• 한국분말재료학회지
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• 제5권2호
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• pp.89-97
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• 1998

Sintering behavior of nanostructured(NS) W-Cu powders prepared by mechanical alloying (MA) was investigated as a function of sintering temperature. MA NS W-2owt%Cu and W-3owt%Cu composite powders with the crystal size of 20-30 nm were annealed at 90$0^{\circ}C$, and thermal characteristics of those powders were investigated by DSC. Sintering behavior of MA NS W-Cu composite powders was investigated during the solid-state sintering and the Cu-liquid phase sintering. The new nanosintering phenonenon of MA W-Cu powders at solid-state sintering temperature was suggested to explain the W-grain growth in the inside of MA powders. The sintering densification of MA NS W-Cu powders was enhanced at Cu melting temperature by arrangement of MA powders, i.e., the first rearrangement of MA powders was occurred, and then the rearrangement of W-grains in the sintered parts was also took place during liquid-phase sintering, i.e., the second rearrangement was happened. Due to the double rearrangement process of MA NS W-Cu powders, the high sintered density with more than 96%o was obtained and the fine and high homogeneous state of W and Cu phases was achieved by sintering at 1200 $^{\circ}C$.

• 한국분말재료학회지
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• 제5권4호
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• pp.286-292
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• 1998

Ni$_3$Al intermetallic compound has been tested as a binder phase, in order to improve the oxidation resistance and the mechanical properties of TiC-Ni cermet at a high temperature. The wettability of $Ni_3Al$ on TiC and the optimum sintering condition were investigated in TiC-(30, 40) vol% $Ni_3Al$ cermets with the sintering temperature (1380~$1430^{\circ}C$) and time (30~99 min). The results are summarized as follows: 1) Ni$_3$Al showed good wettability on TiC above 1400$^{\circ}C$ ; 2) The shrinkages of the specimens increased with the sintering temperature, the sintering time and the binder content, whereas the relative densities were decreased; 3) Any other phase did not appeared in the microstructures of all sintered cermets. The grain sizes of TiC became larger as the sintering temperature and the sintering time as well as the binder content increased; 4) The hardness of the cermets decreased with increase in the sintering temperature and the sintering time as well as the binder content; 5) The transverse-rupture strength of the cermets increased with the sintering temperature and the sintering time, whereas it decreased with the binder content.

• 한국산업융합학회 논문집
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• 제24권3호
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• pp.283-288
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• 2021

A tungsten material using a pressure sintering process and a titanium sintering additive was prepared to evaluate the microstructure, and mechanical properties of flexural strength and hardness. In addition, the reliability on each hardness data was evaluated by analyzing the distribution of the hardness of the tungsten material using the Weibull probability distribution. In particular, the optimal manufacturing conditions were analyzed by analyzing the correlation between the sintering temperature and the mechanical properties of the tungsten sintered body. Although the sintering density of the tungsten material was hardly changed up to 1700 ℃, but it was increased at 1800 ℃. The hardness of the tungsten sintered material increased as the sintering temperature increased, and in particular, the tungsten material sintered at 1800 ℃ showed a high hardness value of about 1790 Hv. It showed relatively excellent flexural strength at a sintering temperature of 1800 ℃.

• The Journal of Advanced Prosthodontics
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• 제14권1호
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• pp.56-62
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• 2022

PURPOSE. The aim of this study was to investigate shade changes in fully- and pre-crystalized CAD-CAM lithium disilicate crowns after the required and additional firing processes. MATERIALS AND METHODS. One hundred and five crowns of shade A1 with high translucency were milled out of CAD-CAM lithium disilicate blocks and categorized as follows (n = 15): (1) restorations fabricated from Straumann n!ce with no additional sintering process; (2) restorations fabricated from Straumann n!ce with one additional sintering process; (3) restorations fabricated from Straumann n!ce with two additional sintering processes; (4) restorations fabricated from Amber Mill with one sintering process; (5) restorations fabricated from Amber Mill with two sintering processes; (6) restorations fabricated from IPS e.max CAD with one sintering process; (7) restorations fabricated from IPS e.max CAD with two sintering processes. All restorations were evaluated with a color imaging spectrophotometer. RESULTS. All restorations presented some color alteration from the original shade both after a single and after two firing processes. CONCLUSION. The required and additional sintering processes for restorations fabricated with chairside CAD-CAM lithium disilicate blocks cause an alteration of the original shade selected. Shade A1 high translucency restorations tend to change to a more yellowish B1 shade after a sintering process.

• 한국재료학회지
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• 제33권12호
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• pp.537-549
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• 2023

The sintering shrinkage behaviors of low temperature cofired ceramics (LTCC) and resistors were compared using commercial LTCC and thick-film resistor pastes, and factors influencing the camber of cofired resistor/LTCC bi-layers were also investigated. The onset of sintering shrinkage of the resistor occurred earlier than that of LTCC in all resistors, but the end of sintering shrinkage of the resistor occurred earlier or later than that of LTCC depending on the composition of the resistor. The sintering shrinkage end temperature and the sintering shrinkage temperature interval of the resistor increased as the RuO₂/glass volume ratio of the resistor increased. The camber of cofired resistor/LTCC bi-layers was obtained using three different methods, all of which showed nearly identical trends. The camber of cofired resistor/LTCC bi-layers was not affected by either the difference in linear shrinkage strain after sintering between LTCC and resistors or the similarity of sintering shrinkage temperature ranges of LTCC and resistors. However, it was strongly affected by the RuO₂/glass volume ratio of the resistor. The content of Ag and Pd had no effect on the sintering shrinkage end temperature or sintering shrinkage temperature interval of the resistor, or on the camber of cofired resistor/LTCC bi-layers.

• The Journal of Advanced Prosthodontics
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• 제16권1호
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• pp.25-37
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• 2024

PURPOSE. To investigate the effect of sintering programs and surface treatments on surface properties, phase transformation and flexural strength of monolithic zirconia. MATERIALS AND METHODS. Zirconia specimens were sintered using three distinct sintering programs [classic (C), speed (S), and superspeed (SS)] (n = 56, each). One sample from each group underwent scanning electron microscopy (SEM) and grain size analysis following sintering. Remaining samples were divided into five subgroups (n = 11) based on the surface treatments: control (CL), polish (P), glaze (G), grind + polish (GP), and grind + glaze (GG). One sample from each subgroup underwent SEM analysis. Remaining samples were thermally aged. Monoclinic phase volume, surface roughness, and three-point flexural strength were measured. Monoclinic phase volume and surface roughness were analyzed by Kruskal-Wallis and Dunn tests. Flexural strength was analyzed by two-way ANOVA and Weibull analysis. The relationships among the groups were analyzed using Spearman's correlation analysis. RESULTS. Sintering program, surface treatment, and sintering × surface treatment (P ≤ .010) affected the monoclinic phase volume, whereas the type of surface treatment and sintering × surface treatment affected the surface roughness (P < .001). Type of sintering program or surface treatment did not affect the flexural strength. Weibull analysis revealed no significant differences between the m and σ_o values. Monoclinic phase volume was positively correlated with surface roughness in the SGG and SSP groups. CONCLUSION. After sintering monolithic zirconia in each of the three sintering programs, each of the surface treatments can be used. However, for surface quality and aging resistance, G or GG can be recommended as a surface finishing method.

• 한국안전학회지
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• 제9권3호
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• pp.28-33
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• 1994

It is very important to have exact informations on the properties and characteristics of the sintering material as a new material of machine elements. To study the sintering spur gear and the sintering specimen to be consisted of Fe-Cu-C, the constant stress amplitude fatigue test is performed by using an electrohydrolic survo-controlled pulsating tester. Consequently, the S-N curves are obtained and the fatigue strength is compared with flaw depth. Accordingly, this study presents the fatigue strength of sintering spur gears, the critical notch depth of sintering materials and the effects of flaw depth on the bending fatigue strength.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.246-247
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• 2006

A new approach to sintering loose packed, coarse aluminum alloy powder to full or near full density is presented. A controlled amount of water vapor is introduced into the sintering atmosphere, which disru pts the oxide film and allows metallurgical contact between particles. In addition, supersolidus liquid phase sintering is used to sinter the part to full density. Since the method is particularly applicable to uncompacted powders, it is potentially useful for sintering aluminum powder preforms manufactured by 3DPrinting and powder injection molding.

• 한국세라믹학회지
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• 제28권10호
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• pp.824-830
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• 1991

$\alpha$-SiC(B; 0.4 wt, C; 3 wt%) was sintered in Ar atmosphere from 205$0^{\circ}C$ to 220$0^{\circ}C$ by means of pressureless sintering and gas pressure sintering in order to find optimum sintering condition of $\alpha$-SiC. Mechanical properties and microstructures of sintered bodies were investigated according to sintering method. The effect of sintering condition on sinterability of $\alpha$-SiC was also examined by using the dilatometer. 97.5% and 98.8% of theoretical density were obtained from pressureless sintering and gas pressure sintering of $\alpha$-SiC powder, respectively. And modulus of rupture was measured as 270~350 MPa and 420 MPa respectively.

• 한국분말재료학회지
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• 제11권1호
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• pp.55-59
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• 2004

TiNi bodies were produced from (Ti＋Ni) powder mixture by spark-plasma sintering procerg. The sintering behavior was investigated through the measurement of change in density, densification rate, phase analysis and microstructure. Irrespective of heating rate, sintered bodies with above 97％ relative density could be obtained. TiNi with B2 structure was confirmed as the major phase and $Ti_2Ni,\;TiNi_3$, unreacted Ti, Ni as the second phase. Increase in heating rate suppressed a formation of intermediate phase during sintering process. Increase in holding time at sintering temperature led to a compositional homogenization.