• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.8
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• pp.1175-1187
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• 1997

Densification behavior and grain growth of zirconia powder compacts are investigated under high temperature. Experimental data are obtained for zirconia powder under pressureless sintering, sinter forging and hot isostatic pressing. The constitutive equations by Kwon et al. are used for diffusional creep and grain growth. The constitutive equations by McMeeking and co-workers are also included to study the effect of power-law creep. These constitutive equations are implemented into a finite element program (ABAQUS) to investigate the friction effect during sinter forging and the canning effect during hot isostatic pressing. The agreements between experimental data and finite element results are very good in pressureless sintering and hot isostatic pressing, but not as good in sinter forging.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.13 no.4
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• pp.23-29
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• 2004

In this study, four kinds of $Si_3N_4$-based ceramic cutting tools with different sintering time were fabricated to investigate the relation among mechanical properties, grain size and tool life. They were used to turn gray cast iron at a cutting speed of 330m/min and depth of cut of 0.5mm and 1mm in dry, continuos cutting conditions. Multiple linear regression model was used to determine the relations among the mechanical property, grain size and the density. It was found that the combination of hardness and fracture toughness showed a good relation with tool life. It was also shown that hardness was the most important single element for the tool life.

• Proceedings of the KSME Conference
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• 2000.04b
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• pp.416-421
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• 2000

We have developed a simple model for describing the non-spherical particle growth phenomena using modified 1-dimensional sectional method. In this model, we solve simultaneously particle volume and surface area conservation sectional equations which consider particles' irregularities. From the correlation between two conserved properties of sections, we can predict the evolution of the aggregates' morphology. We compared this model with a simple monodisperse-assumed model and more rigorous two dimensional sectional model. For the comparison, we simulated silica and titania particle formation and growth in a constant temperature reactor environment. This new model shows a good agreement with the detailed two dimensional sectional model in total number concentration, primary particle size. The present model can also successfully predict particle size distribution and morphology without costing very heavy computation load and memory needed for the analysis of two dimensional aerosol dynamics.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.24 no.7
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• pp.1020-1027
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• 2000

A simple model for describing the non-spherical particle growth phenomena has been developed. In this model, we solve simultaneously particle volume and surface area conservation sectional equations that consider particles' non-sphericity. From the correlation between two conserved properties of sections, we can predict the evolution of the aggregates' morphology. This model was compared with a simple monodisperse-assumed model and more rigorous two-dimensional sectional model. For comparison, formation and growth of silica particles have been simulated in a constant temperature reactor environment. This new model showed good agreement with the detailed two-dimensional sectional model in total number concentration and primary particle size. The present model successfully predicted particle size distribution and morphology without costing very heavy computation load and memory needed for the analysis of two dimensional aerosol dynamics.

• Journal of the Korean Ceramic Society
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• v.39 no.12
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• pp.1183-1189
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• 2002

In order to develope the porous alumina ceramics with high strength, the pore characteristics and compressive strength were investigated in terms of relation to the conditions of spark-plasma sintering and the contents of graphite as a pore precursor. Porous alumina bodies were successfully prepared by spark-plasma sintering and burning out graphite in air. High porous bodies were fabricated by sintering at 1000${\circ}C$ for 3 min under a pressure of 30 MPa, heating rate of 80${\circ}C$/min and on-off pulse type of 12:2. For example, alumina bodies prepared by the addition of 10∼30 vol% graphite showed high porosity of 50∼57%. Also, the open porosity increased with graphite content. The relationship between pore characteristics and graphite contents could be explained by percolation model depending on cluster number and size. Porous alumina bodies prepared by the addition of 10∼30 vol% graphite showed the high compressive strength of 55∼200 MPa. This great improvement in strength was considered to be mainly due to the spark-plasma discharges and the self-heating action between particles.

• The Journal of Advanced Prosthodontics
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• v.12 no.3
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• pp.167-172
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• 2020

PURPOSE. The aim of the present study was to investigate the passive fit of metal substructure after repetitive firing processes in implant-supposed prosthesis. MATERIALS AND METHODS. Five implants (4 mm diameter and 10 mm length) were placed into the resin-based mandibular model and 1-piece of screw-retained metal substructure was produced with the direct metal laser sintering (DMSL) method using Co-Cr compound (n = 10). The distance between the marked points on the multiunit supports and the marginal end of the substructure was measured using a scanning electron microscope (SEM) at each stage (metal, opaque, dentin, and glaze). 15 measurements were taken from each prosthesis, and 150 measurements from 10 samples were obtained. In total, 600 measurements were carried out at 4 stages. One-way ANOVA test was used for statistical evaluation of the data. RESULTS. When the obtained marginal range values were examined, differences between groups were found to be statistically significant (P<.001). The lowest values were found in the metal stage (172.4 ± 76.5 ㎛) and the highest values (238.03 ± 118.92 ㎛) were determined after glaze application. When the interval values for groups are compared with pairs, the differences between metal with dentin, metal with glaze, opaque with dentin, opaque with glaze, and dentin with glaze were found to be significant (P<.05), whereas the difference between opaque with metal was found to be insignificant (P=.992). CONCLUSION. Passive fit of 1-piece designed implant-retained fixed prosthesis that is supported by multiple implants is negatively affected by repetitive firing processes.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.11 no.3
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• pp.127-131
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• 2001

The effect of grain shape on the grain growth behavior of oxide system was investigated as afunction of liquid content during liquid phase sintering. As a model system, the solid grains of $Al_{2}O_{3}$ and MgO were selected during liquid phase sintering, i.e. faceted shape of $Al_{2}O_{3}$ in $CaAl_{2}Si_{2}O_{8}$ liquid phase and spherical shape of MgO in $CaMgSiO_{4}$ liquid phase. The average grain size of MgO with spherical shape was decreased with increasing the liquid phase content, whereas that of $Al_{2}O_{3}$ with faceted shape was independent of liquid phase content. In the case of $Al_{2}O_{3}$ grains with faceted shape, which interfaces are expected to be atomically flat, are likely to grow by the interfacial reaction controled process. Whereas, in the case of MgO grains with spherical shape, which interface are expected to be atomically rough, are likely to grow by the diffusion controlled process.

• Journal of the Microelectronics and Packaging Society
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• v.29 no.4
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• pp.41-47
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• 2022

Ag sintering technologies have received great attention as it was applied to the inverter of Tesla's electric vehicle Model III. Ag sinter bonding technology has advantages in heat dissipation design as well as high-temperature stability due to the intrinsic properties of the material, so it is useful for practical use of SiC and GaN devices. This study was carried out to understand the sinter joining temperature effect on the robust Ag sintered joints in air without pressure within 10 min. Electroplated Ag finished Cu dies (3 mm × 3 mm × 2 mm) and substrates (10 mm × 10 mm × 2 mm) were introduced, respectively, and nano Ag paste was applied as a bonding material. The sinter joining process was performed without pressure in air with the bonding temperature as a variable of 175 ℃, 200 ℃, 225 ℃, and 250 ℃. As results, the bonding temperature of 175 ℃ caused 13.21 MPa of die shear strength, and when the bonding temperature was raised to 200 ℃, the bonding strength increased by 157% to 33.99 MPa. When the bonding temperature was increased to 225 ℃, the bonding strength of 46.54 MPa increased by about 37% compared to that of 200 ℃, and even at a bonding temperature of 250 ℃, the bonding strength exceeded 50 MPa. The bonding strength of Ag sinter joints was directly influenced by changes in the necking thickness and interfacial connection ratio. In addition, developments in the morphologies of the joint interface and porous structure have a significant effect on displacement. This study is systematically discussed on the relationship between processing temperatures and bonding strength of Ag sinter joints.

• Journal of the Korean Ceramic Society
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• v.24 no.4
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• pp.392-396
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• 1987

Pure barium titanate was sintered at $1340^{\circ}C$ for 2, 4, 8, 16 hr to control their grain size. The measurements of breakdown strength and partial discharge characteristics were performed under rising AC voltage(60Hz). With increase of sintering time, the average grain size was increased and breakdown strength was slightly decreased. Partial discharge in pores was observed under high voltage, and a model of dielectric break down in barium titanate ceramics is proposed.

• Proceedings of the Korea Society for Energy Engineering kosee Conference
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• 2003.11a
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• pp.291-297
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• 2003

For the present study, three heat pipes with different thickness of sintered metal wick were manufactured, and their operational performances, such as capillary limit and thermal resistance were tested and compared with theoretical predictions. Experimental results showed good agreement with those by the theoretical model, and that seemed to present that the sintering process we had developed ;n the present study was valid.