• Title/Summary/Keyword: solution accuracy

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The simultaneous determination of germanium and selenium in plant by hydride vapour generator inductively coupled plasma mass spectrometry (HVG-ICPMS을 이용한 식물체 중 게르마늄과 셀레늄의 동시분석 연구)

  • Ham, Yong-Gyu;Kim, Bo-Kyong;Kwon, Young-Uk;Baek, Hyo-Hyu;Lee, Seok-Ki
    • Analytical Science and Technology
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    • v.24 no.3
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    • pp.159-167
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    • 2011
  • In this study, the hydride vapour generator inductively coupled plasma mass spectrometry (HVGICPMS) was applied as the new analytical method to show the high accurate and reproductive data analysing the amounts of selenium and germanium being existed inside a system of plant. In order to decrease the interference effects, such as ion and molecular interference. Mini torch was used into the ICPMS instead of the conventional torch. At conditions of the different kinds and concentrations of acid solution, the different reductive conditions for composing hydride, and the different methods for making ash, the contents of selenium and germanium in lettuce were analysed. The inspection of yields and data comparison from SRM-1574 and -1570a were used for increasing the accuracy of this analysis.

A STUDY OF TROPOSPHERIC EFFECT ON HIGH PRECISION GPS HEIGHT DETERMINATION

  • Wang, Chuan-Sheng;Liou, Yuei-An
    • Proceedings of the KSRS Conference
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    • 2007.10a
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    • pp.382-385
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    • 2007
  • Constantly enhancing positioning accuracy by the Global Positioning System (GPS) technique is of great importance, but challenging, especially after the GPS positioning technique has been improved considerably during the past two decades. The associated main error sources have been reduced substantially, if not eliminated. Troposhpeic influence with its highly temporal and spatial variability appears to be one of the major error sources. It is hence an increased interest among GPS researchers to reduce the tropospheric influence or delay. Two techniques have been commonly implemented to correct the tropospheric impact. The first technique, known as parameter estimation, characterizes the path delay with empirical models and the parameters of interest are determined from the GPS measurements. The second strategy, termed as external correction, involves independent path delay measurements. The present study is an integration of both techniques in which the parameter estimation as well as external correction are used to correct the path delay for $110{\sim}210$ km range baselines. Twenty-four parameters have been obtained in 24 hours solution by setting the cutoff angle at 3 and 15 degrees for parameter estimation strategy. Measurements from meteorological instruments and water vapor radiometer (WVR) are applied in the GPS data processing, separately, as an external strategy of present research work. Interesting results have been found, indicating more stable repeatability in baseline when the external correction strategy is applied especially with the inclusion of WVR observations. The offset of an order of 1 cm is found in the baselines determined by the two strategies. On the other hand, parameter estimation exhibits more stable in terms of GPS height repeatability. The offset in the GPS height determined by the two strategies is on the order of few centimeters.

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A Case Study of Mixed-Mode Design Incorporated Mobile RDD into Telephone RDD (유·무선 RDD를 결합한 혼합조사설계: 2011 서울시장 보궐선거 예측조사 사례 연구)

  • Lee, Kay-O;Jang, Duk-Hyun;Hong, Young-Taek
    • The Korean Journal of Applied Statistics
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    • v.25 no.1
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    • pp.153-162
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    • 2012
  • We proposed a mixed-mode design with a landline survey and mobile survey as the solution for the problems of election opinion polls by the original telephone survey method, mostly with limited population coverage for young people not living at home and with lower efficiency in selecting valid voters. We numerically verified the applicability of the proposed dual frame survey by analyzing the preliminary opinion poll results of the Seoul mayor by-election of October 26 2011. This research achieved the result that relative standard errors were similar between a mobile RDD sample and landline RDD sample though the variance was bigger in the former. Though the combination of mobile RDD and landline RDD is not found to improve the forecast accuracy, it still is expected to have higher reliability for election polls by expanding the population coverage and compensating the weakness of each survey method.

Fabrication of Master for a Spiral Pattern in the Order of 50nm (50nm급 불연속 나선형 패턴의 마스터 제작)

  • Oh, Seung-Hun;Choi, Doo-Sun;Je, Tae-Jin;Jeong, Myung-Yung;Yoo, Yeong-Eun
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.4
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    • pp.134-139
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    • 2008
  • A spirally arrayed nano-pattern is designed as a model pattern for the next generation optical storage media. The pattern consists off types of embossed rectangular dot, which are 50nm, 100nm, 150nm and 200nm in length and 50nm in width. The height of the dot is designed to be 50nm. The pitch of the spiral track of the pattern is 100nm. A ER(Electron resist) master for this pattern is fabricated by e-beam lithography process. The ER is first spin-coated to be 50nm thick on a Si wafer and then the model pattern is written on the coated ER layer by e-beam. After developing this pattern written wafer in the solution, a ER pattern master is fabricated. The most conventional e-beam machine can write patterns in orthogonal way, so we made our own pattern generator which can write the pattern in circular or spiral way. This program generates the patterns to be compatible with the e-beam machine from Raith(Raith 150). To fabricate 50nm pattern master precisely, a series of experiments were done including the design compensation for the pattern size, optimization of the dose, acceleration voltage, aperture size and developing. Through these experiments, we conclude that the higher accelerating voltages and smaller aperture size are better for mastering the nano pattern which is in order of 50nm. With the optimized e-beam lithography process, a spiral arrayed 50nm pattern master adopting PMMA resist was fabricated to have dimensional accuracy over 95% compared to the designed. Using this pattern master, a metal pattern stamp will be fabricated by Ni electro plating for injection molding of the patterned plastic substrate.

Structural Optimization Using Equivalent Static Loads and Substructure Synthesis Method (등가정하중법과 부분구조합성법을 이용한 구조최적설계)

  • Choi, Wook Han;Na, Yoo Sang;Park, Gyung-Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.8
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    • pp.823-830
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    • 2015
  • Structural optimization pursues improved performance of structures. Nowadays, structural optimization is applied to the design of huge and complex structures such as an airplane. As the number of the finite elements is increased, the analysis solution becomes more accurate. However, the design cost using the finite element model is significantly increased. The component mode synthesis method that is using the substructure synthesis method is frequently employed in order to keep the accuracy and reduce the cost. A new design method for structural optimization is proposed to reduce the design cost and to consider the dynamic effect of the structure. The proposed method reduces the design cost by applying the equivalent static loads on the design domain. An example of linear dynamic response optimization is solved and the efficiency of the proposed method is demonstrated.

Variable Passive Compliance Device for Robotic Assembly (조립 로봇용 가변 수동 강성 장치의 설계)

  • Kim, Hwi Su;Park, Dong Il;Park, Chan Hun;Kim, Byung In;Do, Hyun Min;Choi, Tae Yong;Kim, Doo Hyung;Kyung, Jin Ho
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.25 no.6
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    • pp.517-521
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    • 2016
  • General industrial robots are difficult to use for precision assembly because they are operated based on position control. Their position accuracy is also usually higher than the assembly clearance (several tens of ${\mu}m$). In previous researches, force control was suggested as a robotic assembly solution. However, this method is difficult to apply in reality because of speed and cost problems. The RCC provides high speed, but applications are limited because the compliance is fixed, and it cannot detect an assembly condition during a task. A variable passive compliance device (VPCD) was developed herein. The VPCD can detect the assembly condition during tasks. This device can provide proper compliance for successful assembly tasks. The pneumatic system and the Stewart platform with an LVDT sensor were applied for measuring the displacement and variable compliance, respectively. The concept design and analysis were conducted to prove the effectiveness of the developed VPCD.

A Rapid, Simple Determination of Sulfur-containing Compounds and Methylmalonic Acid on Plasma using GC-MS-SIM for the Diagnosis of Homocysteinemia (혈장 중 황함유 화합물과 메틸말론산의 신속 간편한 분석법 개발; GC-MS-SIM을 이용한 호모시스테인혈증의 진단)

  • Yoon, Hye-Ran;Thapa, Maheshwor
    • Journal of The Korean Society of Inherited Metabolic disease
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    • v.15 no.3
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    • pp.138-146
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    • 2015
  • Purpose: If early diagnosis is not made, patients with metabolic disorders as homocystinemia rapidly progress to physical defect or mental retardation resulted in storage of the toxic material into the brain. Therefore, it is necessary to develop an analytical method for a rapid screening and/or correct confirmation diagnosis. Methods: The standard solution of sulfur amino acids spiked plasma was subjected to protein precipitation with methanol, and then consecutively derivatized with trimethylsilyl (TMS) and trifluoroacyl (TFA) and determined by GC-MS. The formation of TMS derivative of the hydroxyl and TFA derivative of amino functional group was performed by BSTFA and MBTFA, respectively. Selective ion monitoring (SIM) mode was used for quantification with selected specific ions. Results: A calibration curve on standard spiked pooled plasma showed a linear relationship with correlation coefficient of 0.9936-0.9992 for all compounds over the range of 0.1-300 ng. The precision and accuracy were within S.D. of 1-15% and RSD of 1-15% for intra-day assay at 2 ng/mL, 15 ng/mL and 30 ng/mL. LOD and LOQ was 0.4 ng/mL and 4 ng/mL respectively. Conclusion: A rapid analytical method was developed to quantify sulfur amino acids and methyl malonic acid, after two-step derivatization procedure with good sensitivity and specificity on human plasma. Advantages of a new method are simplicity and rapidity. The method could be useful for routine analysis, diagnosis of homocysteinemia.

Research on Function and Policy for e-Government System using Semantic Technology (전자정부내 의미기반 기술 도입에 따른 기능 및 정책 연구)

  • Jang, Young-Cheol
    • Journal of Korea Society of Industrial Information Systems
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    • v.13 no.5
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    • pp.22-28
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    • 2008
  • This paper aims to offer a solution based on semantic document classification to improve e-Government utilization and efficiency for people using their own information retrieval system and linguistic expression. Generally, semantic document classification method is an approach that classifies documents based on the diverse relationships between keywords in a document without fully describing hierarchial concepts between keywords. Our approach considers the deep meanings within the context of the document and radically enhances the information retrieval performance. Concept Weight Document Classification(CoWDC) method, which goes beyond using existing keyword and simple thesaurus/ontology methods by fully considering the concept hierarchy of various concepts is proposed, experimented, and evaluated. With the recognition that in order to verify the superiority of the semantic retrieval technology through test results of the CoWDC and efficiently integrate it into the e-Government, creation of a thesaurus, management of the operating system, expansion of the knowledge base and improvements in search service and accuracy at the national level were needed.

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GPS Network Adjustment for Determining KGD2002 Coordinates of the $2^{nd}$ Order Geodetic Control Points (GPS망조정에 의한 2등측지기준점의 세계측지계 성과산정)

  • Lee, Young-Jin;Lee, Hyung-Kyu;Jeong, Gwang-Ho;Lee, Jun-Hyuk
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.25 no.5
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    • pp.451-463
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    • 2007
  • This paper describes issues of GPS network adjustment to determine coordinate sets of the $2^{nd}$ order national geodetic control points based on the Korean Geodetic Datum (KGD2002) which has been newly adopted in 2003, After outlining theoretical background of the GPS network processing, the adjustment procedure applied for this project is detailed. Throughout performing a series of minimally constrained adjustments, some outliers have been removed and magnitude of absolute and relative error for a stochastic modeling has been determined as 4mm+0.4ppm and 8mm+0.8ppm in the horizontal and vertical component, respectively. The over constrained adjustment by fixing the $1^{st}$ order control points was performed to derive final solution, indicating that the accuracy of the estimated coordinates was 2cm and 4cm in the horizontal and vertical component.

A Study on filament Winding Process of A CNG Composite Pressure Vessel (필라멘트 와인딩 압력용기의 최적설계와 CNG자동차 연료 충진용기 개발)

  • Kim, Eui-Soo;Kim, Ji-Hoon;Park, Yoon-So;Kim, Chul;Choi, Jae-Chan
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.933-937
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    • 2002
  • The fiber reinforced composite material is widely used in the multi-industrial field where the weight reduction of the infrastructure is demanded because of their high specific modulus and specific strength. Pressure vessels using this composite material in comparison with conventional metal vessels can be applied in the field where lightweight and the high pressure are demanded from the defense and aerospace industry to rocket motor case due to the merits which are energy cutdown the weight reduction and decrease of explosive damage preceding to the sudden explosion which is generated by the pressure leakage condition). In this paper, for nonlinear finite element analysis of E-glass/epoxy filament winding composite pressure vessel receiving an internal pressure, the standard interpretation model is developed by using the ANSYS, general commercial software, which is verified as the accuracy and useful characteristic of the solution based on Auto LISP and ANSYS APDL. Both the preprocessor for doing exclusive analysis of filament winding composite pressure vessel and postprocessor that simplifies result of analysis have been developed to help the design engineers.

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