment. In addition, when a passivation treatment was applied, its corrosion ratio showed the lowest value. The pattern of general corrosion decreased due to the decrease in the delta ferrite phase with the solution annealing treatment. Consequently, it is suggested that the corrosion resistance of SSC13 elbow fittings can be improved by increasing the ratio of any solution annealing treatment used and by decreasing the ferrite phase. The relationship between the ratio of solution annealing and delta ferrite is expressed as follows: SA (solution annealing ratio,%) = 98 - FN (ferrite volume fraction, %).

Evaluation of a metal level in non-precious metal alloys dental casting having beryllium by lactic acid Solution (베릴륨함유 치과 주조용 비귀금속 합금의 젖산용액에 의한 금속 노출수준 평가)

  • Park, Soo-Chul;Jang, Eun-Jin;Han, Sok-Yoon
    • Journal of Technologic Dentistry
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    • v.33 no.2
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    • pp.121-128
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    • 2011
  • Purpose: The purpose of this study is to investigate the level of each metal in non-precious metal alloys dental casting, still used even banned for use and trade by the law, for oral health. Methods: Two kinds of metal alloys were analyzed. One was Ticonium 100 for removable prosthesis and the other was Rexillium V for dental porcelain. Two samples of each metal alloy were made in 0.5g, 1.0g, and 1.5g. Total number of samples were 12. Two kinds of lactic acid Solution, pH7 and pH4.6, were injected into each samples. After injection, each samples had been for 21days ${\pm}$ 1 hour in the water tank of which temperature was $37^{\circ}C$. The level of metal was measured in each sample by inductively couplled plasma-atomic emission spectrometer. Results: In both metal alloys, metals, chrome, nickel, beryllium, and molybdenum, were founded. In Ticonium 1000, the highest level of nickel was 2.531ppm in 1.5g pH4.6 sample while the highest level of nickel was 4.062ppm in 1.5g pH4.6 sample of Rexillium V. In chemical composition of these methal alloys, chrome(14~17%) was much more than beryllium(1.95~1.99%) and molybdenum(5.0~9.0%) but berllium and molybdenum were founded more than chrome in samples. Therefore, chrome showed better anti-corrosion than other metal alloys. In both metal alloys, more metals were founded in higher pH level and more mass. Levels of chrome was significantly different in samples of both metal alloys in each pH level(p<0.05). Levels of nickels was significantly different in samples of both metal alloys in each pH level(p<0.05). Conclusion: For oral health, further studies are needed in nickel-chrome metal alloy and cobalt metal alloy of non-beryllium in addittion to beryllium metal alloy and also long-term studies needed in various period and other non-percious metal alloys for dental casting.