• Title/Summary/Keyword: solid residue

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Volatile Flavor Compounds Derived from Anchovy Engraulis japonicus Sauce Residues through Maillard Reactions (멸치(Engraulis japonicus) 액젓 부산물로부터 마이야르 반응을 통해 유도 된 휘발성 향기성분)

  • Jin Hyeon Kim;Yong-Jun Cha;Daeung Yu
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.56 no.2
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    • pp.174-181
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    • 2023
  • Volatile flavor compounds of optimal Maillard reactions (MR) derived with the addition of precursors (AP), control (without AP) and raw as anchovy Engraulis japonicus sauce residue were identified and comparatively analyzed using solid phase microextraction/gas chromatography/mass spectrometry (SPME/GC/MS). MR was produced by adding 1% (w/w) glucose and mixed amino acids (threonine 0.543%, glutamic acid 0.194%, glycine 0.382%, w/w) to raw (100 g of anchovy sauce residue and 100 mL of distilled water), and heating at 110 ℃ for 2 h. Among 65 flavor components detected, 7 compounds were produced through Maillard reaction to change in content. A total of 7 volatile flavor compounds, including 2-methylbutanal, 3-methylbutanal, dimethyl disulfide, methylpyrazine, dimethyl trisulfide, methional, and 2-furanmethanol, tended to increase in the order of raw, control, and MR, but methylpyrazine was not detected in control. Amounts of 2-methylbutanal, 3-methylbutanal, dimethyl disulfide, methylpyrazine, dimethyl trisulfide, methional, and 2-furanmethanol having positive odors (dark chocolate-, garlic-, hazelnut-, cooked potato-like) were 11.04, 50.15, 3.25, 8.38, 4.60, 9.59, and 3.08 times higher, respectively, in MR than those in raw.

A Study on Wettability and Defects Behavior of Flow-soldered Joint using Low Residue Flux (저잔사 플럭스를 사용한 플로우 솔더링부의 젖음성 및 결함거동에 관한 연구)

  • 최명기;이창열;정재필;서창제;신영의
    • Journal of Welding and Joining
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    • v.16 no.6
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    • pp.77-85
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    • 1998
  • Effects of non-cleaning and cleaning fluxes on the wetting properties and defects at flow soldered joints were investigated. Non-cleaning flux (R-type of 3.3% solid content) and cleaning flux (RMA-type of 15% solid content) were used. Wetting test was accomplished by wetting balance method with changing surface state of wetting specimen, CU. Sn-37%Pb solder was used for wetting test and flow soldering. As experimental results, the wetting time for vertical force from the surface tension being zero was mainly affected by surface state of the wetting specimen. Non-cleaning flux had a good wettability compared with cleaning flux. In case of non-cleaning flux, conveyor speed had a great affection to defects of bridge, icicle, and poor solder.

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Application of a solid-phase fluorescence immunoassay to determine ampicillin residues in muscle tissue of olive flounder (Paralichthys olivaceus)

  • Jung, Won Chul;Ha, Ji Young;Chung, Hee Sik;Heo, Sung Hyeok;Kim, Suk;Lee, Hu Jang
    • Korean Journal of Veterinary Research
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    • v.46 no.3
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    • pp.291-294
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    • 2006
  • $Parallux^{TM}$, a solid-phase fluorescence immunoassay(SPFIA) developed for antibiotics residue detection in milk, was applied for analysis of fish muscle. The recommended therapeutic dose of ampicillin(100 mg/kg body weight, withdrawal period 7 days) was orally administered to a group of 25 olive flounders(Paralichthys olivaceus) for consecutive five days. Muscle was sampled after drug treatment 1st, 2nd, 3rd, 4th and 5th day. The concentration of ampicillin in muscle, determined by SPFIA, was compared with that of internal standard(10 ppb as ampicillin). The absorbance ratio of sample to internal standard(Bs/Bo) was employed as an index to determine the muscle residue in olive flounder. To investigate the recovery rate, the standard solutions were added to muscle samples to give final concentrations in muscle of 10 and 50 ng/ml. The recovery rates of all spiked samples were > 89% of the spiked value. Ampicillin was detected in muscle of fishes treated until the 3rd day of withdrawal period. The present study showed that the SPFIA can be easily adopted in predicting tissue residues for ampicillin in farmed fishes.

Investigation of thorium separation from rare-earth extraction residue via electrosorption with carbon based electrode toward reducing waste volume

  • Aziman, Eli Syafiqah;Ismail, Aznan Fazli;Muttalib, Nabilla Abdul;Hanifah, Muhammad Syafiq
    • Nuclear Engineering and Technology
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    • v.53 no.9
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    • pp.2926-2936
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    • 2021
  • Rare-earth (RE) industries generate a massive amount of radioactive residue containing high thorium concentrations. Due to the fact that thorium is considered a non-economic element, large volume of these RE processed residues are commonly disposed of without treatment. It is essential to study an appropriate treatment that could reduce the volume of waste for final disposition. To this end, this research investigates the applicability of carbon-based adsorbent in separating thorium from aqueous phase sulphate is obtained from the cracking and leaching process of solid rare-earth by-product residue. Adsorption of thorium from the aqueous phase sulphate by carbon-based electrodes was investigated through electrosorption experiments conducted at a duration of 180 minutes with a positive potential variable range of +0.2V to +0.6V (vs. Ag/AgCl). Through this research, the specific capacity obtained was equivalent to 1.0 to 5.14 mg-Th/g-Carbon. Furthermore, electrosorption of thorium ions from aqueous phase sulphate is found to be most favorable at a higher positive potential of +0.6V (vs. Ag/AgCl). This study's findings elucidate the removal of thorium from the rare-earth residue by carbon-based electrodes and simultaneously its potential to reduce disposal waste of untreated residue.

Residue of Organophosphorus Pesticides in the Coastal Environment on the Cheju Island (제주도 연안 해양환경 중 유기린계 농약의 잔류)

  • Kim, Jeong-Ho;O, Yun-Geun;Park, Byeong-Yun
    • Journal of Environmental Science International
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    • v.8 no.4
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    • pp.503-507
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    • 1999
  • To study the residue of organophosphorus pesticides in the ocean environment on the Cheju island, EPN[O-ethyl-O-4-nitrophenyl phenylphosphonothioate] and monocrotophos [Dimethyl-1-methyl-2-methyl carba-moylvinylphosphate] of organophosphorus pesticides are surveyed on coastal environment of Cheju city and Wimi in May and October 1996. The qualified limit detection of EPN and monocrotophos are 0.005ng/mL and 0.006ng/mL in the water by GC-FPD, respectively. The qualified limit detection of EPN and monocrotophos are 0.010ng/g and 0.012ng/g in the solid such as sediment and sea organism by GC-FPD, respectively. EPN and monocrotophos are not detected in seawater and sedimnet. Moreover EPN and monocrotophos are neither detected in seaweed cava (Ecklonia cava), Agar (Gelidium amansii), turban sell(Batillus cornutus) and sea urchin(Anthocidaris Crassispina). EPN, monocrotophos used in the farm on the Cheju island are not residued in the coastal environment in the Cheju island.

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붉나무열매의 성분연구 제1보 -유기산에 대하여

  • 한구동;김영수
    • YAKHAK HOEJI
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    • v.1 no.1
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    • pp.4-6
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    • 1948
  • The fruits of Rhus javanica L. distributed widely in Korea were extracted with cold water, the filtered clear liquid was evaporated and from the residue large colorless columns, M.P.about 180.deg., were obtained by recrystallisation from hot water. On being incinerated it left a considerable amount of solid residue consisting of calcium. Its aqueous solution which had a strong acid reaction was acidified with sulfuric acid, the precipitate, CaSO$_{4}$, was filtered off, the filtrate was evaporated and from the residue colorless needles, M.P.98-100.deg., were obtained by treating with alcohol. It was identified to be malic acid by determining the mixed melting points of itself and its p-bromphenacylester with authentic specimens. Thus the original substance was proved to be a kind of Ca-salt of malic acid.

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Effect of Extraction on Chemical Composition of Rcd Ginseng Extract (추출 회수에 따른 홍삼 extract의 성분 조성에 관한 연구)

  • 최강주;김만욱;성현순;홍순근
    • Journal of Ginseng Research
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    • v.4 no.1
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    • pp.88-95
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    • 1980
  • Red ginseng was extracted with water and analyzed for yield, saponin, pectin and other chemical composition. It was found that: (1) The total solid content in extract after 6 times of extraction was 46.8%,: including 13.6% of centrifugal residue; (2) 83.7% of total extractable solids and 86% total saponin was extracted after the initial three runs of extraction. (3) No significant changes were observed in HPLC pattern of extracted saponins over a range of extractions; (4) The ratio of centrifugal residue to total solids increased as the number of extractions increased; (5) The ratios of fat, protein, reducing sugar and pectin contents decreased with repeating extraction while those of crude fiber, total sugar and 35% alcohol insoluble residue increased when they were compared with total solids.

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Treatment of residues of excavated carcasses burials (가축매몰지 소멸시 잔존물 처리방안)

  • Kim, Geonha
    • Journal of Korean Society of Water and Wastewater
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    • v.32 no.3
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    • pp.269-277
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    • 2018
  • Burials for the rapid disposal of carcasses have diverse and profound effects on the rural living condition, natural environment, and local economy throughout construction, management and final destruction of burials. In this study, possible residue excavated from standard burials, storage using FRP (Fiberglass Reinforced Plastic) tanks, and microbial-treated burials are characterized as carcasses, contaminated soil by leachate, and wasted plastic film. Treatment technologies for volume reduction of the residue including composting, rendering, and thermal hydrolysis were investigated. If the solid and liquid residues generated during volume reduction treatment are directly transferred to the environmental facilities, it may cause disorder due to high concentrations of organics, antibiotics, and lipid. Benefits and drawbacks of composting as a volume reduction techniques are extensively investigated. We also discussed that proper treatment of excavated soils and the reusing the treated soil as agricultural purpose. For the protection of public health and worker's hygiene, treatment criteria including produced residue qualities, and quality standards for the treated soil as agricultural use are required. In addition, Scientific manual for the proper treatment of residues is required. It is necessary to consider the establishment of a pretreatment facility to the occurrence of large-scale residue treatment.

Impact of Waste Coffee Residue Disposal on the Environment and Anti-microbic Activity of Oyster Shell Waste

  • Ramakrishna, Chilakala;Thenepalli, Thriveni;Nam, Seong Young;Kim, Chunsik;Ahn, Ji Whan
    • Journal of Energy Engineering
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    • v.27 no.1
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    • pp.76-80
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    • 2018
  • The objective of this research paper is to discuss the waste coffee residue disposal and its environmental effects on the environment. As we know, coffee is one of the most demand and swallowed beverages in the world, which leads to large quantities of solid waste. Which can be toxic and a lot of environmental problems occur. In developing countries, there is a lack of proper coffee waste residue management. The coffee beans and residues contain several organic compounds. The wastewater from coffee industry emitted several pollutants (highly concentrated) and it contaminates the soil, ground waters, aquatic life, and also human health. Hence it is essential to treat the coffee waste residues. Mean while, oyster shell waste and its disposal also a big environmental challenge in the coastal regions of southeast Korea. In this paper, we focused the treatment of coffee waste residue with oyster shell waste powder. Primarily, oyster shells are calcinated at higher temperatures and investigated the calcined CaO powder as an anti microbic agent to the bacteria presented in coffee waste residues. We successfully applied calcium oxide from oyster shell waste, as an antimicrobic agent.

Lovastatin Production in Solid-state Fermention by Aspergillus terreus and Its Application for Animal Feed Additive

  • Yoon, Ji-Yong;Han, Kyu-Boem
    • 한국생물공학회:학술대회논문집
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    • 2003.10a
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    • pp.263-267
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    • 2003
  • Solid-state fermentation of lovastatin by Aspergillus terreus was investigated using commercially available 1.2 L polypropylene bottle designed for mushroom cultivation. Moist solid raw materials such as com, rice, and soy bean were tested and com was found to be most suitable for an economical production of lovastatin. 50% or higher water addition prior to the sterilization of com was effective for the maximal lovastatin production. About 0.5% (w/w) lovastatin content in dried cells and corn mass was obtained after 20 days of solid-state fermentation at 30$^{\circ}C$. For safety concerns, aflatoxin Bl and citrinin levels after fermentation were assayed but they were not detected. Lovastatin containing cells and corn residue after fermentation were autoclaved, dried, crushed, and fed to chicken for a period of 3 weeks. Approximately 20% reduction of blood cholesterol level of chicken was observed.

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