• 열처리공학회지
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• 제29권3호
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• pp.113-123
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• 2016

In the present work, we investigated the effects of the carbon potential on the formation of carbide at the carburized surface and anti-pitting fatigue strength in the supercarburized steels. Two low carbon steels with different Cr concentrations were adopted and the repeated supercarburizing treatment carried out with the different carbon potential conditions. The microstructure and carbides at the supercarburized surface were observed by using optical microscope and scanning electron microscope. The microhardness test was performed and the hardness distribution and the effective case depth at the supercarburized surface were discussed. The roller pitting fatigue test was carried out and the fatigue strength was evaluated with different the carbon potential conditions. The microstructure of the fatigue specimen surface was observed by means of scanning electron microscope and scanning transmission electron microscope. Depending on the chemical composition of the steels and the carbon potential condition, the resistance of temper softening and pitting failure was influenced due to the carbide distribution and the formation of coarse network carbide. Thus, it was confirmed that the control of the carbide formation is a key factor to improve the anti-pitting fatigue strength in the supercarburized steels.

• 한국산학기술학회논문지
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• 제16권7호
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• pp.4977-4983
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• 2015

개착식 공법은 도로의 굴착에 따른 시간과 비용의 증가, 교통통제로 인한 민원발생 및 교통지정체 등 많은 문제점을 발생시키고 있다. 이러한 문제점을 해결하기 위하여 비굴착공법에 사용 가능한 하수관거 보수자재에 대한 실험을 시행하였다. 사용한 재료는 PVC프로파일이며, 국가표준시험 방법을 적용하여 기본 물성 평가를 시행하였다. 본 기술은 SPR(Sekisui Pipe Rehabilitation) 기술에 적용되는 프로파일보다 구조적 안정성이 높고, pipe integrity를 높일 수 있는 SWP(Spirally Wound Pipe)용 프로파일 구조를 적용하였다. 복합안정제의 함량을 5 phr을 이용하여 배합을 하였다. 시험 결과 복합안정제와 충격보강제를 투입한 경우에도 인장강도, 충격강도 및 연화온도가 표준의 물성을 만족함을 알 수 있었고, 가공시 부하가 없이 가공할 수 있었다. 접착 수지로 단부마감을 한 프로파일은 같은 압력에서 누수가 발생하지 않았다.

• 한국세라믹학회지
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• 제52권4호
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• pp.229-233
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• 2015

Currently, the majority of commercial white LEDs are phosphor converted LEDs made of a blue-emitting chip and YAG yellow phosphor dispersed in organic silicone. However, silicone in high-power devices results in long-term performance problems such as reacting with water, color transition, and shrinkage by heat. Additionally, yellow phosphor is not applicable to warm white LEDs that require a low CCT and high CRI. To solve these problems, mixing of green phosphor, red phosphor and glass, which are stable in high temperatures, is common a production method for high-power warm white LEDs. In this study, we fabricated conversion lenses with LUAG green phosphor, SCASN red phosphor and low-softening point glass for high-power warm white LEDs. Conversion lenses can be well controlled through the phosphor content and heat treatment temperature. Therefore, when the green phosphor content was increased, the CRI and luminance efficiency gradually intensified. Moreover, using high heat treatment temperatures, the fabricated conversion lenses had a high CRI and low luminance efficiency. Thus, the fabricated conversion lenses with green and red phosphor below 90 wt% and 10 wt% with a sintering temperature of $500^{\circ}C$ had the best optical properties. The measured values for the CCT, CRI and luminance efficiency were 3200 K, 80, and 85 lm/w.

• 한국응용과학기술학회지
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• 제8권1호
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• pp.9-20
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• 1991

In the preparation of acrylic water repellent(EDLWC). quaternized 2-diethylarrunoethylmethacrylate-stearylmethacrylate copolymer (DSACC) and quaternized 1-Iaurovlbis(aminoethyl)-2-dodecylimidazoline(LDDIC) were selected as a basic resin and the improving agent such as softening effect and hydrostatic pressure of the water repellent. EDLWC was prepared by blending waxes and emulsifier for waxes with various ratio to DSACC and LDDIC. As the results of the measurement of water repellency, washable, tear strength and crease recovery to polyester-cotton(P/C) blended fabrics treated with EDLWC only or addition of textile finishing resin, the physical properties were increased. Sodium acetate was the most effective catalyst in the water repellency among the various kinds of catalyst. and the reasonable concentration of the catalyst was 1. 4 wt%. EDLWC was confirmed as durable water repellent with the results of making little difference of water repellency as ${\pm}5$ point after and before washing. The reaction mechanism between P/C blended fabrics and EDLWC in the presence of catalyst was proposed. And also, the longitudinal view of the P/C blended fabrics treated with water repellent was observed with scanning electron microscope.

• 대한치과보철학회지
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• 제36권1호
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• pp.50-63
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• 1998

This study investigated the effects of resin surface primers for rebase resins on the surface texture of denture base resins by the use of scanning electron microscopy. This study also evaluated the bond strength of rebase resins to denture base resin. The denture base resin in this study was Vertex RS (Dentimex Co., Ltd., Holland). The rebase resins used were Tokuso Rebase (Tokuyama Co., Ltd., Japan), Metabase (Sun Medical Co., Ltd., Japan), New True Liner(Harry J, Bosworth Co., Ill.), and Reverse (Nissin Co., Ltd., Japan). The test samples were divided into four parts: Group 1 : Treated with primer with brush. Group 2 : Immersed in the primer for 5 seconds. Group 3 : Immersed in the primer for 10 seconds. Group 4 : Immersed in the primer for 30 seconds. Control group : not treated with primer The results were as follows; 1. The bond strength of rebase resins to denture base resin is increased by application of primers. 2. Regardless of the rebase resin type, there was no significant difference among the bond strength in groups G1, G2, G3, G4. There was a significant difference with the control. (P<0.05) 3. Regardless of each group, the bond strength according to the rebase resin type was decreased in the following order: Tokuso Rebase, New Tru Liner, Reverse and then Metabase. 4. Under the scanning electron microscope, brush application produced a softening of the denture base surface. After immersion, all primers produced a spongelike structure on the denture base resin surface. The results of this study suggest that primers produce a significant effect by means of brush application, therefore it is recommended as the most convenient and logical procedure for application of the primers.

• 한국표면공학회지
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• 제37권2호
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• pp.80-85
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• 2004

Chromium-carbon (Cr-C) and chromium-carbon-phosphorus (Cr-C-P) alloy deposits using trivalent chromium sulfate baths containing potassium formate were prepared to study their current efficiency, hardness change and phase transformations behavior with heat treatment, respectively. The current efficiencies of Cr-C and Cr-C-P alloy deposits increase with increasing current density in the range of 15-35 A/dm$^2$. Carbon content of Cr-C and phosphorous of Cr-C-P layers decreases with increasing current density, whereas, the carbon content of Cr-C-P layer is almost constant with the current density. Cr-C deposit shows crystallization at $400^{\circ}C$ and has (Cr+Cr$_{ 23}$$C_{6}$) phases at $800^{\circ}C$. Cr-C-P deposit shows crystallization at $600^{\circ}C$ and has (Cr+Cr$_{23}$ $C_{6}$$+Cr_3$P) phases at $800^{\circ}C$. The hardness of Cr-C and Cr-C-P deposits after heating treatment for one hour increase up to Hv 1640 and Hv 1540 and decrease about Hv 820 and Hv 1270 with increasing annealing temperature in the range of $400～^{\circ}C$, respectively. The hardness change with annealing is due to the order of occurring of chromium crystallization, precipitation hardening effect, softening and grain growth with temperature. Less decrease of hardness of Cr-C-P deposit after annealing above $700^{\circ}C$ is related to continuous precipitation of $Cr_{23}$ $C_{6}$ and $Cr_3$P phases which retard grain growth at the temperature.

• 대한토목학회논문집
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• 제4권4호
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• pp.1-11
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• 1984

콘크리트의 복잡한 파괴거동(破壞擧動)을 모델할 수 있는 비선형파괴이론(非線型破壞理論)이 본(本) 논문(論文)에서 유도되었다. 본(本) 이론(理論)은 콘크리트균열끝의 파괴진행대(破壞進行帶)에서의 미세균열현상(微細龜裂現象)과 변형연화현상(變形軟化現象)으로 인한 비선형거동(非線型擧動)에 그 근거(根據)를 두고 있다. 이로부터 실제적이고도 단순화(單純化)된 파괴해석(破壞解析)모델이 유도되었으며, 이 단순화된 모델은 파괴진행대(破壞進行帶)의 변화에도 콘크리트의 파괴(破壞)에너지를 일정하게 유지할 수 있는 특정을 가지고 있다. 파괴해석(破壞解析)에 비선형응력(非線型應力)-변형거동(變形擧動)을 이용함으로써 균열면에 평행하게 작용하는 압축응력에 대한 영향이 쉽게 고려될 수 있다. 본 모델을 콘크리트의 많은 파괴실험자료와 비교한 결과 만족스러운 결과를 얻었으며, 종래의 선형파괴이론에 의한 결과는 실제 콘크리트 실험결과와 많은 차이를 보이고 있음을 알 수 있다. 콘크리트 구조의 균열 및 파괴해석에 필요한 콘크리트 파괴에너지의 근사공식이 본 이론으로부터 유도되었다. 끝으로, 철근콘크리트에 대한 파괴이론의 응용 및 확장연구 문제가 토의되었다.

• Journal of Welding and Joining
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• 제21권1호
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• pp.107-113
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• 2003

Joining of $Si_3N_4$ to $Si_3N_4$ with crystallized glass solder was studied. $SiO_2-Al_2O_3-MgO$ glass with $P_2O_5$ as a crystallizing reagent was used as a solder. To improve the hish temperature toughness of joined specimen, two stage heat treatment was applied to Joined sample for the crystallization of joined layer, Two factors, i.e. thickness of soldered layer and crystallization were taken and thier effects on joining strength were investigated by a SEM-EDX observation of joined interface and bending strength both at room and elevated temperatures. Obtained results are summarized as follows: (1) Nitrogen diffused from $Si_3N_4$ to solder during the Joining process. Average amount of nitrogen in soldered layer depended on the thickness of the soldered layer and increased with decrease of the thickness. (2) Joining strength of the specimen having a thinner soldered layer was stronger than that of thicker layer. This can be mainly attributed to the difference of the nitrogen content in the soldered layer. (3) Higher content of nitrogen in solder brought forth higher viscosity of the solder. Hence the crystallization of the solder become more difficult in thinner layer of the solder than thicker one. (4) Thus, the effect of crystallization was evaluated mostly by the thicker layer specimen. Crystallization of soldered layer improved markedly the fracure strength of joining at higher temperatures than the softening temperature of glass solder.

• 멤브레인
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• 제17권3호
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• pp.191-196
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• 2007

본 연구에서는 경도 이온의 화학적 침전을 위하여 지하수에 과량의 Lime-Soda ash를 주입하여 플럭(floc)을 형성한 다음 침전과정을 십자흐름(Crossflow) 방식의 관형 세라믹 분리막을 이용한 한외여과(UF) 공정으로 대체하였다. 그 결과 두유 포장팩 세척수로 사용하고 있는 지하수의 총경도를 10 mg/L as $CaCO_3$ 이하로 감소시킬 수 있었다. 한편, TMP(Trans-membrane pressure) 및 유량 변화 실험에서 투과선속(Permeate flux, J) 및 무차원한 투과선속($J/J_0$) 변화를 조사하여, TMP 및 유량이 무기물로 형성된 응집 플럭에 의한 막오염에 미치는 영향을 알아보았다. 그 결과, 본 실험 범위에서 TMP 및 유량 변화가 막오염과 총경도 제거율에 미치는 영향은 거의 없었다.

• Applied Biological Chemistry
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• 제42권3호
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• pp.223-228
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• 1999

제주산 궁천조생 온주밀감의 저장효과를 검토하기 위하여 저장 중 각각 $3^{circ}C$, 90%와 85% 상대습도에서 저온저장하였으며, 습도 조절이 안된 상온저장과 비교하였다. 중량감소는 저장 98일까지 각각 90% 습도에서는 3.40%, 85% 습도에서는 6.92%, 상온저장에서는 11.87%로서 습도가 높을수록 중량감소는 적었다. 그러나 90% 습도에서 저장한 감귤은 저장 98일 이후 부패율이 3.87%에서 급격히 증가하여 126일에 48.75%에 이르렀다. 과육율과 가용성고형물은 저장기간 중 큰 변화를 보이지 않았다. 경도는 저장 중 계속하여 감소하였고, 특히 상온저장에서 감소가 심하였다. 산 함량과 비타민 C 변화는 호흡작용에 의해 저장기간이 경과함에 따라 계속하여 감소하였다. 상온저장에서는 저온저장에 비해 착색이 계속 진행됨을 알 수 있었다. 관능평가와 내용성분을 기준한다면 품질 유지를 위해서는 $3^{circ}C$, 85% 상대습도에서 수확후 100일 정도가 조생온주 밀감의 최적 저장기간으로 판단되었다.