• 제목/요약/키워드: shrinkage rate

검색결과 453건 처리시간 0.025초

토기 복원용 Epoxy Putty 개발 및 물성에 관한 연구 (A study on the development and the physical properties of Epoxy Putty for earthenware restoration)

  • 배진수;정다솜;김우현;강석인;위광철
    • 보존과학회지
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    • 제30권1호
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    • pp.103-109
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    • 2014
  • 본 연구는 토 도기 보존 처리과정에 있어서 결손부위를 복원하는 재료의 문제점과 단점 등을 보완한 재료를 개발하고자 하였다. 우선 기존 재료의 문제점으로는 높은 수축률과 낮은 접착력으로 인한 2 차 파손의 문제, 심한 황변현상으로 인한 이질감의 문제, 재료의 비가역성으로 인한 재용해의 문제 및 높은 강도로 인한 가공성의 문제, 작업 과정 중 긴 경화 시간으로 인한 처짐 현상 및 도구나 장갑에 묻어 유물의 표면을 오염시키는 문제 등이 있다. 이러한 문제점을 해결하기 위해 현재 사용되고 있는 토 도기 복원 재료들 중 Epoxy 수지를 중심으로 종류 및 물성을 파악한 후 개발 목표를 설정하였다. 개발 된 Epoxy는 5 분 내외에 경화가 이루어지는 토기 복원용 Epoxy Putty이다. 토기 복원 방법에 있어서 Epoxy Putty의 경우 페이스트(Paste) 형태로 빠르게 경화되어 작업의 편리성을 높였으며, 표면 오염 등의 단점을 보완하였다. 또한 Epoxy 원액에 백색의 Micro-balloon을 사용함으로 인해 Coloring에 용이하고 경량화하도록 하였으며, 저수축 및 가공성이 우수한 복원 재료를 개발하였다.

경소백운석(輕燒白雲石) 부산물(副産物)을 활용(活用)한 바닥 몰탈용 팽창재(膨脹材)의 특성검토(特性檢討) (A Study on Characterization of Expansion Agent in Mortar with Light Burned Dolomite By-Product)

  • 이건호;민승의;이형우;조진상;조계홍;한춘
    • 자원리싸이클링
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    • 제21권6호
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    • pp.12-22
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    • 2012
  • 본 연구는 제강용도로 사용하기 위해 돌로마이트를 하소후 남은 2 mm 이하의 경소백운석 부산물을 건축용 바닥 몰탈의 기존 팽창재로서 활용 가능성을 검토하고자 하였다. 경소백운석은 $600{\sim}800^{\circ}C$ 정도에서 하소하였을 때 반응성이 높은 준결정상태의 활성 마그네시아로 존재하게 되며, 이 활성화된 마그네시아는 수화초기 Brucite gel을 형성하여 수화물 비율을 상대적으로 줄여 치밀한 조직을 형성하는 원인으로 작용하고, 수화후기에는 결정질의 Brucite가 형성되어 수축 현상을 억제하며 부피가 2배 이상 팽창하여 화학적 수축균열 방지 역할을 하게 되는 것이다. 실험결과 경소백운석은 기존 사용 중인 팽창재 대비 동일량 적용시 압축강도는 우수하게 확인되었으나, 반응성은 기존 팽창재(생석회+무수석고)에 비해 다소 낮게 측정되었다. 하지만 팽창재로서의 역할은 충분한 것으로 확인되었으며, 공사기간 단축 등 부가적인 효과를 나타내었다.

MILC 성장 속도에 비정질 실리콘의 기하학적 형상이 미치는 영향 (The Effect of Geometric Shape of Amorphous Silicon on the MILC Growth Rate)

  • 김영수;김민선;주승기
    • 한국재료학회지
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    • 제14권7호
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    • pp.477-481
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    • 2004
  • High quality polycrystalline silicon is very critical part of the high quality thin film transistor(TFT) for display devices. Metal induced lateral crystallization(MILC) is one of the most successful technologies to crystallize the amorphous silicon at low temperature(below $550^{\circ}C$) and uses conventional and large glass substrate. In this study, we observed that the MILC behavior changed with abrupt variation of the amorphous silicon active pattern width. We explained these phenomena with the novel MILC mechanism model. The 10 nm thick Ni layers were deposited on the glass substrate having various amorphous silicon patterns. Then, we annealed the sample at $550^{\circ}C$ with rapid thermal annealing(RTA) apparatus and measured the crystallized length by optical microscope. When MILC progress from narrow-width-area(the width was $w_2$) to wide-width-area(the width was $w_1$), the MILC rate decreased dramatically and was not changed for several hours(incubation time). Also the incubation time increased as the ratio, $w_1/w_2$, get larger. We can explain these phenomena with the tensile stress that was caused by volume shrinkage due to the phase transformation from amorphous silicon to crystalline silicon.

기상 활성화법에 의한 대나무 활성탄 제조 (Production of Activated Carbon from Bamboo by Gas Activation Method)

  • 조광주;박영철
    • 에너지공학
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    • 제13권2호
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    • pp.166-172
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    • 2004
  • The activated carbon was produced from Sancheong bamboo by steam and carbon dioxide gas activation methods. The carbonization of raw material was conducted at 90$0^{\circ}C$ and gas activation reactions were conducted with respect to various conditions. -activation temperature 750-90$0^{\circ}C$, the flow rate of steam 0.5-2g-$H_2O$/g-char$.$hr, the flow rate of carbon dioxide 5-30$m\ell$-$CO_2$/g-char-min and activation time 1-5 hr. The prepared activated carbons were measured yield, the adsorption capacity of iodine and methylene blue, BET specific surface area and pore size distribution. The adsorption capacity of iodine (680.5-1526.1 mg/g) and methylene blue (18.3-221.5 mg/g) increased with creasing activation temperature and activation time. The adsorption capacity of iodine and methylene blue increased with the activation gas quantity in the range of 0.5-1.5g-$H_2O$/g-charㆍhr, 5-18.9$m\ell$-Co$_2$/g-charㆍmin. But those decreased over those range due to the pore shrinkage. The steam activation method was superior in efficiency to carbon dioxide activation method.

펄스전류활성소결법을 이용한 스퍼터링 타겟용 Cu-Mn 소결체 제조 및 특성평가 (Fabrication and Property Evaluation of Cu-Mn Compacts for Sputtering Target Application by a Pulsed Current Activated Sintering Method)

  • 장준호;오익현;임재원;박현국
    • 한국분말재료학회지
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    • 제23권1호
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    • pp.1-7
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    • 2016
  • Cu-Mn compacts are fabricated by the pulsed current activated sintering method (PCAS) for sputtering target application. For fabricating the compacts, optimized sintering conditions such as the temperature, pulse ratio, pressure, and heating rate are controlled during the sintering process. The final sintering temperature and heating rate required to fabricate the target materials having high density are $700^{\circ}C$ and $80^{\circ}C/min$, respectively. The heating directly progresses up to $700^{\circ}C$ with a 3 min holding time. The sputtering target materials having high relative density of 100% are fabricated by employing a uniaxial pressure of 60 MPa and a sintering temperature of $700^{\circ}C$ without any significant change in the grain size. Also, the shrinkage displacement of the Cu-Mn target materials considerably increases with an increase in the pressure at sintering temperatures up to $700^{\circ}C$.

Prediction and Measurement of Residual Stresses in Injection Molded Parts

  • Kwon, Young-Il;Kang, Tae-Jin;Chung, Kwansoo;Youn, Jae Ryoun
    • Fibers and Polymers
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    • 제2권4호
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    • pp.203-211
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    • 2001
  • Residual stresses were predicted by a flow analysis in the mold cavity and residual stress distribution in the injection molded product was measured. Flow field was analyzed by the hybrid FEM/FDM method, using the Hele Shaw approximation. The Modified Cross model was used to determine the dependence of the viscosity on the temperature and the shear rate. The specific volume of the polymer melt which varies with the pressure and temperature fields was calculated by the Tait\`s state equation. Flow analysis results such as pressure, temperature, and the location of the liquid-solid interface were used as the input of the stress analysis. In order to calculate more accurate gap-wise temperature field, a coordinate transformation technique was used. The residual stress distribution in the gap-wise temperature field, a coordinate transformation technique was used. The residual stress distribution in the gap-wise direction was predicted in two cases, the free quenching, under the assumption that the shrinkage of the injection molded product occurs within the mold cavity and that the solid polymer is elastic. Effects of the initial flow rate, packing pressure, and mold temperature on the residual stress distribution was discussed. Experimental results were also obtained by the layer removal method for molded polypropylene.

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PTT/Wool/Modal Air vortex사 편성물의 의류 착용성능과 쾌적물성 (Wearing Performance and Comfort Property of PTT/Wool/Modal Air Vortex Yarn Knitted Fabrics)

  • 김현아
    • 한국의류학회지
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    • 제40권2호
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    • pp.305-314
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    • 2016
  • This paper investigated the applicable possibility of PTT and wool staple fibers to the air vortex system as high quality yarns for a high emotional and comfort garment. It was found that the tactile hand of vortex yarn knitted fabrics was harsher than ring and compact yarns knitted fabrics. It was observed that formability and sewability of air vortex yarn knitted fabrics seemed worse than ring and compact yarns due to low tensile and compressional resilience and high bending and shear hysteresis of air vortex yarn knitted fabrics. It revealed that wicking and drying rates of air vortex yarn knitted fabric were better than ring and compact yarns; in addition, the heat keepability of vortex yarn knitted fabric was higher than ring and compact yarns due to low thermal conductivity and max heat flow rate ($Q_{max}$). Any difference of thermal shrinkage between air vortex and ring yarn knitted fabrics was not shown, but pilling characteristic of air vortex yarn knitted fabric was superior. However, it was shown that wicking, drying, thermal property and pilling characteristics of air vortex yarn knitted fabric were superior due to air vortex yarn structure with parallel fibers in the core part and periodical and fasciated twists in the sheath part of the yarns.

재생 골재의 품질 평가에 관한 연구 (콘크리트폐재의 미분말을 혼입한 재생몰탈의 경우) (A Study on the Quality Evaluation of Recycled Aggregate (In the case of the Mortar Produced With Recycled Concrete Powder))

  • 서상교
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1996년도 봄 학술발표회 논문집
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    • pp.172-179
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    • 1996
  • Recently, the broken concrete lumps resulting from the demolition of concrete structures are creshed for reuse as aggregates(i.e. recycled fine and gravel). And also, in the processing of crusing, the recycled powder of an equivalent of between 20% to 30% by wt.% of the broken concrete lumps is generated. The extensive research of recycled concrete aggregates has been carried out in various parts of the world. But less reseatch on the reuse of recycled concrete powder has been carried out. It is the purpose of this report that the study on the quality evaluation of recycled aggregates for recycled concrete. In specially, this report deals with the properties such as flow, compressive strength, bending strength, drying shrinkage and wight loss rate of mortars replaced standard fine aggregate with recycled powders at the rate of 3, 7, 15, 20 and 30 wt.%. Since the characteristics of recycled mortars with the recycled powders were comparable to those of the normal mortar without the recycled powders as described above, its concretes could be found extensive application in such field as concrete products.

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사형(砂型)의 열전달(熱傳達)에 관(關)한 연구(硏究) (A Study on Heat Transfer in Sand Molds)

  • 이종남;김광배
    • 한국주조공학회지
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    • 제2권1호
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    • pp.2-11
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    • 1982
  • In order to investigate the relationship between the thermal characteristics of the various molds as green sand mold, dry sand mold, $CO_2$ mold and shell mold, and the solidification characteristics of molten metal, the thermal analysis of rarious molds and melt were performed. The structure of Al-Castings was a/so observed. Results obtained in this experiment were as follows : 1) The heating rate of the molds was increased in the order of green sand mold, $CO_2$ mold, dry sand mold and shell mold, On the other hand the solidification time of the melts was shortened in the order of dry sand mold castings, $CO_2$ mold castings, green sand mold castings and shell mold castings. 2) The arrest temperature period in the heating curve of the green sand mold was resulted from the eraporation of moisture contained in mold, which was transfered to the outer side of the mold. 3) The temperature fluctuation of the melt in the shell mold was considered to be resulted from the combution heat of resin contained in the mold. 4) The amounts of heat absorption of the molds were increased in the order of dry sand mold, $CO_2$ mold, green sand mold and shell mold. 5) The higher the solidification rate was, the longer was its shrinkage pipe and the finer its grain size.

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제지(製紙) 슬러지 소각재(燒却滓)를 활용(活用)한 섬유보강(纖維補强)콘크리트의 균열(龜裂) 억제(抑制) 효과(效果) (Effect on the Crack Resistance of Fiber Reinforced Concrete using Incinerated Paper Mill Sludge Ash)

  • 김남욱
    • 자원리싸이클링
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    • 제17권4호
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    • pp.10-20
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    • 2008
  • 본 연구는 아직까지 활용실적이 적은 제지슬러지소각재를 대량으로 활용할 수 있는 방법을 도출하기 위하여 제지슬러지소각재를 시멘트의 대체재로 사용하고자 하였다. 또한 제지슬러지소각재 대체 시 나타나는 단점인 수화열 및 흡수율의 증가로 인한 수축균열을 폴리프로필렌섬유 및 셀룰로오스섬유를 혼입하여 이에 대한 제어효과를 고찰하여 제지슬러지소각재의 시멘트 대체재로써의 활용가능성을 규명하였다.