• 제목/요약/키워드: salt spray

검색결과 232건 처리시간 0.027초

분무 건조된 W-Co 복합염의 열분해 및 분말 특성에 관한 연구 (A Study On Properties and Thermal Decomposition of W-Co Salt Powders Synthesized by Spray Drying)

  • 권대환;안인섭;하국현;김병기;김유영
    • 한국재료학회지
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    • 제11권11호
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    • pp.953-959
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    • 2001
  • Homogeneous spherical W-Co salt powders were made by spray drying of aqueous solution of ammonium $metatungstate(NH_4)_6(H_2W_{12}O_{40}){\cdot}4H_2O,\; AMT)$ and cobalt nitrate $hexahydrate(Co(NO_3)_2{\cdot}6H_2O)$. The thermal decomposition process of spray dried W-Co salt powders was studied by TG, XRD, SEM, TEM and FT-IR. Spray dried W-Co salt powders were calcined for 1 hour in the temperature from$ 350^{\circ}C$ to $800^{\circ}C$ in atmosphere of air. At the temperatures over $600^{\circ}C$, spherical $CoWO_4/WO_3$ composite oxide powders were obtained. The primary particle size of W/Co composite oxide powders increased with increasing thermal decomposition temperature due to the particle growth. The observed crystallite size by TEM was in the range of 60nm and that of $CoWO_4$ calculated by Scherrer's formula at $800^{\circ}C$ was smaller than 55nm. The crystallite site was identified by XRD and TEM.

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Zr기 비정질 합금 다이캐스팅 주조품의 부식 특성에 미치는 블라스팅 처리의 영향 (The Effect of Blasting Treatment on the Corrosion Characteristics in the Zr-based Amorphous Alloy Die Castings)

  • 이병철;김성규;박봉규;배차헌;박흥일
    • 한국주조공학회지
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    • 제34권2호
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    • pp.60-66
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    • 2014
  • A Zr-based amorphous alloy specimen was produced by vacuum die casting process. The salt spray test was carried out using the specimens in the as-cast, $Al_2O_3$ and $ZrO_2$ particle blasted state. Using these specimens, the SEM-EDX and XRD analyses, DSC measurement and bending strength test were conducted. After the salt spray test, the specimens were not experienced phase change and thermal characteristics of the alloys were remained unchanged. In the as-cast specimen, corrosion products were not observed. However, in the $Al_2O_3$ particle blasted specimen, pitting corrosion occurred and the detected corrosion products were $ZrCl_2$ and $NaZrO_3$. Due to the salt spray test, bending strength of the $Al_2O_3$ blasted specimens showed about 100 MPa lower strength than the other specimens. The bending fracture surface was vein pattern which was shown typically in the amorphous alloys.

전조 후 Zn-Ni 전기도금한 강 볼트의 염수분무 특성에 관한 연구 (A Study on the Characteristics of Salt Spray Test of Roll Formed and Zn-Ni Electrodeposited Steel Bolts)

  • 보보무로드;손요헌;김인수
    • 소성∙가공
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    • 제21권5호
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    • pp.330-335
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    • 2012
  • Roll formed steel bolts are electrodeposited with Zn-Ni to protect themselves from corrosion. However, white storage stain or white rust(corrosion) is found on Zn-Ni electrodeposited surface of steel bolts when they are exposed to moisture. In this paper a new process is introduced to protect Zn-Ni electrodeposited steel bolt from white storage stain or white rust for a long time under the salt spray test and high humidity test conditions. The better corrosion resistance could be gotten by the additional process of Ni-P electroless deposition and heat treatment to conventional manufacturing method of Zn-Ni coated steel bolt. The corrosion resistance of Zn-Al powder slurry coated steel bolt showed better than that of Zn-Ni electrodeposited one.

옥외용 고분자 전기절연재료의 염수 및 UV조사에 의한 열화 특성 (The Aging Characteristics of Polymer Electrical Insulation Materials bv UV Radiation and Salt Water Spray)

  • 최남호;한상일;한상옥;박강식;김종석;박양범
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1997년도 추계학술대회 논문집
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    • pp.221-224
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    • 1997
  • In this study we investigated the acting characteristics of Polymers for electrical insulation by UV radiation and salt water spray treatment. We used the Polymers such as EPDM, SR. PTFE. EVA. We measured contact angle and surface resistance to know the aging characteristic of Polymer surface. And we use SEM to observe the change of the surface shape. Dry flashover voltage test impulse voltage test were carried for the polymer insulator(EVA) . Through this experiment and the analysis we could know the polymers have a good resistance to weathering conditions like as salt spray UV irradiation and mix of them. And we can compare the aging characteristics between Polymers. As a result, we could know that the surface characteristics of PTFE is better than the other. And the degree, electrical characteristics is affected by change of surface shape is not big.

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Deposition and Characterization of Electrophoretic Paint on AZ31 Magnesium Alloy

  • Nguyen, Van Phuong;Moon, Sungmo
    • 한국표면공학회지
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    • 제49권2호
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    • pp.141-146
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    • 2016
  • In this study, electrophoretic paint (E-paint) was deposited on the knife-abraded surface of AZ31 magnesium alloy (AZ31), and its adhesion and corrosion resistance were examined by tape peel-test and salt spray test, respectively. E-paint started to deposit on AZ31 Mg alloy after an inductance time and pores were found in the E-paint layer which is ascribed to hydrogen bubbles generated on the surface during the painting process. The pores disappeared after curing for 15 min at $160^{\circ}C$. The E-paint on AZ31 exhibited good adhesion after immersion in deionized water for 500 h at $40^{\circ}C$. The E-paint sample without scratch showed no corrosion after 1500 h of salt spray test. However, on the scratched sample, blisters were visible adjacent to the scratched sites after 500 h of salt spray test.

해양심층수 기능성소금 제조를 위한 분무건조기 특성의 수치해석적 연구 (A Numerical Study on the Spray Dryer Characteristic for Manufacture of Deep Sea Water Salt)

  • 김현주;신필권;박성제
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2003년도 추계학술대회 논문집
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    • pp.24-29
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    • 2003
  • Deep sea water has cold temperature, abundant nutrients and minerals, and good water quality that is pathogen-free and stable. Compared with surface water, deep sea water contains more nutrition salt, such as nitrogen and phosphor. Moreover, if has the good balance of minerals. Because of the ability of the spray drying process to produce a free-flowing power considering of spherical particles with a well-defined size distribution and the rapid drying times for heat-sensitive material, spray drying is attractive for a wide range of applications spray drying is a unique unit operation in which powders are produced from a liquid feed in a single processing step. Key component of the process are atomizer, spray chamber. Design of spray chamber should be based on the atomizer type, the production rate, and the particle size required. Because of the complex processes taking place during spray drying, traditional design method are based on pilot-plant tests and empirical scale-up rules. Modern technique such as CFD have a role to play in design and troubleshooting.

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여러 종류의 소금으로 제조한 새우젓의 이화학적 특성 및 관능적 특성 (Physicochemical and Sensory Properties of Salt-Fermented Shrimp Prepared with Various Salts)

  • 이강덕;최차란;조정용;김학렬;함경식
    • 한국식품영양과학회지
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    • 제37권1호
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    • pp.53-59
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    • 2008
  • 본 연구는 여러 종류의 소금(한국산 천일염, 정제염, 함초 해수농축염, 함초 스프레이 천일염, 해수농축염, 분무건조염)을 사용하여 제조한 새우젓의 발효과정 중 이화학적 및 관능적 특성에 대하여 조사하였다. 발효 60일까지는 분무건조염으로 제조한 새우젓의 암모니아태 질소의 함량이 다른 소금에 비하여 낮은 값을 보였으며 아미노태 질소 역시 발효기간 동안 낮은 값을 나타내었다. 발효 90일에는 함초 성분이 포함된 소금으로 제조한 새우젓의 아미노태 질소 값이 약 980 mg%로 가장 높았고 분무건조염은 680 mg%로 가장 낮아 소금 종류에 따른 차이를 보였다. 그러나 아미노태 질소는 발효가 진행됨에 따라 그 차이가 감소하였다. VBN은 발효 14일부터 60일까지 분무건조염으로 제조한 새우젓이 다른 시료에 비해 낮은 값을 보였으며 TMA는 발효 180일 후 정제염이 가장 높은 값을 나타내어 소금의 종류에 따라 근소한 차이를 보였다. 180일 동안 발효시킨 새우젓을 대상으로 실시한 관능평가의 결과 짠맛, 전체적인 맛, 전체적인 기호도 등에서 시료 간에 유의적인 차이가 나타났고, 천일염 및 가공염으로 제조한 새우젓이 전체적인 기호도에서 정제염으로 제조한 새우젓에 비해 높게 평가되었다.

동복알루미늄의 내염특성 연구 (Study on Salt-Proof Characteristics of Copper Clad Aluminum)

  • 김진사;배덕권
    • 전기학회논문지
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    • 제58권9호
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    • pp.1764-1768
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    • 2009
  • As the demand of electric power is increasing rapidly, the need of the compact and light electric power device is also increased. Copper clad aluminum (CCA) is newly proposed electrical conductor, because of its light-weight and low-cost characteristics, to replace the existing conductor made of copper. This paper presents the salt-proof characteristics of the copper clad aluminum (CCA) to certificate long time safe operation of the newly proposed electrical conductor. The two types of the CCA conductor were tested in the neutral salt spray tester. The experimental results of two types of the CCA with salt spray were presented in this paper. The results comprise resistance measured data, micro picture of the selected surface, and component measured data according to the elapsed time. The period of the experiment was 1,000 hours. There was no evidence to show the corrosion of CCA during the whole period of the experiments.

실링이 플라즈마 스프레이 코팅된 알루미나 코팅재의 내부식성에 미치는 영향 (Effect of Sealing on the Corrosion Resistance of Plasma-Sprayed Alumina Coatings)

  • 권의표;김세웅;이종권
    • 한국재료학회지
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    • 제32권10호
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    • pp.442-447
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    • 2022
  • Sealing treatment is a post-surface treatment of the plasma spray coating process to improve the corrosion resistance of the coating material. In this study, the effect of the sealing on the corrosion resistance and adhesive strength of the plasma spray-coated alumina coatings was analyzed. For sealing, an epoxy resin was applied to the surface of the coated specimen using a brush. The coated specimen was subjected to a salt spray test for up to 48 hours and microstructural analysis revealed that corrosion in the coating layer/base material interface was suppressed due to the resin sealing. Measurement of the adhesive strength of the specimens subjected to the salt spray test indicated that the adhesive strength of the sealed specimens remained higher than that of the unsealed specimens. In conclusion, the resin sealing treatment for the plasma spray-coated alumina coatings is an effective method for suppressing corrosion in the coating layer/base material interface and maintaining high adhesive strength.