• Title/Summary/Keyword: sample injection method

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Study on the Coefficient of Consolidation of Marine Clay by Rowecell Consolidation Test (ROWECELL시험에 의한 해성점토의 압밀계수에 대한 연구)

  • 김종국;차영일;김혁기;김영웅
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.725-732
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    • 2003
  • It was achieved that Rowecell test for this undisturbed sample was picked by Block sampler($\phi$:250mm, L:500mm) and hydraulic piston sampler($\phi$:76mm, L:850mm) in the marine clay of YONGYUDO and YEONGJONGDO in this research. Ratio of coefficient of consolidation was analyzed through comparison with C$\_$h/ by CPTu and C$\_$v/ and C$\_$h/ by existent consolidation test. According to analysis, coefficient of consolidation of block sample is fairly greater than coefficient of consolidation of piston sample. And the bigger diameter of undisturbed sample, sample disturbance could know decreasing. Coefficient of consolidation by Rowecell test measured more greatly than coefficient of consolidation by existent consolidation test. Rowecell test could know decreasing consolidation rate because of smear effect by Mandrel injection. Also, C$\_$h/ by CPTu shows deviation by each analysis method, selection of suitable analysis method judged by important leading in the coefficient of consolidation.

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Effects of Coptidis Rhizoma on the Change of Interleukin-6 and $TNF-{\alpha}$ Level induced by LPS I.C.V. Injection in Mice (황연(黃連)이 Lipopolysaccharide 뇌실 주입으로 유발된 생쥐의 IL-6와 $TNF-{\alpha}$ 변화에 미치는 영향)

  • Sim Eun-Yeong;Yun Jeong-Moon;Lee Tae-Hee
    • Herbal Formula Science
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    • v.12 no.1
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    • pp.209-223
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    • 2004
  • Objective: This study was conducted to investigate the effects of Coptidis Rhizoma on the plasma IL-6 and $TNF-{\alpha}$ level in mice by intracerebroventricular(I.C.V.) injection of Lipopolysaccharide (LPS). Method: 6 mice were assigned to each of the Normal group, the Control group, and the individual Experimental groups. In the Normal group only saline was administered intragastrically, and in the Control group LPS was injected intracerebroventricularly 1 hr after intragastric administration of saline. In the Experimental groups Coptidis Rhizoma(0.5g/kg, 1.0g/kg, 3.0g/kg) was administered intragastrically to mice 1 hr prior to LPS (100ng/mouse) I.C.V. Injection. To measure the plasma IL-6 and $TNF-{\alpha}$ level of mice, their blood samples were collected from retro-orbital venous plexus, immediately centrifuged at $4^{\circ}C$, and plasma was removed and stored frozen at $-83^{\circ}C$ for later determination of plasma IL-6 and $TNF-{\alpha}$. Result: 1. LPS I.C.V. Injection increased plasma IL-6 level significantly in a dose-dependent manner compared with Normal group. (P<0.01) The plasma IL-6 concentration reached a significant maximal level about 1 hr after LPS(100ng/mouse) I.C.V. Injection.(P<0.001) 2. Both the 0.5g/kg(Sample A) and 1.0g/kg(Sample B) groups to which Coptidis Rhizoma was administered intragastrically 1 hr prior to LPS(100ng/mouse) I.C.V. Injection showed insignificant lower plama IL-6 level in 1 hr than Control group(P>0.05), and 3.0g/kg group(Sample C) conversely showed higher plama IL-6 level than Control group. 3. LPS I.C.V. Injection increased plasma $TNF-{\alpha}$ level significantly in a dose-dependent manner compared with Normal group.(P<0.05) The plasma $TNF-{\alpha}$ concentration reached a significant maximal level about 1 hr after LPS(100ng/mouse) I.C.V. Injection.(P<0.001) 4. All Sample groups(0.5g/kg, 1.0g/kg, and 3.0g/kg) to which Coptidis Rhizoma was administered intragastrically with each constituent-dose 1 hr prior to LPS(100ng/mouse) I.C.V. Injection showed significant lower $TNF-{\alpha}$ plama level in 1 hr than Control group.(P<0.001) These data revealed that Coptidis Rhizoma might have anti inflammatory effect by reducing the plasma $TNF-{\alpha}$ level in a dose dependent manner in mice LPS I.C.V. Injection.

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Microquantitative Analysis of Quercetin by Gas Chromatography (Gas Chromatography법에 의한 Quercetin의 미량분석에 관한 연구)

  • 이숙연;김성경
    • YAKHAK HOEJI
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    • v.26 no.2
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    • pp.117-121
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    • 1982
  • This investigation was intended to develope the quantitative gas liquid chromatographic method for quercetin. The method involves derivatization of the sample with trimethylsilylimidazole containing cholesterol as an internal standard and injection into a gas chromatograph with 3% OV-17 column. The calibration curve for the quercetin was linear over a sample in the range of 4-16.mu.g. The minimum detectable amount using FID in $1.6{\times}10^{-10}$ a.f.s. was determined to be $6.64{\times}10^{-10}mol$.

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Simulation of injection-compression molding for thin and large battery housing

  • Kwon, Young Il;Lim, Eunju;Song, Young Seok
    • Current Applied Physics
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    • v.18 no.11
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    • pp.1451-1457
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    • 2018
  • Injection compression molding (ICM) is an advantageous processing method for producing thin and large polymeric parts in a robust manner. In the current study, we employed the ICM process for an energy-related application, i.e., thin and large polymeric battery case. A mold for manufacturing the battery case was fabricated using injection molding. The filling behavior of molten polymer in the mold cavity was investigated experimentally. To provide an in-depth understanding of the ICM process, ICM and normal injection molding processes were compared numerically. It was found that the ICM had a relatively low filling pressure, which resulted in reduced shrinkage and warpage of the final products. Effect of the parting line gap on the ICM characteristics, such as filling pressure, clamping force, filling time, volumetric shrinkage, and warpage, was analyzed via numerical simulation. The smaller gap in the ICM parting line led to the better dimensional stability in the finished product. The ICM sample using a 0.1 mm gap showed a 76% reduction in the dimensional deflection compared with the normal injection molded part.

Determination of Aqueous Ammonia with Indophenol Method : Comparision and Evaluation for the Reaction-Rate, Equilibrium and Flow-Injection Analysis Methods (인도페놀법을 이용한 수용액 중 암모니아 정량에 관한 연구 : 평형법, 반응속도법, 흐름주입분석법의 비교와 평가)

  • 정형근;김범식
    • Journal of Environmental Science International
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    • v.4 no.1
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    • pp.91-103
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    • 1995
  • The reaction rate, equilibrium, and flow injection analysis methods were fundamentally evaluated for the determination of aqueous ammonia. The selected indophenol blue method was based on the formation of indophenol blue in which ammonium ion reacted with hypochlorite and phenol in alkaline solution. In the optimized reaction condition, the reaction followed 1st order reaction kinetics and the final product was stable. The absorbance measurements before and after the equilibrium were utilized for the reaction rate and equilibrium methods. The reaction rate methods, based on the relative analytical signals for the possibility of eliminating interferents, were shown to have good linear calibration curves but the detection limit and the calibration sensitivity were poorer than those in the equilibrium method. The detection limits were 32-49 pub and 24 pub for the reaction rate and equilibrium methods, respectively In the flow injection analysis, the absorbance was measured before the equilibrium reached and thus resulted in 30% reduction of calibration sensitivity. However, the detection limit was 11 ppb, indicating that the peak-to-peak noise for the blank was remarkably improved. Compared to the manual methods, the optimized experimental condition in a closed reaction system reduced the blank absorbance and the inclusion of ammonia from the atmosphere was prevented. In addition, highly reproducible mixing of sample and reagents and analytical data extracted from continuous recording showed excellent reproducibility.

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High Brightness Prism Light-guide Plate for TFT-LCDs Using Optical Simulation and Novel Injection Mold Process (광학시뮬레이션과 새로운 사출성형법을 사용한 TFT-LCD용 고휘도 프리즘 도광판)

  • Han, Jeong-Min;Shon, Jin-Geun
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.61 no.2
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    • pp.93-96
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    • 2012
  • We have designed high performance prism light-guide plate (LGP) in 17 inch TFT-LCD. In test result to embody high brightness BLU in case of LGP of base and upper surface with 17 inch, thickness 8mm adding prism construct. Using optical simulation, we forecast the brightness and uniformity in LGP with prism structure. And we adopted novel injection mold method and Nickel stamper to make actual evolution sample. Novel injection mold process has steady heating time zone in heat cycle time of injection mold process. For this novel heat cycle control, we achieved above 90[%] height prism structure as our design. It is superior brightness improvement than previous that of printing form about some 20[%] and in this course to embody actual material it succeeded prism LGP production by 17 inch injection form process.

Indirect Determination of Nitrite by Flame Atomic Absorption Spectrometry Using a Lead(IV) Dioxide Oxidant Microcolumn

  • Noroozifar, Meissam;Khorasani Motlagh, Mozhgan;Taheri, Aboozar;Homayoonfard, Marjan
    • Bulletin of the Korean Chemical Society
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    • v.27 no.6
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    • pp.875-880
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    • 2006
  • A new, simple and fast flow injection analysis (FIA) method has been developed for the indirect determination of nitrite. The proposed indirect automatic method is based on the oxidation of nitrite to nitrate using a lead(IV) dioxide oxidant microcolumn where the flow of the sample through the microcolumn reduces the $PbO_2$ solid phase reagent to Pb(II), which is measured by flame atomic absorption spectrometry. The absorbance of Pb(II) are proportional to the concentration of nitrite in the samples. The calibration curve was linear up to 30 mg $L ^{-1}$, with a detection limit of 0.11 mg $L ^{-1}$ for a 400 mL injected sample volume and a sampling rate of about 80 $h ^{-1}$. The results exhibit no interference from the presence of large amounts of ions. The developed procedure was found to be suitable for the determination of nitrite in foodstuffs and wastewaters. A relative standard deviation better than 0.9% was obtained in a repeatability study. The reliability of the method was established by parallel determination against the standard method.

Emission Characteristics of Nano-sized Particles in Bio-ethanol Fuelled Engine with Different Injection Type (바이오-에탄올연료 및 분사방식에 따른 엔진 나노입자 배출 특성)

  • Lee, Jin-Wook;Patel, Rishin;Ladommatos, Nicos
    • Transactions of the Korean Society of Automotive Engineers
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    • v.17 no.4
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    • pp.55-62
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    • 2009
  • As an experiment investigation, the effects of ethanol blended gasoline fuel with different injection method on nano-sized particle emission characteristics were examined in a 0.5L spark-ignited single-cylinder engine with a compression ratio of 10. Because this engine nano-particles are currently attracting interest due to its adverse health effects and their impact on the environments. So a pure gasoline and an ethanol blended gasoline fuels, namely E85 fuel, used for this study. And, as a particle measuring instrument, a fast-response particle spectrometer (DMS 500) with heated sample line was used for continuous measurement of the particle size and number distribution in the size range of 5 to 1000nm (aerodynamic diameter). As this research results, we found that the effect of ethanol blending gasoline caused drastic decrease of nano-particle emissions when port fuel injection was used for making better air-fuel mixture than direct fuel injection. Also injection timing, specially direct fuel injection, could be a dominant factor in controlling the exhaust particle emissions.

Effects of Synthesis Method, Melamine Content and GPC Parameter on the Molecular Weight of Melamine-Urea-Formaldehyde Resins

  • KIM, Minjeong;PARK, Byung-Dae
    • Journal of the Korean Wood Science and Technology
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    • v.49 no.1
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    • pp.1-13
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    • 2021
  • This study was conducted to investigate the effects of the synthesis method, melamine content, and GPC parameters (such as flow rate, column-detector temperature, and sample injection temperature) on the molecular weight of melamine-urea-formaldehyde (MUF) resins. Two different synthesis methods were employed. In the first method, MUF-A resins were synthesized by simultaneously reacting urea, formaldehyde, and melamine (5%, 10%, and 20%) using the reaction of alkaline-acid-alkaline steps under controlled temperature and viscosity. In the second method, MUF-B resins were synthesized by first reacting melamine at the same levels with formaldehyde and then by adding urea. The highest weight average molecular weight (Mw) of MUF-A resins was found at 10% melamine content when the flow rate was 0.3 and 0.8 ml/min; Mw decreased slightly at 20% melamine content. The results showed that Mw increased with an increase in the melamine content when the flow rate was 0.5 and 1.0 ml/min. In addition, Mw was the highest when the flow rate, column-detector temperature, and injection temperature were 0.3 ml/min, 50℃, and 25℃, respectively. On the contrary, MUF-B resins had greater Mw and number average molecular weight (Mn) than MUF-A resins. Overall, Mw and Mn increased as the melamine content increased. The optimal GPC parameter for MUF resins was determined as follows: a flow rate of 0.5 ml/min, a column-detector temperature of 50℃, and a sample injection temperature of 50℃.

A study to identify an occupational hazards for hospital working health care providers from needle stick injury as an occupational hazards of health care providers in hospital and prevention (의료요원의 주사바늘 상해 실태와 예방대책을 위한 일 연구)

  • Han, Jung-Suk;Kang, Kyu-Sook;Kim, Hea-Sook
    • The Korean Nurse
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    • v.34 no.2
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    • pp.45-57
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    • 1995
  • A study .to identify an occupational hazards for hospital working health care providers from needle stick injury as an occupational hazards of health care providers in hospital and prevention A survey of 2430 health professionals (2184 nurses, 182 doctors, and 64 Lab technicians) was conducted to describe and provide information about 1) the experience of needle stick. 2) the number of needle stick, 3) the treatment after needle stick. 3) the situation of needle stick, 4) the report of needle stick, 5) the cause of needle stick, 6) the discard method of used needles, and 7) how to worry about getting infection disease after needle stick. Data were collected using questionnarires constructed by the authors and tested by a pilot study. Results of the study showed that 96.7% of the sample had an experience of needle stick (96.8% of the nurses, 96.7% of the doctors, and 92.2% of Lab technicians). Seventy seven percent of the sample experienced less than 10 needle sticks, 19% of the sample experienced 11 to 20 needle sticks, and the rest of the sample experienced more than 20 needle sticks. The situations where needle sticks occurred include intrvenous injection (36.5%), intramuscular injection (21.6%), blood withdraw (17.8%), and preparation(11.8%). The study showed that needle sticks (67.5%) usually occurred after client treatment. Health professionals used recapping method (55%) after they used needles. Needle sticks were predominantly caused by the carelessness of health professionals (61%), After needle sticks, 88.2% of the sample subjects treated needle sticks using disinfection technique by themselves. Most of health professionals (92.6%) did not report the accident. and 95.6% of them did not receive any test or further treatment. After needle sticks, 87.8% of nurses, 83.6% of doctors, and 96.6% of lab technicians worried about hepatitis infection. 'Health professionals also worried about AIDS infection, tetanus, venereal infection, and skin injury. These findings suggest that health professionals are at high-risk of needle stick and fail to report needle stick accidents. They should pay more attention to needle stick in order to avoid unwanted infection.

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