• Title/Summary/Keyword: semi-liquid

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Formulations of Bacillus thuringiensis Insecticides by Liquid and Semi-Solid Fermentations. (액상 및 반고체배지 발효에 의한 Bacillus thuringiensis 살충제의 제조)

  • 이형환
    • Microbiology and Biotechnology Letters
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    • v.26 no.4
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    • pp.369-372
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    • 1998
  • Microbial insecticide formulations were prepared by liquid and semi-solid fermentations using Bacillus thuringiensis subsp. kurstaki, HL-106 (BTK-HL106), B. thuringiensis subsp. israelensis HL-63 (BTI-HL63) and B. sphaericus 1593 (BS-1593) strains. The liquid fermentation medium contained molasses 2%, dextrose 1.5%, peptone 2%, D-xylose 0.025%, CaCl$_2$ 0.1%, K$_2$HPO$_4$ 0.1%, KH$_2$PO$_4$ 0.1%, MgSO$_4$$.$7H$_2$O 0.03%, FeSO$_4$$.$7H$_2$O 0.002%, ZnSO$_4$$.$7H$_2$O 0.02%. The composition of the semi-solid fermentation medium was rice bran 45.2%, zeolite 31%, yeast powder 0.02%, corn powder 5%, dextrose 3%, lime 0.3%, NaCl 0.06%, CaCl$_2$ 0.02%, and H$_2$O 15.42%. Insecticide formulations produced in the liquid fermentation named BTK-HL106, BTI-HL63 and BS-1593 pesticides and those in the semi-solid fermentation were designated as BTK-HL106-1, BTI-HL63-1 and BS-1593-1 pesticides, respectively. The number of spore (endotoxin crystals) was 2.65${\times}$10$\^$9/ spores per $m\ell$ in the BTK-HL106 and 3.5${\times}$10$\^$10/ in the BTK-HL106-1 3.8${\times}$10$\^$9/ spores in the BTI-HL63 and 7.0${\times}$10$\^$10/ in the BTI-HL63-1, and 7.5${\times}$10$\^$9/ in the BS-1593 and 1.4${\times}$10$\^$10/ in the BS-1593-1. The spores in the BS-1593 formulation was produced two times more than the other formulations. The spores in the BTI-HL63-1 were contained twice than those in the BTK-HL106-1, and five times than those in the BS-1593-1. The results indicated that spore (endotoxin crystals) productions in the semi-solid fermentation increased about ten times than those in the liquid fermentations. $LC_{50}$s of the BTI-HL63 and BS-1593 were 4.5 $\mu\textrm{g}$, and those of the BTI-HL63-1 and BS-1593-1 were 1.5 $\mu\textrm{g}$. $LC_{50}$ of the BTK-HL106 was 1.5 mg and that of the BTK-HL106-1 was 0.9 mg. The $LC_{50}$s of the formulations in the semi-solid fermentations showed about two to three times higher than those in the liquid fermentations.

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A Study on Induction Heating with Forced Surface Cooling in Semi-Solid Forming Process (반용융 성형에서 강제 표면 냉각에 의한 유도 가열 방법에 관한 연구)

  • Park Joon Hong;Choi Young
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.1
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    • pp.97-102
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    • 2005
  • The procedure of semi-solid forming is composed of heating a billet, forming, compression holding and ejecting step. There are several methods to heat a billet during semi-solid forming process such as electric heating and induction heating. Usually in semi-solid forming process, induction heating has been adopted to achieve more uniform temperature of semi-solid material. Although induction heating is better method than any others, however, there is still difference of temperature between internal part and surface part of semi-solid material. Worse yet, in case of high liquid fraction of semi-solid material, liquid of the billet will flow down though solid of the billet still remains, which is very difficult to handle. In the present study, induction heating of semi-solid material with compulsive surface cooling has been performed to obtain uniform distribution of temperature. Distribution of temperature of the billets was measured and compared with that of conventional distribution of temperature. By this new induction heating method, not only temperature over the whole billet become uniform, but also control of temperature is possible.

A Study on Induction Heating with Compulsive Surface Cooling in Semi-Solid Forming Process (반용융 성형에서 간제 표면 냉각에 의한 유도 가열 방법에 관한 연구)

  • Choi, J. C.;Kim, B. M.;Choi, Y.;Park, J. H.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.11a
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    • pp.465-468
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    • 2000
  • The procedure of semi-solid forming is composed of heating a billet, forming, compression holding and ejecting step. There are several methods to heat a billet during semi-solid forming process such as electric heating and induction heating. Usually in semi-solid forming process, induction heating has been adopted to achieve more uniform temperature of semi-solid material. Although induction heating is better method than any others, however, there is still difference of temperature between internal part and surface part of semi-solid material. Worse yet, in case of high liquid fraction of semi-solid material, liquid of the billet will flow down though solid of the billet still remains, which is very difficult to handle. In the present study, induction heating of semi-solid material with compulsive surface cooling has been performed to obtain uniform distribution of temperature. Distribution of temperature of the billets was measured and compared with that of conventional distribution of temperature. By this new induction heating method, not only temperature over the whole billet become uniform, but also control of temperature is possible.

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Finite Element Analysis of Extrusion Process in Semi-Solid State (반용융 재료의 압출공정에 관한 유한요소해석)

  • 황재호;고대철;민규식;김병민;최재찬
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.06a
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    • pp.5-15
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    • 1997
  • It is the objective of this study that by conducting the serni-solid extrusion using A12024, the effect of various process variables on the quality of extruded product and extrusion force is understood. The results of experiment are compared with those of finite element simulation in order to verify the effectiveness of the developed FE-simulation code. In order to simulate densification in the deformation of serni-solid material, the semi-solid material is assumed to be composed of solid region as porous skeleton following compressible visco-plastic model and liquid region following Darcy's equation for the liquid flow saturated in the interstitial space. Then the flow and deformation of the semi-solid alloy are analyzed by coupling the deformation of the porous skeleton and the flow of the eutectic liquid. It is assumed that initial solid fraction is homogeneous. Yield and plastic potential function presented by Kuhn and constitutive model developed by Gunasekera are used for solid skeleton.

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A Semi-solid Bonding between Rolled Steel for Structural Parts and Lead Bronze Alloy (구조용 압연강재와 연청동 합금의 반용융 확산접합)

  • 김우열;박홍일;이길근;서원찬
    • Journal of Welding and Joining
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    • v.18 no.1
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    • pp.70-76
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    • 2000
  • A rolled steel for structural parts and lead bronze alloy were bonded each other by a new semi-solid diffusion bonding process to investigate the effect of the process parameters, for example bonding temperature and bonding time, on the interface characteristics, and bonding behavior. It can be possible that manufacture of the bonded steel/lead bronze which has a cylindrical shape with inserted the lead bronze alloy into the steel ring by the diffusion bonding process under the semi-solid condition of the lead bronze alloy without any pressure and flux. It has been know that the control of the amount of the liquid phase in semi-solid lead bronze alloy was very important to obtain soundness interface, since the shear strength of the bonded steel/lead bronze at 850℃ for 60 minutes under the condition of about 40% of the liquid phase in the lead bronze alloy shows maximum value, 210 MPa. The shear strength increases with an increase in bonding time and show maximum value, and then decreases.

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Deformation Analysis of Semi-Solid Aluminum Material Considering Seperation Phenomena of Solid Particles (고상입자의 분리현상을 고려한 Semi-Solid 알루미늄재료의 변형해석)

  • 최진석;강충길;김기훈
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.03a
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    • pp.98-105
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    • 1997
  • The behaviour of alloys in the semi-solid state strongly depends on the imposed stress state and on the morphology of the phase which can very from dendritic to globular. The estimation of behaviour characteristic in the compression simulation with seim-solid materials are calculated by finite element method with proposed algorithm. The proposed theoretical model and a various boundary conditions for compression process is investigated with the coupling calculation between the liquid phase flow and the solid phase deformation. The simulation process considering soldification phenomena is performed to the isothermal conditions of two dimensional problems. To analysis of compression process by using semi-solid materials, a new stress-strain relationship is described, and compression analysis is performed by viscoelastic model for the solid phase and the Darcy's law for the liquid flow. The calculated results for compression force and ram displacement will be compared to experimental data.

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Effects of Microstructure Morphology on Fluid Flow Characteristics of A356 Commercial Alloy in Semi-Solid Slurry (반고상 A356 합금 슬러리의 미세조직에 따른 유동특성에 관한 연구)

  • Kim, Jae-Min;Lee, Seung-Hoon;Hong, C.P.
    • Journal of Korea Foundry Society
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    • v.25 no.6
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    • pp.240-248
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    • 2005
  • The rheocasting characteristics are strongly influenced by the microstructural morphology such as particle size, form factor and contiguity. In this study, the effect of structural morphology on fluid flow characteristics of A356 semi-solid alloy was investigated with a vacuum suction fluidity test. Semi-solid metal slurry was made by the mechanical stirring, the liquidus casting, and H-NCM to be analysed. H-NCM could obtain uniform and fine globular microstructures of 0.9 form factor and 55 ${\mu}m$ particle size. Inoculation was found to be effective for reducing particle size, however, for H-NCM it should be avoided due to the cause of increasing contiguity. The fluidity test indicated that the non-stirring method had higher fluidity and smaller liquid segregation in the same solid faction of 0.4 than the stirring method, for smaller particle size and higher form factor. It was observed that liquid segregation decreased as the particle size is smaller and form factor is higher. The results of die-casting experiment were a good agreement with those of fluidity test.

The effect of the injection condition on liquid segregation in semi-solid die casting process (반응고 다이캐스팅공정에서 사출조건이 액상편석에 미치는 영향)

  • 신현기;서판기;강충길
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.05a
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    • pp.70-73
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    • 2003
  • Semi-solid processing is now becoming of great interest for the production of various parts by pressure die casting. Many advantages are associated with this forming process at the condition that the forming operation is performed under appropriate conditions in terms of alloy microstructure, injection velocity and pressure. In this study, to look into the relation along them, the experiment of semi-solid die casting has been peformed with various condition of injection, and investigated their microstrucure and solid fraction

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A Compression Behavior of Semi-Solid Material and Finite Element Analysis Considering Flow of Liquid Phase (반응용재료의 압축거동 및 액상의 유동을 고려한 유한요소해석)

  • Gang, Chung-Gil;Yun, Jong-Hun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.12
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    • pp.3715-3727
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    • 1996
  • Compression behavior of semi-solid aluminum alloys with controlled solid fractions was investigated in the present study. The stress and strain relationships were obtained from the compression test. Variations of the solid fraction distribution and the material behaviour were investigated for various friction coeffieiants and die speedsd. For a finite element analysis, the semi-solid material was described by a compressible regid viscoplastic model for the solid region and darcy's law for the liquid region. The computed results were compared with experimental data for the validity of the yield criteria.

Neutralization of Synthetic Alkaline Wastewater with CO2 in a Semi-batch Jet Loop Reactor (Semi-batch Jet Loop Reactor에서 연소 배가스중 CO2를 이용한 알칼리 폐수 중화)

  • Son, Min-Ki;Sung, Ho-Jin;Lee, Jea-Keun
    • Journal of the Korean Society of Combustion
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    • v.18 no.2
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    • pp.17-22
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    • 2013
  • In this study, we tested the absorption of $CO_2$ in combustion gas into an alkaline wastewater to simultaneously control $CO_2$ and wastewater. During the experiment, we investigated the effects of operating parameters on neutralization characteristics of the wastewater by using $CO_2$ in a bench-scale semi-batch jet loop reactor (0.1 m diameter and 1.0 m in height). The operating parameters investigated in the study are gas flow rate of 1.0-2.0 L/min, liquid recirculation flow rate of 4-32 L/min, and liquid temperature of $20-25^{\circ}C$. It was shown that the initial pH of wastewater rapidly decreased with increased gas flow rate for a given liquid recirculation flow rate. This was due to the increase in the gas holdup and the interfacial area at higher gas flow rate in the reactor. At constant gas flow rate, the time required to neutralize the wastewater initial pH of 10.1 decreased with liquid recirculation flow rate ($Q_L$), reached a minimum value in the range of $Q_L$ = 16-24 L/min, and then increased with further increase in $Q_L$. Further, the time required to neutralize the wastewater was shortened at higher temperatures.