• Title/Summary/Keyword: semi-quantitative analysis

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Comparison of Quantitative Analysis of Radioactive Corrosion Products Using an EPMA and X-ray Image Mapping

  • Jung, Yang Hong;Choo, Young Sun
    • Corrosion Science and Technology
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    • v.19 no.5
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    • pp.231-238
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    • 2020
  • Radioactive corrosion product specimens were analyzed using an electron probe microanalyzer (EPMA) and X-ray image mapping. It is difficult to analyze the composition of radioactive corrosion products using an EPMA due to the size and rough shape of the surfaces. It is particularly challenging to analyze the composition of radioactive corrosion products in the form of piled up, small grains. However, useful results can be derived by applying a semi-quantitative analysis method using an EPMA with X-ray images. A standard-less, semi-quantitative method for wavelength dispersive spectrometry. EPMA analysis was developed with the objective of simplifying the analytical procedure required. In this study, we verified the reasonable theory of semi-quantitative analysis and observed the semi-quantitative results using a sample with a good surface condition. Based on the validated results, we analyzed highly rough-surface radioactive corrosion products and assessed their composition. Finally, the usefulness of the semi-quantitative analysis was reviewed by verifying the results of the analysis of radioactive corrosion products collected from spent nuclear fuel rods.

Wooden framed structures with semi-rigid connections: Quantitative approach focused on design needs

  • Santana, C.L.O.;Mascia, N.T.
    • Structural Engineering and Mechanics
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    • v.31 no.3
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    • pp.315-331
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    • 2009
  • Mechanical connections are recognized as extremely important elements in the aspect of strength and structural safety. However, classical structural model does not consider the connection stiffness properties, and are based on models with pinned or rigid joints only. In fact, mechanical connections are deformable and behave not linearly, affecting the whole structure and inducing nonlinear behavior as well. The quantification of this effect, however, depends on the description of the working of the connectors and the wood response under embedment. The theoretical modeling of wood structures with semi-rigid connections involves not only the structural analysis, but also the modeling of both single and grouped moment resisting connectors and the study of the wood properties under embedment. The proposal of this paper is to approach these aspects, and to quantitatively study the influence of the moment resistant connection in wooden framed structures. Comparisons between rigid and semi-rigid connections and between linear and nonlinear analysis lead to quantitative results.

A preliminary study of semi-quantitative, comparative evaluation of split or half fingerprints using Densitometric Image Analysis (DIA) - Inter-analyst differences for split or half fingerprints -

  • Song, Minkyu;Kim, Seung-chan;Choi, Sung-Woon
    • Analytical Science and Technology
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    • v.34 no.2
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    • pp.56-67
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    • 2021
  • Due to the difficulty of grading visualized fingerprints with previously known evaluation methods for the comparison of split fingerprints, a preliminary study was performed with the densitometric image analysis (DIA) method as a potential quantitative and supplementary evaluation method. Each image of inked split fingerprints was divided into 4 zones for analysis. Weekly intra- and inter- analysis by two analysts with three whole fingerprints that were constructed by combining inked split fingerprints showed that the average area values and the ranges of difference fluctuation were not significantly different between strong fingerprints and strong-weak pairs, while they were different in weak fingerprints and weak-weak pairs. In the case of weak fingerprints, the exact acquisition of ridges was difficult and this seemed to influence the results. An additional study is needed for the improved reliability using DIA method with weak fingerprints such as 8 zones division rather than 4 zones. In addition, the analysis results performed by several analysts at different times should be used to improve the reliability of the analysis method further. Based on the above result, it can be judged that utilizing the DIA method as a secondary evaluation method of the existing scoring system would be effective with the additional studies especially on weak fingerprints.

Prediction of Maintenance Period of Equipment Through Risk Assessment of Thermal Power Plants (화력발전설비 위험도 평가를 통한 기기별 정비주기 예측)

  • Song, Gee Wook;Kim, Bum Shin;Choi, Woo Song;Park, Myung Soo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.10
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    • pp.1291-1296
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    • 2013
  • Risk-based inspection (RBI) is a well-known method that is used to optimize inspection activities based on risk analysis in order to identify the high-risk components of major facilities such as power plants. RBI, when implemented and maintained properly, improves plant reliability and safety while reducing unplanned outages and repair costs. Risk is given by the product of the probability of failure (POF) and the consequence of failure (COF). A semi-quantitative method is generally used for risk assessment. Semi-quantitative risk assessment complements the low accuracy of qualitative risk assessment and the high expense and long calculation time of quantitative risk assessment. The first step of RBI is to identify important failure modes and causes in the equipment. Once these are defined, the POF and COF can be assessed for each failure. During POF and COF assessment, an effective inspection method and range can be easily found. In this paper, the calculation of the POF is improved for accurate risk assessment. A modified semi-quantitative risk assessment was carried out for boiler facilities of thermal power plants, and the next maintenance schedules for the equipment were decided.

A Study on Semi Quantitative Risk Analysis for Air Separation Unit using a GRA(Generic Risk Analysis) Method (GRA(Generic Risk Analysis) 기법을 이용한 공기분리시설에 대한 준 정량적 위험성 평가에 관한 연구)

  • Shin, Jung-Soo;Byun, Hun-Soo
    • Journal of the Korean Institute of Gas
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    • v.17 no.1
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    • pp.56-66
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    • 2013
  • The gas production plants supply the inert gas to production plants for maintaining safe operation and also supply combustible, flammable, explosive and toxic gases as functions of basic materials needed for producing chemical goods. In addition, gas plants need to be safe and reliable operation because they are operated under high temperature, high pressure, cryogenic and catalytic reactions. As these plants have a complex process in operation, there has been a risk that major industrial accidents such as a fire, explosion and toxic gas released, also risks of asphyxiations by inert gases and burns caused by high temperature and cryogenic substances. This study is to carry out the semi quantitative risk assesment method which is the generic risk analysis (GRA). This method is applied to air separation unit(ASU) to identify its initial risk, safety barriers, residual risk and elements important for safety(EIS). The result of this study, suggested the management tools and procedures of implementation for EIS management.

Relationship between 18F-FDG PET/CT Semi-Quantitative Parameters and International Association for the Study of Lung Cancer, American Thoracic Society/European Respiratory Society Classification in Lung Adenocarcinomas

  • Lihong Bu;NingTu;Ke Wang;Ying Zhou;Xinli Xie;Xingmin Han;Huiqin Lin;Hongyan Feng
    • Korean Journal of Radiology
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    • v.23 no.1
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    • pp.112-123
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    • 2022
  • Objective: To investigate the relationship between 18F-FDG PET/CT semi-quantitative parameters and the International Association for the Study of Lung Cancer, American Thoracic Society/European Respiratory Society (IASLC/ATS/ERS) histopathologic classification, including histological subtypes, proliferation activity, and somatic mutations. Materials and Methods: This retrospective study included 419 patients (150 males, 269 females; median age, 59.0 years; age range, 23.0-84.0 years) who had undergone surgical removal of stage IA-IIIA lung adenocarcinoma and had preoperative PET/CT data of lung tumors. The maximum standardized uptake values (SUVmax), background-subtracted volume (BSV), and background-subtracted lesion activity (BSL) derived from PET/CT were measured. The IASLC/ATS/ERS subtypes, Ki67 score, and epidermal growth factor/anaplastic lymphoma kinase (EGFR/ALK) mutation status were evaluated. The PET/CT semi-quantitative parameters were compared between the tumor subtypes using the Mann-Whitney U test or the Kruskal-Wallis test. The optimum cutoff values of the PET/CT semi-quantitative parameters for distinguishing the IASLC/ATS/ERS subtypes were calculated using receiver operating characteristic curve analysis. The correlation between the PET/CT semi-quantitative parameters and pathological parameters was analyzed using Spearman's correlation. Statistical significance was set at p < 0.05. Results: SUVmax, BSV, and BSL values were significantly higher in invasive adenocarcinoma (IA) than in minimally IA (MIA), and the values were higher in MIA than in adenocarcinoma in situ (AIS) (all p < 0.05). Remarkably, an SUVmax of 0.90 and a BSL of 3.62 were shown to be the optimal cutoff values for differentiating MIA from AIS, manifesting as pure ground-glass nodules with 100% sensitivity and specificity. Metabolic-volumetric parameters (BSV and BSL) were better potential independent factors than metabolic parameters (SUVmax) in differentiating growth patterns. SUVmax and BSL, rather than BSV, were strongly or moderately correlated with Ki67 in most subtypes, except for the micropapillary and solid predominant groups. PET/CT parameters were not correlated with EGFR/ALK mutation status. Conclusion: As noninvasive surrogates, preoperative PET/CT semi-quantitative parameters could imply IASLC/ATS/ERS subtypes and Ki67 index and thus may contribute to improved management of precise surgery and postoperative adjuvant therapy.

A pilot application study of densitometric image analysis as a potential comparative evaluation method for visualized fingerprints

  • Kim, Eun-Ji;Kim, Soo-Kyung;Seo, Kyung-Suk;Choi, Sung-Woon
    • Analytical Science and Technology
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    • v.33 no.4
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    • pp.197-207
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    • 2020
  • The current comparison methods with scoring systems that are used to compare visualized latent fingerprints (LF) have disadvantages. Evaluators using these methods are prone to make errors and fail to discriminate LFs correctly to notice the differences among those LFs. Therefore, a comparative and quantitative evaluation method that is capable of obtaining more objective and quantitative results is needed. Densitometric image analysis (DIA) is used in other fields as a reliable semi-quantitative comparison method. To apply DIA to LFs, the potential variables that can occur during the DIA process were tested. The visualized ridges of LFs can be compared using the concentration of dots against the background to make it possible to analyze the ridges with DIA. The variables that can be present during the DIA process include the thickness of the analysis line, the number of ridges to be taken, the number of divided zones within each of the fingerprints, and the angles of the analysis line against the ridge lines that were selected. From the analysis of the inked fingerprints and circular lines that are similar to fingerprints, the angle of the analysis lines with the ridge line was the most significant variable. The preliminary test result was applied to the comparison of LFs that were developed with the powder method and then compared with the AFIS analysis. A similar trend was found, and a more detailed and semi-quantitative comparison of the visualized LFs was possible. In the future, it is necessary to check the evaluative ability of the DIA method by analyzing the visualized LFs with other various development methods. However, DIA is currently an option that can be used as an objective comparative evaluation method during fingerprint studies with supplementary role.

Analysis for the Driving Dynamic Characteristics of Large Scale Semi-Trailer Equipped with Swivel Axle and Hydropneumatic Suspension Unit (회전 차축 및 유기압 현가장치를 장착한 대용량 세미 트레일러의 주행 동특성 해석)

  • Ha, Taewan;Park, Jungsoo
    • Journal of the Korea Institute of Military Science and Technology
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    • v.25 no.2
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    • pp.196-209
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    • 2022
  • Driving dynamic characteristics of semi-trailer loaded with precise equipments are very important to protect them from vibration, impact or other disturbances. In this paper, in order to identify the driving dynamic characteristics of the large scale semi-trailer equipped with swivel axle and hydropneumatic suspension unit, Dynamics Modeling & Simulation(M&S) were performed using general Dynamics Analysis Program(RecurDyn V9R2). The semi-trailer was modeled as two types - one is Multi Rigid Body Dynamics(MRBD) model, and the other Rigid-Flexible Body Dynamics(RFlex) one. The natural vibration mode and frequencies of semi-trailer body, acceleration of dummy-weight, pitch, roll and yaw of dummy-weight, swivel axle and hydropneumatic suspension cylinder support structure, and acting force of hydropneumatic suspensions etc. were obtained from the M&S. Additionally frequency analysis were performed using the data of behavior obtained from above M&S. Generally the quantitative results of RFlex are larger than them of MRBD in view of magnitude of the comparable parametric values.

Typical Pseudo-accident Scenarios in the Petrochemical Process (석유화학 공정의 가상사고 시나리오 유형분석)

  • 윤동현;강미진;이영순;김창은
    • Journal of the Korean Society of Safety
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    • v.18 no.3
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    • pp.75-80
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    • 2003
  • This paper presents a set of typical pseudo-accident scenarios related to major equipments in petrochemical plants, which would be useful for performing such quantitative risk analysis techniques as fault tree analysis, event tree analysis, etc. These typical scenarios address what the main hazard of each equipment might be and how the accident might develop from an "initiating event". The proposed set of accident scenarios consists of total thirteen (13) scenarios specific for five (5) major equipments like reactor, distillation column, etc., and has been determined and screened out of one hundred and twenty-five (125) potential accident scenarios that were generated by performing semi-quantitative risk analysis practically for twenty-five (25) petrochemical processes, considering advices from the operation experts. It is assumed that with simple consideration or incorporation of plant-specific conditions only, the proposed accident scenarios could be easily reorganized or adapted for the relevant process with less time and labor by the safety engineers concerned in the petrochemical industries.ndustries.

물리정수법에 의한 형광 X선분석과 만장굴석주의 연대측정

  • 택훈
    • Proceedings of the Speleological Society Conference
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    • 1993.07a
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    • pp.163-172
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    • 1993
  • Cheju island is situated at about 90km south of southern most tip of the Korean peninsula. Its shape is an ellips with size of 80$\times$40$km^2$, and it is characterized by a symmetrical form whose peak is Mt. Halla (1950m). Major chemical composition of the rock samples from Manjang gul cave is determined by XRF using the fundamental parameter method consisting of fully auto quantitative analysis, semi quantitative analysis (order estimation) and group quantitative analysis. Judging from chemical composition ($SiO_2 = 53.07Wt% Fe_2 O_3=11.34Wt%, MgO=6.48Wt%, Na_2 O=3.07Wt%, K_2 O=1.05Wt%$), this rocks may belong to non alkalic basalt. K-Ar ages of two rocks samples from the Manjang gul cave are also determined. The discrepancy of K-Ar ages is found. They are 0.03Ma and 0.42Ma, respectively. This paper describes some problems experienced in dating young volcanic rocks and then discusses chemical composition, X-ray fluorescence analysis and the age of the formation of a lava tunnel such as Manjang gul cave in cheju Island.

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