• Title/Summary/Keyword: sedimentation method

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Cations of Soil Minerals and Carbon Stabilization of Three Land Use Types in Gambari Forest Reserve, Nigeria

  • Falade, Oladele Fisayo;Rufai, Samsideen Olabiyi
    • Journal of Forest and Environmental Science
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    • v.37 no.2
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    • pp.116-127
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    • 2021
  • Predicting carbon distribution of soil aggregates is difficult due to complexity in organo-mineral formation. This limits global warming mitigation through soil carbon sequestration. Therefore, knowledge of land use effect on carbon stabilization requires quantification of soil mineral cations. The study was conducted to quantify carbon and base cations on soil mineral fractions in Natural Forest, Plantation Forest and Farm Land. Five 0.09 ha were demarcated alternately along 500 m long transect with an interval of 50 m in Natural Forest (NF), Plantation Forest (PF) and Farm Land (FL). Soil samples were collected with soil cores at 0-15, 15-30 and 30-45 cm depths in each plot. Soil core samples were oven-dried at 105℃ and soil bulk densities were computed. Sample (100 g) of each soil core was separated into >2.0, 2.0-1.0, 1.0-0.5, 0.5-0.05 and <0.05 mm aggregates using dry sieve procedure and proportion determined. Carbon concentration of soil aggregates was determined using Loss-on-ignition method. Mineral fractions of soil depths were obtained using dispersion, sequential extraction and sedimentation methods of composite soil samples and sieved into <0.05 and >0.05 mm fractions. Cation exchange capacity of two mineral fractions was measured using spectrophotometry method. Data collected were analysed using descriptive and ANOVA at α0.05. Silt and sand particle size decreased while clay increased with increase in soil depth in NF and PF. Subsoil depth contained highest carbon stock in the PF. Carbon concentration increased with decrease in aggregate size in soil depths of NF and FL. Micro- (1-0.5, 0.5-0.05 and <0.05 mm) and macro-aggregates (>2.0 and 2-1.0 mm) were saturated with soil carbon in NF and FL, respectively. Cation exchange capacity of <0.05 mm was higher than >0.05 mm in soil depths of PF and FL. Fine silt (<0.05 mm) determine the cation exchange capacity in soil depths. Land use and mineral size influence the carbon and cation exchange capacity of Gambari Forest Reserve.

Study on the size-based separation of nano to micron particles in natural water and soil using flow and sedimentaion Field-flow fractionation (흐름 및 침강 장-흐름 분획법에 의한 자연수 및 토양 중 나노 크기로부터 마이크론 입자들의 크기별 분리에 관한 연구)

  • Eum, Chul Hun;Kang, Dong Young;Lee, Tae Woo;Lee, Seungho
    • Analytical Science and Technology
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    • v.22 no.1
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    • pp.75-81
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    • 2009
  • A flow and sedimentation field-flow fractionation method has been used to characterize colloidal particles in environmental samples. The opposed flow sample concentration (OFSC) method was employed. The OFSC procedure was optimized for the analysis of particles in ground water with respect to various experimental parameters including sample introduction time, flow rates, etc. The effectiveness in low concentration and characterization of the OFSC-FlFFF was demonstrated with GW-1 and GW-2 ground water samples. Ground water of upto 100 mL has been successfully loaded, concentrated, and characterized by OFSC-FlFFF. The OFSC technique allow the application of FlFFF possible for the separation and characterization of colloidal particles in very low concentrations. The results show FFF provides a simplified alternative to existing off-line concentration procedures, and shows a high potential for the applications to the analysis of dilute colloidal particles in the environmental samples.

Thermoluminescence Dating of Pottery Shards by Subtraction Method (Subtraction 방법을 이용한 TL 연대측정법에 의한 토기 시편의 절대연대 결정)

  • Shin, Hyun-Sang;Lee, Chang-Woo;Nam, Young-Mee;Jee, Kwang-Yong;Park, Byung-Bin
    • Analytical Science and Technology
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    • v.13 no.4
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    • pp.403-411
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    • 2000
  • This study described a method of thermoluminescence dating of pottery shards using subtraction method. TL measurement was achieved using two different types of samples prepared by quartz inclusion method and fine-grain technique. Fine grains (size range: $5-10{\mu}m$) were separated by suspending grounded pottery samples into acetone solution and sedimentation quantitatively. In quartz inclusion method quartz grains in the size range of 90 to $125{\mu}m$ diameter were obtained by extracting the quartz crystals embed in the pottery shards and etching them with 1.0 M HF solutions. The archaeological dose of both the quartz and fine grains was determined from the dose calibration curves obtained from sequential irradiation of $^{137}Cs$ gamma and $^{241}Am$ alpha source to the samples and TL measurement of natural samples, in which the alpha dose of 4.60 Gy for the Packjae pottery was obtained using subtraction method. Annual alpha dose rates ($3.05{\pm}0.11$ mGy/yr.) were determined by the analysis of U, Th contents in the pottery shards and evaluation of the values with Bell's equation. Dividing the alpha dose accumulated in the pottery shards by the annual alpha dose rate, we found age of approximately $1508{\pm}80$ years B.P. (AD. ca. 492 yr.) for the Packjae pottery. It matches well with the archeological age estimate (middle of 5th century) within 10 percent uncertainty and thereby conforms the age of the pottery sample.

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Development of Computer Code for Simulation of Multicomponent Aerosol Dynamics -Uncertainty and Sensitivity Analysis- (다성분 에어로졸계의 동특성 묘사를 위한 전산 코드의 개발 -불확실성 및 민감도 해석-)

  • Na, Jang-Hwan;Lee, Byong-Whi
    • Nuclear Engineering and Technology
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    • v.19 no.2
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    • pp.85-98
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    • 1987
  • To analyze the aerosol dynamics in severe accidents of LMFBR, a new computer code entitled MCAD (Multicomponent Aerosol Dynamics) has been developed. The code can treat two component aerosol system using relative collision probability of each particles as sequences of accident scenarios. Coagulation and removal mechanisms incorporating Brownian diffusion and gravitational sedimentation are included in this model. In order to see the effect of particle geometry, the code makes use of the concept of density correction factor and shape factors. The code is verified using the experimental result of NSPP-300 series and compared to other code. At present, it fits the result of experiment well and agrees to the existing code. The input variables included are very uncertain. Hence, it requires uncertainty and sensitivity analysis as a supplement to code development. In this analysis, 14 variables are selected to analyze. The input variables are compounded by experimental design method and Latin hypercube sampling. Their results are applied to Response surface method to see the degree of regression. The stepwise regression method gives an insight to which variables are significant as time elapse and their reasonable ranges. Using Monte Carlo Method to the regression model of LHS, the confidence level of the results of MCAD and their variables is improved.

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Protein and Arabinoxylan Contents of Whole Grains from Wheat Genetic Resources Cultivated in Korea (국내에서 재배된 밀 유전자원의 통밀에서 단백질 및 아라비노자일란 함량 분석)

  • Yang, Jinwoo;Park, Jinhee;Son, Jae-Han;Kim, Kyeong-Hoon;Kim, Kyeong-Min;Jeong, Han-Yong;Kang, Chon-Sick;Son, Ji-Young;Park, Tae-Il;Choi, Changhyun
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.66 no.1
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    • pp.29-36
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    • 2021
  • Recently, phytochemicals in whole grains have received increasing attention because the increased consumption of whole grains and whole grain products has been associated with a reduced risk of chronic diseases. Among the phytochemicals in whole wheat, arabinoxylan influences various physiological activities and can aid the treatment of numerous health conditions, either directly or indirectly. In this study, 614 wheat germplasms, collected from the world, were cultivated in 2018 and harvested in 2019 in South Korea. The qualities of these whole grains, including seed protein content, were evaluated using the NIR spectrophotometric method, and arabinoxylan content was determined using enzymatic methods. The ash content was 0.36 to 2.80% and protein content was 7.66 to 20. The SDS-sedimentation for gluten complex ability ranged from 26.85 to 80.63 mL, and protein content showed a high correlation with SDS-sedimentation in the germplasms. Verify the result of the enzymatic method of arabinoxylan, the reliability of the experimental method was determined through repeatability, reproducibility, and recovery. The average value of the 614 resources was 51.64 mg/g of whole grain, and when classified according to the country of origin, the South Korean origin resources tended to have a higher content compared to the genetic resources of other countries. These results are expected to be used as basic data for setting standards for whole grain quality in wheat breeding systems.

Preparation of Nickel Hexacyanoferrate Ion Exchanger for Electrochemical Separation of Cations (양이온의 전기화학적 분리를 위한 페리시안니켈 이온교환체의 제조에 관한 연구)

  • Lee, Ji Hyun;Hwang, Young Gi
    • Applied Chemistry for Engineering
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    • v.21 no.1
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    • pp.52-57
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    • 2010
  • Although chemical sedimentation and ion exchange are usually applied to the treatment of heavy metal ions and radioactive cations, they have some serious disadvantages like a great consumption of chemicals, the disposal of valuable metals, and the secondary pollution of soil by the solid-waste. The advanced countries recently have studied the electrochemical ion exchange, combined electrochemical reduction and ion exchange, for the development of the alternative technique. This study has been performed to investigate the optimum condition for the preparation of the nickel hexacyanoferrate (NiHCNFe) which is an electrochemical ion exchanger. NiHCNFe film was deposited on the surface of nickel plate by chemical method or electrochemical method. The morphology and composition of NiHCNFe were observed by SEM and EDS, respectively. The peak current density of NiHCNFe was measured from the cyclic voltammograms of the continuous oxidation-reduction reaction in a parallel plane ion exchange electrode reactor. It was found that the chemical preparation method was better than the electrochemical method. The concentrated NiHCNFe was apparently deposited on nickel plate when dipping in the preparing solution for 118 h, especially. It also had a best durable performance as an ion exchange electrode.

Use of Spectrophotometry for Quantitative Determination of Soil Clay Content (분광광도계를 이용한 점토함량 분석)

  • Park, Soon-Nam;Kim, Kye-Hoon;Kang, Ji-Young
    • Applied Biological Chemistry
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    • v.48 no.2
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    • pp.183-188
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    • 2005
  • This study was conducted to develop a method for the quantitative determination of soil clay content by spectophotometry. The optimum wavelength obtained with reference clay minerals for spectrophotometry was 500 nm. For the proposed spectrophotometry, 0.5 g of soil sample was put in the 250 ml Erlenmeyer flask and 100 ml dispersing agent was added. After shaking the flask at 130 rpm with a mechanical shaker overnight, the flask was removed from the shaker and was shaken up-and-down for 30 seconds. With a micro-pipet, 4 ml of the suspension was transferred into the previously-inserted cell and the absorbance was measured instantly. Results by the spectrophotometry for clay content analysis were compared with those by the conventional sedimentation technique (the pipet method). The proposed equation was $y\;=\;38.03x_1-0.17x_2-1.17$, where y, $x_1$, and $x_2$ were clay content (%) by the pipet method, water content corrected clay content (%) by spectrophotometry, and organic matter content ($g{\cdot}kg^{-1}$), respectively. The regression coefficient for the equation was $r\;=\;0.984^{**}$, indicating highly significant correlation between the results of the two methods.

A Study on the Behavior Characteristics of Large Deep Foundations (대형 깊은 기초의 지지거동 특성에 관한 연구)

  • Park, Choon-Sik;Jung, Kwang-Min
    • Journal of the Korean Geosynthetics Society
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    • v.19 no.1
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    • pp.83-91
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    • 2020
  • In this study, the characteristics of support behavior according to the change of ground condition of the cast-in-place pile and the large Caisson foundation, which are increasingly used as foundations of large structures and bridges. the allowable bearing capacity calculated using the yield load analysis method was analyzed to calculate similar allowable bearing capacity for each method. In addition, the allowable bearing capacity calculated by the ultimate load analysis method was found to have a large difference in bearing capacity for each method. Through this point, it can be usefully used as an empirical formula for evaluating the settlement characteristics of piles in future design and construction. In addition, as a result of examining the ground force distribution during sedimentation of large caissons, the section of the weathered rock layer showed almost constant ground force distribution as ground forces decreased after yield occurred at the base corner. And in the bed rock layer section, the foundation's center was transformed into a ground force in the form of a convex downward due to an increase in the ground resistance of the central part. Using these results, the theory previously presented by Fang (1991) and Kőgler (1936) was proved.

The paleo-shoreline and formation age of the 1st marine terrace in Heunghae-eup Pohang City, South Korea : evaluation of the mode and rate of the late Quaternary tectonism (I) (포항시 흥해읍 일대 해안단구 제1면의 구정선 고도와 형성 시기 - 한반도 제4기 후기 지각운동의 양식과 변형률 산출을 위한 연구(I) -)

  • Shin, Jae Ryul;Park, Kyung Geun
    • Journal of the Korean association of regional geographers
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    • v.22 no.3
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    • pp.703-713
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    • 2016
  • This study documents the altitude of paleo-shoreline and formation age of the $1^{st}$ marine terrace emerged around Heunghae-eup Pohang City (South Korea). As a result, the $1^{st}$ terrace representing 10 m of the paleo-shoreline was formed at MIS 5c around 100,000 BP and was influenced repetitive sedimentation of sea-wave till regression of MIS 5a. The result is recognized as a definite truth for the $1^{st}$ terrace in the eastern coast of the Korean peninsula based on synthetic reviews of previous studies and cross-validation of absolute age data. Furthermore, this study deduces a sea stand at MIS 5c from the geomorphological contrast method, but precise determination of paleo-shoreline of the $2^{nd}$ terrace should be required to estimate that of MIS 5c.

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Geochemical Study of Black Shale in Uhangri Formation, Haenam Area (해남지역(海南地域)에 분포(分布)된 우항리층내(牛項里層內) 흑색(黑色)셰일의 유기지화학적(有機地化學的) 연구(硏究))

  • Lee, Dai Sung;Yun, Hyun Soo
    • Economic and Environmental Geology
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    • v.12 no.4
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    • pp.207-221
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    • 1979
  • The studied area occupies the southern part of Haenam peninsula located in the southwestern corner of Korea. The stratigraphic sequences of the area are grouped into following three units in ascending order. (1) Late Cretaceous sedimentary rocks of Uhangri Formation which consist of the alternative beds of black shales and tuffaceous sediments, Hwangsan acidic fine grained tuffs and Jindo rhyolite flows. (2) Late Cretaceous biotite granite and acidic porphyries which intruded the Late Cretaceous sedimentary rocks. (3) Tertiary(?) pitchstone. The study purposes to delineate any of geochemical aspects on the deposition of the sequences, the average amounts of organic materials and the effect to the maturation of hydrocarbonization which has been occured by the intrusives. Sixty nine black shale samples were collected from Uhangri Formation in the northern and southern coasts of the peninsula. Organic carbons, total extracted organic matters and hydrocarbons were mainly determined by the Soxhlet extraction method, together with C-H-N elemental analyses. Based on the field and laboratory studies, the following interpretations have been obtained. (1) The paleohydrostatic condition of the sedimentation which took place was relatively calm and stable to delineate a lacustrine environment. (2) The amounts of organic material were more or less constant throughout the period of the deposition of the sediments. (3) The degree of hydrocarbonization of the Uhangri Formation in the northern coast was taken place higher than that in the southern coast due to the differences of thermal effect by the biotite granite which is assumed to be as a heat source in the area. Among the northern coast, some black shales in Uhangri and Mogsam areas which had been under the most moderate temperature environment snow symptomatic oily material, whereas, those in Sinseongri area do not, which were presumably to be intensive thermal alteration by the later acidic porphyries.

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