• 한국식품영양과학회지
• /
• 제21권6호
• /
• pp.701-705
• /
• 1992

수리취의 삶는 방법을 달리하여 조리한 후 그들의 이화학적 특성을 생수리취와 비교 분석하였다. 조리수는 물, 1%소금, 1%중조를 첨가하여 사용하였으며 삶는 시간은 물과 소금 첨가 조리수에서 30분, 중조첨가 조리수에서 10분으로 하였다. 삶는 수리취액의 pH는 중조를 조리수에 이용한 것이 8.21로 가장 높았고, 수리취잎의 색도 중 녹색도(a)의 경우 중조처리구가 생수리취(-10.50)와 가장 유사한 값을 나타내었으며, 클로로필 및 비타민 C의 함량 또한 중조의 경우가 다른 처리구에 비해 조리방법에 따른 변화의 정도가 적었다. 생수리취의 무기질은 Mg, K, Ca의 순으로 그 함량이 높았으며, 삶은 후에는 조리수에 따라 그들의 함량에 다소 차이가 있었고, 소금, 중조 처리구의 경우 Na의 함량이 증가하였다. 생수리취의 가용성 단백질은 70%가 albumin으로 구성되어 있었으나, 조리에 의해 albumin은 감소한 반면 glutelin, globulin 및 prolamin의 함량은 증가하였다. 수리취에서 분리 정제한 알콜 불용성 물질의 식이섬유 함량은 조리방법에 따라 NDF, ADF, cellulose, lignin값이 감소한 반면 hemicellulose값은 증가하였다.

• Journal of Microbiology and Biotechnology
• /
• 제22권12호
• /
• pp.1681-1691
• /
• 2012

This work was conducted to evaluate the effect of dilute sodium hydroxide (NaOH) on barley straw at boiling temperature and fractionation of its biomass components into lignin, hemicellulose, and reducing sugars. To this end, various concentrations of NaOH (0.5% to 2%) were applied for pretreatment of barley straw at $105^{\circ}C$ for 10 min. Scanning electron microscopy (SEM), atomic force microscopy (AFM), and Fourier transform infrared (FTIR) spectroscopy studies revealed that 2% NaOH-pretreated barley straw exposed cellulose fibers on which surface granules were abolished due to comprehensive removal of lignin and hemicellulose. The X-ray diffractometer (XRD) result showed that the crystalline index was increased with increased concentration of NaOH and found a maximum 71.5% for 2% NaOH-pretreated sample. The maximum removal of lignin and hemicellulose was 84.8% and 79.5% from 2% NaOH-pretreated liquor, respectively. Reducing sugar yield was 86.5% from 2% NaOH-pretreated sample using an enzyme dose containing 20 FPU of cellulase, 40 IU of ${\beta}$-glucosidase, and 4 FXU of xylanase/g substrate. The results of this study suggest that it is possible to produce the bioethanol precursor from barley straw using 2% NaOH at boiling temperature.

• 한국원자력학회:학술대회논문집
• /
• 한국원자력학회 1997년도 춘계학술발표회논문집(1)
• /
• pp.489-494
• /
• 1997

A comparative transient analyses were performed for oxide and nitride cores or a large (3000 MWt), pool-type, liquid-metal-cooled reactor (LMR). The study was focused on three representative accident initiators with failure to scram : the unprotected loss-of-flow (ULOF), the unprotected transient overpower (UTOP), and the unprotected fast transient overpower (UFTOP). The margins to fuel melting and sodium boiling have been evaluated for these representative transients. The results show that there is an increase in safety margin with nitride core which maintains the physical dimensions of the oxide core.

• 한국응용과학기술학회지
• /
• 제6권2호
• /
• pp.45-51
• /
• 1989

Allyl aliphatic carboxylates were synthesized by azotropic reaction with benzene between allyl alcohol and capric acid, lauric acid, myristic acid, palmitic acid or stearic acid respectively. allyl aliphatic carboxylates oligomers were prepared from polymerization giving allyl aliphatic carvboxylates in the presence of potassium persulfate in methanol, and the ${\alpha}-sulfonation$ of these five allyl aliphatic carboxylates oligomers were carried by direct addition of dry sulfur trioxide. Especially, molecular weights of fatty acid alylester oligomers and their sodium salts of ${\alpha}-sulfo$ fatty acid allylester oligomers were measured by boiling point method.

• 한국세라믹학회지
• /
• 제25권1호
• /
• pp.66-72
• /
• 1988

The effect of salts on the formation of ${\alpha}$-hemihydrated gypsum at boiling temperature under atmospheric pressure was studied by the solubility measurement method, and the formation of ${\alpha}$-hemihydrated gypsum from by-product gypsum of phosphoric acid process in the salts solution were investigated. The order of catalytic effect of salt on the formation of ${\alpha}$-hemihydrated gypsum are as follows: NH4Cl>NaCl>NaNO3. In the salts solution of sodium nitrate, sodium chloride, and ammonium chloride, prismatic ${\alpha}$-hemihydrated gypsum was obtained and the crystal form was converted to needle form in complex solution with sulfuric acid. The P2O5 content in gypsum was largely decreased in this atmosphoric solution process.

• 한국원자력학회:학술대회논문집
• /
• 한국원자력학회 1997년도 추계학술발표회논문집(1)
• /
• pp.645-650
• /
• 1997

An oxide fuel small size core (1200 MWt) was analyzed in comparison with a large size core (3600 MWt) in order to evaluate the size effects on transient safety performances of liquid-metal reactors (LMRs). in the first part of the study, main static safety parameters (i.e., Doppler coefficient, sodium void effect, etc.) of the two cores were characterized, and the second part of the study was focused on the dynamic behavior of the cores in two representative transient events: the unprotected loss-of-flow(ULOF) and the unprotected transient overpower (UTOP). Margins to fuel molting and sodium boiling have been evaluated for these representative transients. Results show that the small core has a generally better or equivalent level of safety performances during these events.

• 한국응용과학기술학회지
• /
• 제6권1호
• /
• pp.21-26
• /
• 1989

Four fatty acid vinyl esters were synthesized by transesterification between vinyl acetate and lauric acid, myristic acid, palmitic acid, stearic acid, respectively. Fatty acid vinyl ester oligomers were prepared from polymerization of four fatty acid vinyl esters in the presence of potassium persulfate in methanol. The ${\alpha}-sulfonation$ of these four fatty acid vinyl ester oligomer were carried by direct addition of sulfur trioxide. Especially, molecular weights of sodium ${\alpha}-sulfo$ fatty acid vinyl ester oligomers were measured by boiling point method.

• Nuclear Engineering and Technology
• /
• 제53권1호
• /
• pp.111-120
• /
• 2021

During the core disruptive accident (CDA) of sodium-cooled fast reactor (SFR), the molten fuel and steel are solidified into debris particles, which form debris bed in the lower plenum. When the boiling occurs inside debris bed, the flow of coolant and vapor makes the debris particles relocated and the bed flattened, which called debris bed relocation. Because the thickness of debris bed has great influence on the cooling ability of fuel debris in low plenum, it's very necessary to evaluate the transient changes of the shape and thickness in relocation behavior for CDA simulation analysis. To simulate relocation behavior, a large number of debris bed relocation experiments were carried out by improved bottom gas-injection experimental method in this paper. The effects of different experimental factors on the relocation process were studied from the experiments. The experimental data were also used to further evaluate a semi-empirical onset model for predicting relocation.

• 한국식품과학회지
• /
• 제8권4호
• /
• pp.207-211
• /
• 1976

오징어의 동부근육(胴部筋肉)을 각종방법(各種方法)으로 처리(處理)하여 cross section하고 Van Gieson방법(方法)으로 염색(染色)하여 박막상(薄膜狀)의 표피층(表皮層)이 박리(剝離)되는 상태(狀態)를 현미경으로 관찰한 결과(結果)는 다음과 같다. 1. 일반적으로 사용되는 온탕법(溫湯法)에서 1, 2, 3층(層)은 제거(除去)되지만 4층(層)은 거의 제거(除去)되지 않았다. 2. 열탕처리(熱湯處理)에 의해서 근섬유(筋纖維) 조직(組織)에 근섬유(筋纖維)의 방향(方向)으로 많은 균열 현상을 보였다. 3. 초산소오다가 질산소다. 황산(黃酸)소오다 및 주석산(酒石酸)소오다 처리(處理)보다 박리상태(剝離狀態)가 현저히 우수하였으며 특(特)히 고농도(高濃度)에서 현저하고 약품처리(藥品處理) 방법중(方法中) 가장 우수한 효과(?果)를 보였다. 4. 단백(蛋白) 분해효소(分解酵素) 처리시(處理時) 표피(表皮)의 1, 2, 3, 4, 층(層)은 완전히 제거(除去)되며 특(特)히 표피(表皮)와 육(肉)과의 경계면 섬유(纖維)를 현저하게 팽윤(澎潤)시켰다. 5. 효소(酵素)와 초산소오다로 처리(處理)하는 2종류(種類)의 박피법(剝皮法)은 유효(有效)하다는 것을 확인(確認)하였다.

• Journal of the Korean Wood Science and Technology
• /
• 제48권6호
• /
• pp.878-887
• /
• 2020

A neutral extract (NE), that is soluble in cold water and has excellent antioxidant activity, from Pinus radiata pine bark was prepared by sodium bicarbonate treatment, and its chemical characteristics were investigated. NE was prepared by treating P. radiata bark with 0.8% NaHCO₃ aqueous solution with a 5 : 1 liquor-to-bark ratio at boiling temperature for 1 h, resulting in 44% yield and final pH of 6.66. The yield of NE was 11% higher than that of the hot water extract (HWE) due to the increase in the solubility of polyphenols, the main component in the bark, by NaHCO₃ treatment. NE was characterized through FT-IR, NMR, and MALDI TOF MS analyses. The results indicated that NE is mostly composed of proanthocyanidins (PAs) consisting of procyanidin (PC) units. The acetylated neutral extract (Ac-NE) had weight average molecular weight (${\bar{M}}w$) of 5,300 Da. The Ac-NE had wide molecular weight distribution and its polydispersity (${\bar{M}}w/{\bar{M}}n$) was 6 times higher than that of pure PA. The antioxidant activity of NE was determined by 2-diphenyl-1-picrylhydrazyl (DPPH) free radical scavenging assay and showed that NE had comparable antioxidant activity with pure PA.