• 한국세라믹학회지
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• 제55권6호
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• pp.576-580
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• 2018

In this study, a small amount of CoO was added to commercial Gd-doped $CeO_2$ (GDC) powder. The CoO addition greatly enhanced sinterability at low temperatures, i.e., more than 98% of relative density was achieved at $1,000^{\circ}C$. When GDC/8YSZ (8 mol% yttrium stabilized zirconia) bilayers were sintered, Co-doped GDC showed excellent adhesion to the YSZ electrolyte. Transmission electron microscope (TEM) analysis showed that there were no traces of liquid films at the grain boundaries of GDC, whereas liquid films were observed in the Co-doped GDC sample. Because liquid films facilitate particle rearrangement and migration during sintering, mechanical stresses at the interface of a bilayer, which are developed based on different densification rates between the layers, might be reduced. In spite of $Co^{2+}$ doping in GDC, the electrical conductivity was not significantly changed, relative to GDC.

• 한국세라믹학회지
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• 제45권9호
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• pp.544-548
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• 2008

The formation of $TiB_2-SiC$ ceramics from $TiB_2$-Polycarbosilane (PCS) mixtures was investigated. The powder mixture of $TiB_2$ with PCS was pressed at $300^{\circ}C$ with 200 MPa and sintered at $1700{\sim}2000^{\circ}C$ for 1 h in a flowing Ar atmosphere. The sintered density of $TiB_2$ with PCS is 93.7% after sintering at $2000^{\circ}C$ for 1 h, which is slightly smaller than that of the specimen without PCS. The microstructure of $TiB_2$ with PCS consists of small and uniform $TiB_2$ particles with well dispersed SiC particles derived from PCS. It is believed that the addition of PCS was effective to suppress the grain growth of $TiB_2$.

• 자원리싸이클링
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• 제11권5호
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• pp.34-38
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• 2002

최근 전자기기의 경박단소화로 페라이트 코아의 사용주파수가 고주파화 되고 있다. Mn-Zn ferrites에서 전력손실은 hysteresis loss, eddy current loss, residual loss로 구성되어 있으며, 500 KHz 이상의 주파수 영역에서는 residual loss가 주도적인 손실을 나타낸다. Induction level이 50 mT 이하인 경우 전력손실은 주파수의 3승 이상에 비례하여 증가한다. 작은 grain과 치밀한 미세구조는 고주파 대역에서 eddy current loss를 감소시킬 뿐만 아니라 자속밀도를 증가시켜 Residual loss역시 억제한다. Resonance frequency와 static permeability를 곱한 값이 큰 시편일수록 고주파 영역에서 낮은 전력손실을 보인다.

• 한국세라믹학회지
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• 제44권10호
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• pp.580-584
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• 2007

The ZrC layer instead of SiC layer is a critical and essential layer in TRISO coated fuel particles since it is a protective layer against diffusion of fission products and provides mechanical strength for the fuel particle. In this study, we carried out computational simulation before actual experiment. With these simulation results, Zirconium carbide (ZrC) films were chemically vapor deposited on $ZrO_2$ substrate using zirconium tetrachloride $(ZrCl_4),\;CH_4$ as a source and $H_2$ dilution gas, respectively. The change of input gas ratio was correlated with growth rate and morphology of deposited ZrC films. The growth rate of ZrC films increased as the input gas ratio decreased. The microstructure of ZrC films was changed with input gas ratio; small granular type grain structure was exhibited at the low input gas ratio. Angular type structure of increased grain size was observed at the high input gas ratio.

• 한국산업융합학회 논문집
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• 제6권4호
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• pp.299-305
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• 2003

This research is for the relationship with heat treatment cooling temprature and the characteristic of Mechanical properties of Boron-Addition-Steel, the main material and SM25C steel, the sub material, structure viewing fractography, hardness test, tensite test and are carried out after the manufacturing small-specimen treated with heat of $750^{\circ}C$, $850^{\circ}C$, $1050^{\circ}C$. The influence to the Mechanical properties accompanied by AISI51B20, Boron-Addition-steel shows the following result. 1. The influenc of heat treatment by the content of cabon-steel is dominant. Addition of boron result is Strengthening structure effectively by segregation and improving over all mechanical characters such as good. it results from the increase of temacity by the stability of inter granular with improvement of harden-ability. 2. Boron-Addition-Steel exist in the from of martensite structure accompanied by the ferrite precipitition centering around grain boundary, and is improved to Hv 200. 3. The height of harden-ability and fatigue stress the influence of heat results from crystal structure of martensite by difference of strength level in the structure of ferrite and doesn't have am effect on sensibility of temperature, and turns out to defend on production and growth of Matrix-structure-factor.

• 한국전기전자재료학회논문지
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• 제16권6호
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• pp.538-548
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• 2003

We studied effects by Re$_2$O$_3$(R=Dy, Gd, Ho) addition on the properties of Mn-Zn ferrite. The doping concentration range from 0.05 wt% to 0.25 wt%. All samples were prepared by standard fabrication of ceramics. With increasing the rare earth oxides, specific density and initial permeability increased on the whole. But, the tendencies such as upper result had the measured value on limitation and characteristics saturated or decreased properties after that. In case of excessive addition of additive beyond some level, initial permeability properties of ferrite have gone down in spite of anomalous grain. With increasing the content of additive, both the real and imaginary component of complex permeability and the magnetic loss (tan$\delta$) increased. Because the increased rate of real component had higher than imaginary component, magnetic loss increased none the less for increasing the real component related with magnetic permeability. But, the magnetic loss of ferrite doped with the rare earth oxides was lower than that of Mn-Zn ferrite at any rate. The small amount of present rare earth oxides in Mn-Zn ferrite composition led to enhancement of resistivity in bulk, and more so in the grain boundary. It was seem to be due to the formation of mutual reaction such as between iron ions and rare earth element ions.

• 한국재료학회지
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• 제13권6호
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• pp.365-368
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• 2003

Small amounts of additives such as mol % 0.13 NiO and mol % 0.01 $CaCO_3$were added to Cu-Zn-Mg ferrites. Basic composition of the Cu-Zn-Mg ferrites was $Cu_{Cu}$X/$Fe_{0.054}$ /$Zn_{0.486}$$Mg_{0.407}$ $Fe_{1.946}$ $O_4$(group A) and $Cu_{0.263}$$Fe_{0.027}$ $Zn_{0.503}$ $Mg_{0.262}$ $Fe_{1.973}$ $O_4$(group B). Specimens were sintered at different temperatures (1010, 1030, $1050^{\circ}C$) for 2 hours in air followed by an air cooling. Then, effects of various composition and sintering temperatures on the microstructure and the magnetic properties such as inductions, coercive forces, and initial permeabilities of the Cu-Zn-Mg ferrites were investigated. The average grain size increased with the increase of sintering temperature. The magnetic properties obtained from the aforementioned Cu-Zn-Mg ferrite specimens were 1,724 gauss for the maximum induction, 1.0 oersted for the coercive force, and 802 for the initial permeability. These magnetic properties indicated that the specimens could be utilized as the core of IFT (intermediate frequency transformer) and antenna in the amplitude modulation.

• 센서학회지
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• 제9권1호
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• pp.76-82
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• 2000

본 연구에서는 내부전극 접합기술을 이용하여 적층구조의 PTC 서미스터를 제작하였다. 적층구조 PTC 서미스터는 저항, 소형, 대전류 등의 특징을 갖는다. PTC 특성을 조사하기 위하여 첨가제효과, 전압-전류특성, 온도특성, 복합임피던스 특성 등을 측정하였다. 적층구조 PTC서미스터는 저항의 온도특성과 전압-전류특성에서 높은 비선형성을 나타내었다. 적층수가 증가함에 따라 상온저항이 감소되는 특성이 결정립의 효과에 기인됨을 알았다. 전류의 스윗칭 변화는 적층구조가 갖는 열용량의 크기에 비례하였으며, 적층수가 증가할수록 스윗칭 시간이 증가하였다.

• 한국주조공학회지
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• 제37권4호
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• pp.101-107
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• 2017

This study investigated the effect of Pd on the microstructure, tensile and creep properties of Mg-4Al-2Sn (AT42) alloy at a high temperature for transportation-related industrial applications. AT42-xPd (x = 0, 1 and 2 wt. %) alloys were prepared using a permanent mould casting method. The microstructures of the as-cast alloys were characterized by the presence of the intermetallic phases $Mg_{17}Al_{12}$, $Mg_2Sn$ and $Al_4Pd$. The addition of Pd was found to improve the tensile properties of AT42 at room and at elevated temperatures, and to increase the creep resistance at elevated temperatures. A small amount of Pd could markedly improve the tensile properties of AT42 by means of grain-refinement and the dispersion of secondary phase strengthening. Moreover, the thermally stable phase $Al_4Pd$ effectively improves the creep resistance of AT42 due to the strengthened grain boundaries and the suppressed formation of $Mg_{17}Al_{12}$.

• 한국해양공학회지
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• 제20권4호
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• pp.43-49
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• 2006

Detailed investigations were carried out on the stability of the dredged soil bed against wave actions, aimedat establishing the design method of artificial tidal flats using dredged soil. The soil was dredged at Nagoya port, Japan, and has a mean grain size of 0.013mm. Basic features of artificial dredged soil bed against wave actions were explained from a series of model experiments in a wave flume. The two types of section shapes were employed; one is a horizontal bed and the other is a sloped one. Changes of the bed profile, shear strength, grain size distribution and water content, according to the wave actions, were measured in detail. The cumulative effect of the wave actions, over about one week, was investigated. A dredged soil bed moves withthe wave actions with relatively small wave height. It should be especially. noted that the clay component is dissolved and flown out, away from the surface layer, and consequently the surface layer hardens, as if it is covered with sand. Wren the wave height is gradually increased, the bed is not liquefied and the shear strength of the dredged bed is increased by a wave-induced dissipation of pore pressures in the bed and a decrease of clay component by the wave-induced leakage.