• 제목/요약/키워드: sodium acetate

검색결과 372건 처리시간 0.024초

Sodium Acetate Trihydrate를 이용한 구형의 PCM 입자의 제조 (Preparation of spherical shape of PCM by using sodium acetate trihydrate)

  • 김종국;정경택;설용건;김동형;이태규
    • 태양에너지
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    • 제17권2호
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    • pp.67-74
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    • 1997
  • 잠열 저장물질로서 비조화 축열재인 sodium acetate trihydrate를 사용하여 구형의 PCM 입자를 제조하였다. 비조화 축열재의 단점인 상분리 현상 및 과냉각 현상을 방지하기 위하여 점증제로서 gelatin, 조핵제로서 sodium pyrophosphate decahydrate를 사용하였다. 혼합조성의 용융 PCM을 이용하여 연속적으로 지름이 3-3.5 mm 인 구형 PCM 입자가 제조되었다. 용융 PCM 방출속도가 1.3-1.8 ml/min 인 범위 내에서는 PCM 입자크기가 방출속도에 영향을 받지 않았다. 제조된 PCM 입자의 물성을 측정하기 위하여 DSC, SEM과 XRD를 이용하였다.

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첨가제로 아세트산 나트륨-3수화물을 함유한 물 액적의 증발 특성 (Evaporation Characteristics of a Water Droplet Containing Sodium Acetate Trihydrate as an Additive)

  • 박재만;신창섭
    • 한국안전학회지
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    • 제19권2호
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    • pp.61-68
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    • 2004
  • The evaporation phenomena of waterr droplet which has sodium acetate trihydrate($CH_3COONa{\cdot}3H_2O$) as a fire suppression additive were studied. Solutions of sodium salt up to 50% and heated stainless-steel surface were used in the experiment. The evaporation process was recorded using a charge-coupled-device camera at 120 frames per second. The average evaporation rate of the sodium acetate trihydrate soluation was lower than that of pure water at a given surface temperature and decreased with the concentration increase due to the precipitation of salt in the liquid film and change of surface tension. The variation of liquied film diameter was measured by time and it was increased by the hot surface temperature increase.

납의 흡입독성 연구를 위한 에어로졸 발생장치의 고안 및 실시간 모니터링을 이용한 성능평가 (Design of Aerosol Generator for Inhalation Toxicology Study of Lead and Evaluation with Real Time Monitoring)

  • 정재열;김정만;김태형;정명수;고광재;김상덕;강성호;송용선;이기남
    • 동의생리병리학회지
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    • 제16권2호
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    • pp.373-379
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    • 2002
  • This paper was the design of aerosol generator for inhalation toxicology study of lead and evaluation with real time monitoring, and applied several engineering methodology to classical aerosol generator to cope with it's disadvantages. According to the testing conditions, source temperature 50℃ and inlet-duct band heater temperature 150℃, aerosol generation results for sodium chloride and lead acetate were as followings: CPM(Count Per Minute) for Sodium chloride that used for the testing material in aerosol generation and inhalation system was decreased in the 2nd and the 3rd hour's serial trials, but CVs(coefficient of variation) were maintained within 10%. CPMs for 5 and 2.5 gram of lead acetate that used for aerosol generation and inhalation exposure of lead showed similar results because of the sedimentation of lead acetate on piezoelectric crystal with time. For that reason, heating and mixing of nebulizing solution will be needed to generate lead aerosol with stable profile and maximum generation efficiency. Fluctuations of 10 and 5 gram lead acetate were low but 2.5gram was high. However, CVs for 10, 5, and 2.5gram lead acetate were within 10%. Considering the theoretical efficiencies for sodium chloride and lead acetate, 5gram sodium chloride and 2.5gram lead acetate were appropriate choice. Aerosol generation characteristics for two materials with 1 hour interval were different with respect to the fluctuation of CPM and the decrease to 10gram in it's material. For that reason, sodium chloride can not be used to estimate the aerosol generation and it's related parts for lead acetate. According to the testing conditions, source temperature 20, 50, 70℃, and inlet-duct band heater temperature 20, 50, 100, 150, 200℃, aerosol generation results for sodium chloride and lead acetate were as followings: Excluding inlet-duct band temperature 200℃, maximum CPM for sodium chloride was manifested in source temperature 70℃ with each inlet-duct band temperature conditions. We suggest that this condition was the optimum in the design of aerosol generator, inhalation system, and the testing. Maximum CPMs for 10, 5, and 2.5gram sodium chloride were from source temperature 70℃ and inlet-duct band temperature 20℃. Excluding inlet-duct band temperature 50, 200℃, maximum CPMs for lead acetate were indicated in source temperature 50℃ with each inlet-duct band temperature conditions. We suggest that this condition was the optimum in the design of aerosol generator, inhalation system, and the testing for lead inhalation study. Source and inlet-duct band temperatures for 10, 5, 2.5gram lead acetate were 50 and 100℃, 50 and 100℃, 50 and 150℃, respectively. In conclusion, considering above 2 paragraphs of results for aerosol generation, 5gram efficiencies for sodium chloride, lead acetate were higher than 2.5gram's. If inlet-duct band temperature was same, aerosol generation was increased with increase of source temperature. To get maximum aerosol generation will be the conditions that set the appropriate inlet-duel band temperature for each materials and increase the source temperature.

Effect of Different Ratios of Concentrate and Roughage on Lipid Synthesis by Rumen Microorganisms In Vitro

  • Sasaki, H.;Horiguchi, K.;Takahashi, T.
    • Asian-Australasian Journal of Animal Sciences
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    • 제16권1호
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    • pp.36-38
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    • 2003
  • The effect of different feeding ratios of concentrate to roughage on ruminal lipid synthesis in vitro was examined. Three sheep fitted with a rumen fistula were fed three different ratios (8:2, 4:6 and 0:10) of concentrate and roughage, and their rumen liquor were used for incubation. $^{13}C$-labeled glucose or sodium acetate as substrate was added to cultures of rumen liquor, and they were incubated for 6 h. The total lipid in the culture of the rumen liquor was extracted, and the percentage of $^{13}C$ excess was analyzed. The percentage of $^{13}C$ excess recovered when incubated with glucose increased with increased ratio of concentrate in the diet. The values of cultures incubated with glucose were higher than those incubated with sodium acetate except the roughage-only feeding. In the roughage-only diet, the percentage of $^{13}C$ excess when incubated with sodium acetate was highest of all diets. The recovery percentage of $^{13}C$ from glucose increased with increased ratio of concentrate. The recovery percentage of $^{13}C$ from sodium acetate addition in only roughage feeding was highest among the three diets. The recovery percentage of $^{13}C$ from glucose was markedly higher than that of sodium acetate addition in all feedings. The results indicate that high concentrate feeding facilitates lipid synthesis by rumen microorganisms, and that glucose may be the precursor for lipid synthesis rather than acetic acid.

결정성 염을 포함한 유⋅무기계 자기치유 소재의 결정 생성 효과에 따른 치유 특성 연구 (A Study on the Self-heaing Properties of Inorganic-organic Additives with Recycling Sodium Acetate)

  • 박동철;권혁;황무연;김태형;이강범
    • 한국건설순환자원학회논문집
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    • 제10권4호
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    • pp.584-592
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    • 2022
  • 본 논문에서는 구체방수 혼화재로 사용되는 아세트산나트륨을 활용하여 자기치유 성능 향상 및 강도 성능 개선을 위한 연구를 진행하였다. 선행연구로 개발된 유ㆍ무기계 자기치유 핵심소재와 재생 아세트산나트륨을 혼합 제조하여 자기치유 모르타르, 콘크리트의 기초성능 및 투수 저감 성능을 평가하였다. 재생 아세트산나트륨을 첨가 실험결과 무수화물 단독으로 사용한 배합에 비해 무수화물과 삼수화물을 7:4 비율로 혼합한 소재의 압축강도 개선 효과가 3~7 %로 확인되었다. 또한, 최대 투수감소율은 92.6 %로 자기치유 특성을 만족하는 결과를 확인하였다.

참외 시설재배 토양에 대한 유효규산 추출방법 비교 (Evaluation of Available Soil Silicon Extracting Procedures for Oriental Melon)

  • 조현종;최희열;이용우;정종배
    • 한국토양비료학회지
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    • 제37권4호
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    • pp.251-258
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    • 2004
  • 밭작물에 대한 규산질 비료의 시용이 널리 이루어지고 있으나 적정시용수준이 밝혀져 있지 못하며 또한 밭토양에서의 유효규산 측정방법이 구명되어있지 못한 실정이다. 본 연구는 참외 시설재배지 토양에 대하여 유효규산 측정방법을 구명하기 위해 수행되었다. 경북 성주지역의 참외 시설재배지,10개소의 토양과 참외 잎 시료를 채취하여 가용성 토양 규산 함량과 잎 중의 총 규산 함량을 분석하였다. 가용성 토양 규산은 0.5 N HCI, 1 N sodium acetate buffer (pH 4.0). citric acid 1%, water, Tris buffer (pH 7.0), 그리고 1주간 담수하는 방법 등으로 추출하였으며, 식물체 규산은 autoclave 방법으로 추출하였다. 추출액중의 가용성 규산은 비색법으로 정량하였다. 각 추출방법별로 가용성 토양규산 함량과 식물체규산 함량과의 관계를 비교하였는데, 1 N sodium acetate buffer 방법이 토양 규산과 식물체 규산 관계를 가장 뚜렷한 포화곡선으로 나타내었다. 포화곡선으로부터 산출된 참외 잎 중의 포화 규산 함량은 약 $14g\;SiO_2\;kg^{-1}$이었고 1 N sodium acetate buffer 방법으로 추출할 경우토양 규산 함량 $120mg\;SiO_2\;kg^{-1}$이 참외에 적정한 수준인 것으로 나타났다. 특히 1 N sodium acetate buffer방법의 경우 참외 잎 중의 규산 함량이 포화되는 수준 이하의 토양 규산 함량 범위에서는 토양 규산 함량과 식물체 규산 함량 사이에 유의성 있는 상관관계가 있었다. 따라서 현재 우리나라에서 논토양의 유효규산 측정방법으로 널리 사용퇴고 있는 1 N sodium acetate buffer를 이용한 유효규산 추출방법이 밭토양에도 적용될 수 있을 것으로 판단되나 앞으로 다양한 작물과 토양을 대상으로 계속적인 연구가 요구된다.

지속성 제제의 개발에 관한 연구 (I) 아스코르빈산 나트륨의 CAP 마이크로캅셀의 제조 및 평가 (Studies on the Development of Sustained Release Preparation (I) Preparation and Evaluation of CAP Microcapsules of Sodium Ascorbate)

  • 신상철;고익배
    • Journal of Pharmaceutical Investigation
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    • 제21권4호
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    • pp.253-262
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    • 1991
  • Microencapsulation of sodium ascorbate with cellulose acetate phthalate(CAP) by coacervation/ phase separation method were carried out. Various factors affecting microencapsulation, i.e., surfactant concentration. CAP concentration, stirring speed and treatment of spermaceti as a sealing agent were studied. Dissolution rate. particle size distribution, surface feature and stability test were investigated. CAP microcapsules prepared using 0.5% span 80 as a surfactant showed smooth and round surfaces. The release of sodium ascorbate was retarded by microencapsulation with CAP and by sealant treatment with spermaceti. When triturated with sodium bicarbonate, CAP microcapsules were more stable than unencapsulated sodium ascorbate under various RH conditions at $37^{\circ}C$.

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Carbonic anhydrase influences asymmetric sodium and acetate transport across omasum of sheep

  • Rabbani, Imtiaz;Rehman, Habib;Martens, Holger;Majeed, Khalid Abdul;Yousaf, Muhammad Shahbaz;Rehman, Zia Ur
    • Animal Bioscience
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    • 제34권5호
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    • pp.880-885
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    • 2021
  • Objective: Omasum is an important site for the absorption of short chain fatty acids. The major route for the transport of acetate is via sodium hydrogen exchanger (NHE). However, a discrepancy in the symmetry of sodium and acetate transport has been previously reported, the mechanism of which is unclear. In this study, we investigated the possible role of carbonic anhydrase (CA) for this asymmetry. Methods: Omasal tissues were isolated from healthy sheep (N = 3) and divided into four groups; pH 7.4 and 6.4 alone and in combination with Ethoxzolamide. Electrophysiological measurements were made using Ussing chamber and the electrical measurements were made using computer controlled voltage clamp apparatus. Effect(s) of CA inhibitor on acetate and sodium transport flux rate of Na22 and 14C-acetate was measured in three different flux time periods. Data were presented as mean±standard deviation and level of significance was ascertained at p≤0.05. Results: Mucosal to serosal flux of Na (JmsNa) was greater than mucosal to serosal flux of acetate (JmsAc) when the pH was decreased from 7.4 to 6.4. However, the addition of CA inhibitor almost completely abolished this discrepancy (JmsNa ≈ JmsAc). Conclusion: The results of the present study suggest that the additional protons required to drive the NHE were provided by the CA enzyme in the isolated omasal epithelium. The findings of this study also suggest that the functions of CA may be exploited for better absorption in omasum.

알칼리 처리된 제지슬러지의 메탄발효에 미치는 몇몇 첨가제의 효과 (The effects of some additives on Methane Fermentation of Paper Mill Sludge treated with Alkali)

  • 최종우;이규승;박승희
    • 농업과학연구
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    • 제22권2호
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    • pp.134-142
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    • 1995
  • 제지슬러지의 메탄발효 효율을 높이기 위하여, 본 연구에서는 중온($35^{\circ}C$)과 고온($60^{\circ}C$) 메탄발효를 실시하였으며, 발효 촉진제로 기질(ethyl acetate), $F_{430}$의 구성성분(nickel), 생육인자 및 환원제(sulfur) 등의 화합물을 첨가한 후 메탄 생성 효율을 비교 조사하였다. 1. 제지슬러지를 단순히 $60^{\circ}C$로 가열해 주어도 섬유소가 분해됨을 간접적으로 확인하였으며, pH를 교정하기 위한 NaOH처리로 그 효과가 더 큰 것으로 나타났다. 2. 중온($35^{\circ}C$) 메탄발효 가스중 40%의 메탄함량을 나타낸 처리구는 nickel trioxide(5일), nickel sulfate(10일), nickel acetate(15일) 순 이었다. 3. 중온에서의 메탄생성 효율은 대조구(0.62%), ethyl acetate(0.21%), nickel acetate(2.14%), nickel sulfate(3.02%), nickel trioxide(3.34%)로 대조구에 비하여 최고 5.4배까지 증가하였으며, nickel화합물에서는 acetate< sulfate< trioxide의 순으로 메탄발효를 촉진하였다. 4. 고온 메탄발효 가스중 40%의 메탄함량을 나타낸 처리구는 nickel trioxide(3일), 혼합(5일), sodium sulfide(6일), 대조구(10일)의 순이었다. 5. 고온에서의 메탄생성 효율은 대조구(9.6%), ethyl acetate(4.8%), sodium sulfide(16.5%), nickel trioxide(19.8%), 혼합(31.9%) 처리구순으로 대조구에 비하여 최고 3.32배의 보다 높은 효율을 보여 주었으며, 중온 보다는 약 10배의 높은 효율을 나타내었다. 6. 중온과 고온 메탄발효후 pH는 메탄발효가 잘 진행된 발효조는 7.0($60^{\circ}C$, 혼합처리구)이었으나, 진행되지 못한 발효조($35^{\circ}C$, ethyl acetate)에서는 5.4로 나타났다. 7. 메탄발효폐액의 특성은 메탄발효가 잘 진행된 폐액의 COD 값이 컸으며, 전질소 함량은 낮았고, pH는 중성을 유지하였다.

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Application of Response Surface Methodology for Optimization of Lactic Acid Production Using Date Juice

  • Chauhan Kishor;Trivedi Ujjval;Patel K.C.
    • Journal of Microbiology and Biotechnology
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    • 제16권9호
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    • pp.1410-1415
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    • 2006
  • Media components, including date juice, sodium acetate, peptone, and $K_{2}HPO_4$, which were screened by Plackett-Burman fractional factorial design, were optimized for lactic acid production from date juice using the response surface method (RSM). Sodium acetate, peptone (p<0.0001), and $K_{2}HPO_4$ (p=0.0029) were highly significant in influencing the lactic acid production. Close correlationship between predicted and experimental values was observed. When the optimum values of the parameters obtained through RSM (25.0 g/l date sugar, 15.0 g/l sodium acetate, 19.1 g/l peptone, and 4.7 g/l $K_{2}HPO_4$) were applied, lactic acid production (22.7 g/l) increased by 50.33%, compared with unoptimized media (15.1 g/l). The subsequent validation experiments confirmed the validity of the statistical model.