• 한국기계연구소 소보
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• 통권9호
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• pp.83-93
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• 1982

The influence of different heat treatment conditions on microstructure, mechanical and fatigue properties of Spheroidal Graphite cast Iron with 0.4-0.6% Mn was investigated. 1) Maximum tensile strength was arrived by tempering at about $450^{\circ}C$after quenching. Tempering at higher than $600^{\circ}C$ was changed martensitic structure to ferritic structure and secondary graphites were precipitated. 2) The relationship between matrix hardness and total hardness of the specimens are as following. [HB]$T$=0.7[HB] [HB]$M$+35 Maximum tensile strength was arrived at the total hardness of HB400-450. 3) Endurance ratio decreases with increasing total hardness, and fatigue limits can be presumed from as following. $\sigmaf$=$\sigmat$

• Journal of Pharmaceutical Investigation
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• 제8권3호
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• pp.24-31
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• 1978

The relationship between temperature and apparent logarithmic hardness of ointments were clearly demonstrated. The followings were obtained as the results: 1. When the ointment base was mixed with additives and heated or cooled at various temperatures, the apparent logarithmic hardness in the first trend before reaching the critical point is subject to change mainly by the contents of the additive while in the secondary trend after reaching the critical point is subject to change mainly by the temperature. 2. No Change in the critical point was observed at different temperatures. It is assumed that the crittical point of such ointment bases has no relationship with temperatures and that the critical point itself should rather depend on the physicochemical properties of the additives.

• 대한금속재료학회지
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• 제46권8호
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• pp.477-481
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• 2008

The secondary hardening and fracture behavior in P/M high speed steels bearing V content of 9 to 10 wt% have been investigated in terms of austenitizing temperature and precipitation behavior. Austenitizing was conducted at 1,100 and $1,175^{\circ}C$ of relatively low and high temperatures. Coarse primary carbides retained after austenitization were mainly V-rich MC type. They give a significant influence on hardeness and toughness, as well as wear resistance. Tempering was performed in the range of $500{\sim}600^{\circ}C$. The peak hardness resulting from the precipitation of the fine MC secondary carbides was observed near 520, irrespective of austenitizing temperature. Aging acceleration(or deceleration) did not occur with increasing austenitizing temperature because it mainly influences contents of V and C of matrix through the dissloution of coarse primary MC containing lots of V and C. The precipitation of secondary MC carbides, which also contain V and C, did not change the aging kinetics itself. In the 10V alloy containing much higher C content, the impact toughness was lower than 9V alloy, because of the larger amount of primary carbide and high hardness.

• 동력기계공학회지
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• 제5권3호
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• pp.88-94
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• 2001

Stellite 12 alloy-powders were overlaid on 410 stainless steel valve seat using plasma transferred arc(PTA) process. Variation of the microstructure, hardness, wear and corrosion of overlaid deposit with current change was investigated. The deposit showed hypoeutectic microstructure, which was consisted of primary cobalt dendrite and networked $M_7C_3$ type eutectic carbides. As current increased, the amount of eutectic carbide decreased and its dendritic secondary arm spacing increased. Hardness of the deposit was decreased with increase of current. Stress relief heat treatment at $600^{\circ}C$ for two hours resulted in slight increase of hardness in the deposit and showed uniform hardness distribution in base metal without any hardened layer in HAZ. Specific wear decreased with increase of sliding distance. The deposit of high hardness with a lot of eutectic carbide showed relatively low specific wear. Initial corrosion current density of the deposit in 0.1N sulfuric acid was lower than those of 410 stainless steel, and showed a little variation with PTA current.

• 대한치과기공학회지
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• 제25권1호
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• pp.63-70
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• 2003

The microstructure and hardness of a porcelain fused Au-Pt-Cu-In alloy was investigated using optical microscopy, secondary electron microscopy, electron probe microanalyzer, transmission electron microscope, and vickers hardness. The hardness of the heat-treated Au-Pt-Cu-In quartenary alloy reached a maximum value in 30 min at 550$^{\circ}C$ in the range of 150 to 950$^{\circ}C$. In the aged Au-Pt-Cu-0.5In alloy at 550$^{\circ}C$, the hardness of the alloy rapidly increased until 30min with increasing aging time and after that it was remained nearly constant value. Based on above results, glazing and final aging of the porcelain fused Au-Pt-Cu-0.5In alloy were performed at 920 and 550$^{\circ}C$, respectively. The hardness of Au-Pt-Cu-0.5In alloy glazed at 920$^{\circ}C$ was 90 Hv and that of the alloy aged for 30 min at 550$^{\circ}C$ increased to 160 Hv. This indicates that a ceramic-metal crown with high strength can be manufactured using the glazing at 920$^{\circ}C$ and followed final aging at 550$^{\circ}C$ for 30 min.

• Korean Chemical Engineering Research
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• 제46권3호
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• pp.529-534
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• 2008

생체복합재료인 참굴 (Crassostrea gigas) 패각은 생성되는 형태에 따라 정상패각과 재생패각으로 구분되었다. 산과 알칼리를 이용한 탈 석회화과정 및 단백질제거반응을 통해 재생패각 내에서 얻어진 유기막이 키틴 특성을 가지고 있음을 FT-IR (Fourier transform infrared spectrometer)과 XRD (X-ray Diffractometer)를 통해 확인하였다. 불용성단백질의 함량은 정상패각이 재생패각과 비교하여 두배 이상 이었던 반면 수용성단백질 2차구조는 재생패각의 경우 random과 같은 불규칙구조가 많은 부분을 차지하고 있음을 확인할 수 있었다. 수용성단백질의 아미노산 조성과 단백질 2차구조분석을 통해 재생패각의 탄산칼슘 합성전략을 분자수준에서 논의하였고 재생패각 형성과 관련된 생광물화 전략이 패각의 재료학적 특성에 미치는 결과로써 해석되었다.

• 한국재료학회지
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• 제29권4호
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• pp.211-220
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• 2019

In this study, three kinds of bainitic steel plates are manufactured by varying the chemical compositions and their microstructures are analyzed. Tensile and Charpy impact tests are performed at room and low temperature to investigate the correlation between microstructure and mechanical properties. In addition, heat affected zone (HAZ) specimens are fabricated by a simulation of welding processes, and the HAZ microstructure is analyzed. The base steel that has the lowest carbon equivalent has the highest volume fraction of acicular ferrite and the lowest volume fraction of secondary phases, so the strength is the lowest and the elongation is the highest. The Mo steel has a higher volume fraction of granular bainite and more secondary phases than the base steel, so the strength is high and the elongation is low. The CrNi steel has the highest volume fraction of the secondary phases, so the strength is the highest and elongation is the lowest. The tensile properties of the steels, namely, strength and elongation, have a linear correlation with the volume fraction of secondary phases. The Mo steel has the lowest Charpy impact energy at $-80^{\circ}C$ because of coarse granular bainite. In the Base-HAZ and Mo-HAZ specimens, the hardness increases as the volume fraction of martensite-austenite constituents increases. In the CrNi-HAZ specimen, however, hardness increases as the volume fraction of martensite and bainitic ferrite increases.

• 한국주조공학회지
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• 제14권6호
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• pp.566-575
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• 1994

The effects of varying the pouring temperature and the die preheating temperature in producing centrifugally cast HP alloy modified with Nb was evaluated on the basis of the resultant macrostructure, microstructure and hardness of these castings. Increased die preheating temperatures and pouring temperatures resulted in an increase in the thickness of the columnar dendritic zone, the primary and secondary dendrite arm spacing and the thickness of the zone of porosity at the casting I.D.(inner diameter). Lower die preheating temperature and pouring temperatures result in increased grain fineness and an increased zone of equiaxed grains. A higher hardness was achieved toward the casting O.D.(outer diameter) compared to the casting I.D., attributable to alloy segregation toward the casting I.D. and segregation differences resulting from reduced solidification cooling rates toward the casting I.D. Also, a higher hardness was realized at the cold end of the casting attributed to a more uniform distribution of carbides.

• Restorative Dentistry and Endodontics
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• 제20권1호
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• pp.303-315
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• 1995

An adequate and homogeneous cure of light-activated restroative material is very important for improvement of marginal adaptation and prevention of marginal leakage, secondary caries and pulpal irritation as well as expressing natural physical property of that material. The purpose of this study was to evaluate the change of surface hardness and cure uniformity of light-activated glass ionomer cements. Restorative(Fuji II LC, Vitremer) and lining(Baseline VLC, Vitrebond) light-activated glass ionomer cements were investigated for this study. The surface hardness of the top and bottom surfaces and cure uniformity of each 1mm, 1.5mm, 2mm, 2.5mm & 3mm in the thickness of specimen were measured immediately, at 1 hour, 24 hours and 1 week after light activation. The surface hardness change and cure uniformity of all the specimens were measured by Knoop hardness tester. The results were as follows. 1. The surface hardness of top and bottom surfaces in all groups increased with time(p<0.01). 2. Both top and bottom surfaces hardness of Vitrebond group measured immediately after light-activation were significantly lower than those of the other groups(p<0.01). 3. The surface hardness of top and bottom surfaces of restorative light -activated glass ionomer cements was higher than those of lining materials at 1 week(p<0.10). 4. Surface hardness of Vitremer group decreased as the specimen thickness increased, except top and bottom surfaces hardness of the specimen at 1 week(p<0.01). There was no significant difference in the surface hardness of Fuji II LC with changes in the thickness except bottom surface hardness of specimen at 24 hours and 1 week (p>0.05). 5. Surface hardness of Vitrebond group significantly decreased as the specimen thickness increased(p<0.01). There was no significant difference in the surface hardness of Baseline VLC group with changes in the thickness except bottom surface hardness of specimen measured immediately after light -activation(p>0.05). 6. The hardness ratio of top against bottom surface in all groups decreased with time(p<0.05). 7. There was no significant difference in the hardness ratio of top against bottom surface with changes of the thickness except Vitrebond group, 24 hours and 1 week of Vitremer group and 1 week of Baseline VLC group (p>0.05). These results suggest that surface hardness of restorative ligh-activated glass ionomer cements were highter than those of lining light-activated materials. In all groups, the surface hardness and cure uniformity continuously increased with time.

• 한국재료학회지
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• 제25권9호
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• pp.497-502
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• 2015

The hardenability of boron steel specimens with different molybdenum and chromium contents was investigated using dilatometry and microstructural observations, and then was quantitatively measured at a critical cooling rate corresponding to 90 % martensite hardness obtained from a hardness distribution plotted as a function of cooling rate. Based on the results, the effect of an austenitizing temperature on the hardenability and tensile properties was discussed in terms of segregation and precipitation behavior of boron atoms at austenite grain boundaries. The molybdenum addition completely suppressed the formation of pro-eutectoid ferrite even at the slowest cooling rate of $0.2^{\circ}C/s$, while the chromium addition did at the cooling rates above $3^{\circ}C/s$. On the other hand, the hardenability of the molybdenum-added boron steel specimens decreased with an increasing austenitizing temperature. This is associated with the preferred precipitation of boron atoms since a considerable number of boron atoms could be concentrated along austenite grain boundaries by a non-equilibrium segregation mechanism. The secondary ion mass spectroscopy results showed that boron atoms were mostly segregated at austenite grain boundaries without noticeable precipitation at higher austenitization temperatures, while they formed as precipitates at lower austenitization temperatures, particularly in the molybdenum-added boron steel specimens.