• Journal of the Korean Society for Nondestructive Testing
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• v.29 no.6
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• pp.534-549
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• 2009

As the thin film technology has emerged in various fields, adhesion of the film interface becomes an important issue in terms of the longevity and durability of thin film devices. Diverse nondestructive methods utilizing acoustic techniques have been developed to assess the interfacial integrity. As an effective technique based on the ultrasonic wave focusing and the surface acoustic wave(SAW) generation, scanning acoustic microscopy(SAM) has been investigated for adhesion evaluation. Visualization of film microstructures and quantification of adhesion weakness levels by SAW dispersion are the recent achievements of SAM. To overcome the limitations in the theoretical dispersion model only suitable for perfectly elastic and isotropic materials, a new model has been more recently developed in consideration of film anisotropy and viscoelasticity and applied to the adhesion evaluation of polymeric films fabricated on semiconductive wafers.

• Proceedings of the KIEE Conference
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• 2004.07c
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• pp.1667-1669
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• 2004

In this paper, the elastic epoxy added elastomer having viscoelasticity to existing epoxy was measured thermal, structural properties by DSC (Differential Scanning Calorimetry) and FESEM (Field Emission Scanning Electron Microscope). Specimens were made of dumbbell forms by the ratio of 5, 10, 15, and 20[phr] by regulation with elastomer contents. The measurement temperature dimensions of DSC were -20[$^{\circ}C$] to 150[$^{\circ}C$] and rising temperature was 4[$^{\circ}C$/min]. Also we observed structure through FESEM at the magnification of 1000 times with the voltage of 15[kV] after breaking by quenching specimens. As experimental results, we could know that thermal and structural properties were improved quantity according to decrease of elastomer contents. Namely, it increased glass transition temperature, high temperature, and matrix structure. In general, thermal, structural properties of 15[phr] was excellent among the specimens.

• Macromolecular Research
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• v.15 no.2
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• pp.109-113
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• 2007

The surface molecular motion of monodisperse polystyrene (PS) films was examined using scanning vis-coelasticity microscopy (SVM) in conjunction with lateral force microscopy (LFM). The dynamic storage modulus, E', and loss tangent, $tan\delta$, at a PS film surface with number-average molecular weights, $M_n$, smaller than 30 k were found to be smaller and larger than those for the bulk sample, even at room temperature, meaning that the PS surface is in a glass-rubber transition or fully rubbery sate at this temperature when the $M_n$ is small. In order to quantitatively elucidate the dynamics of the molecular motion at the PS surface, SVM and LFM measurements were performed at various temperatures. The glass transition temperature, $T_g$, at the surface was found to be markedly lower than the bulk $T_g$, and this discrepancy between the surface and bulk became larger with decreasing $M_n$. Such an intensive activation of the thermal molecular motion at the PS surfaces can be explained in terms of an excess free volume in the vicinity of the film surface induced by the preferential segregation of the chain end groups.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2005.05a
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• pp.307-312
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• 2005

As the various manufacturing technology of optical glass is developed, the aspherical lenses are applied to many fields. However, It is still very difficult to manufacture glass lens because of the high cost and the short life of core. In recent years, the demands of the aspherical glass lenses increase since it is difficult to obtain the desirable performance in the plastic lens. In the glass mold lens, it has merits of high productivity and reproductivity since lens is manufactured by the only forming with high precision mold. The fabricating conditions for glass mold lens are glass surface that does not cause fusion, viscosity of 108-1013 poise for the $0.2{\mu}m$ accuracy, and viscoelasticity for the roughness less than 100 angstrom. In this thesis, ultra-precision grinding characteristics of tungsten carbide for forming the aspherical glass lens core were studied and the result of it is applied to manufacture the tungsten carbide-base core of the glass lens used to the laser scanning unit and the camera phone.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1737-1740
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• 2005

As the various manufacturing technology of optical glass is developed, the aspherical lenses are applied to many fields. However, It is still very difficult to manufacture glass lens because of the high cost and the short life of core. In recent years, the demands of the aspherical glass lenses increase since it is difficult to obtain the desirable performance in the plastic lens. In the glass mold lens, it has merits of high productivity and reproductivity since lens is manufactured by the only forming with high precision mold. The fabricating conditions for glass mold lens are glass surface that does not cause fusion, viscosity of 108-1013 poise for the $0.2{\mu}m$ accuracy, and viscoelasticity for the roughness less than 100 angstrom. In this thesis, ultra-precision grinding characteristics of tungsten carbide for forming the aspherical glass lens core were studied and the result of it is applied to manufacture the tungsten carbide-base core of the glass lens used to the laser scanning unit and the camera phone.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1910-1913
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• 2005

As the various manufacturing technology of optical glass is developed, the aspherical lenses are applied to many fields. However, It is still very difficult to manufacture glass lens because of the high cost and the short life of core. In recent years, the demands of the aspherical glass lenses increase since it is difficult to obtain the desirable performance in the plastic lens. In the glass mold lens, it has merits of high productivity and reproductivity since lens is manufactured by the only forming with high precision mold. The fabricating conditions for glass mold lens are glass surface that does not cause fusion, viscosity of 108-1013 poise for the $0.2{\mu}m$ accuracy, and viscoelasticity for the roughness less than 100 angstrom. In this paper, ultra-precision grinding characteristics of tungsten carbide for forming the aspherical glass lens core were studied and the result of it is applied to manufacture the tungsten carbide-base cores of the glass lens used to the laser scanning unit and the camera phone.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.07a
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• pp.461-464
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• 2004

In this paper, the elastic epoxy added elastomer having viscoelasticity to existing epoxy was measured thermal, structural properties through TGA(Thermogravimetric Analysis) and FESEM(Field Emission Scanning Electron Microscope). Specimens were made of dumbbell forms by the ratio of 5[phr], 10[phr], 15[phr], and 20[phr] by regulation with elastomer contents. The measurement temperature dimensions of TGA were $0[^{\circ}C]\;to\;800[^{\circ}C]$, and rising temperature was $5[^{\circ}C/min]$. And we observed structure through FESEM at the magnification of 1000times with the voltage of 15[kV] after breaking by quenching specimens. As thermal analysis results, we could know that thermal and structural properties was improved quantity according to decrease of elastomer contents. In general, thermal, structural properties of 15[phr] was excellent among the specimens.

• Journal of the Society of Cosmetic Scientists of Korea
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• v.25 no.4 s.34
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• pp.123-131
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• 1999

Liquid crystal known as a rheological barrier to coalescence of oil droplets, increases emulsion stability, water-holding capacity and promotes active material penetration to skin. Some investigation for its rheological characteristics have been reported but its relations to consumer perception have been rarely published. In this study, oil/water emulsion and oil/liquid crystal/water systems were manufactured using the same composition or Behenyltrimethylammonium chloride/Cetostearyl alcohol/Lanolin oil. and rheological properties or each system were investigated with Cone and Plate rheometer. The formation of liquid crystalline phase was observed with polarized microscope and Differential Scanning Calorimeter. Continuous shear experiment, creep, yield and water holding capacity were measured for oil/water and oil/liquid crystal/water systems. The results were compared with sensory evaluations. Oil/liquid crystal/water system showed higher,viscosity at the same shear rate. higher viscoelasticity and higher yield stress than oil/water system. These properties were expected to show good spreadability and excellent richness without waxiness in hair can: products of creme type. This expectation was consistent with the results of sensory experiments. Water-holding capacity was evaluated by measuring residual water of specimens at specific temperature and relative humidity. Oil/liquid crystal/water system was proved to have higher ability to hold water in comparison with oil/water system. The results indicated that oil/liquid crystal/water system was of benefit to rheological properties creme type hair care products.

• Journal of Fashion Business
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• v.17 no.6
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• pp.28-43
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• 2013

Recent trends toward the collaborations among various sectors of academia and research areas have brought interests and significances in new activities especially in the fashion and textile areas. One of the collaboration examples is the recent research projects on 3D virtual clothing systems based on the 3D CAD software. The 3D virtual clothing systems provide simulated apparels with high degrees of fidelity in terms of color, texture, and structural details. However, since real fabrics exhibit strong nonlinearity, anisotropy, viscoelasticity, and hysteresis, the 3D virtual clothing systems need fine tuning parameters for the simulation process. In this study, characteristics of silk fabrics, which are woven by using degummed silk and raw silk yarns, are being analyzed and compared. Anisotropic properties may be measured as warp and filling direction properties separately in woven fabrics, such as warp tensile stress or filling bending rigidity. Hysteretic properties may be measured as bending hysteresis or shear hysteresis by using KES measurements. These data provide deformation-force relationships of the fabric specimen. Three-dimensional effects obtained when using these characteristic fabrics are also analyzed. The methods to control the three-dimensional appearance of the sewn fabric specimens when utilizing a programmable microprocessor-based motor device, as prepared in this study, are presented. Based on the physical and mechanical properties measured when using the KES equipment, the property parameters are being into a 3-dimensional virtual digital clothing system, in order to generate a virtual clothing product based on the measured silk fabric properties.

• Applied Chemistry for Engineering
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• v.24 no.1
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• pp.104-111
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• 2013

Poymer blends of two degradable aliphatic polyesters, relatively expensive material polylactic acid (PLA) and relatively inexpensive material poly(butylene adipate-co-terephthalate) (PBAT), were used in this study. Three different kinds of modifiers were used with various amounts. Diisocyanate type methylenediphenyl 4,4'-diisocyanate (MDI) and hexamethylene diisocyanate (HDI) were used as modifiers and epoxy type coupling agents also used. The melt flow index (MFI) and dynamic viscoelasticity of various compositions of PLA/PBAT blends were studied. The mechanical property and morphology with respect to the fracture surface of PLA/PBAT blends were also investigated using tensile test and field emission scanning electronic microscopy, respectively. These tests were also used to verify the compatibility of PLA/PBAT and the effect of mechanical properties due to the use of modifiers. Tensile properties of PLA/PBAT blends modified with HDI were improved remarkably.