• Title/Summary/Keyword: rough surfaces

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Gd$_2O_3$:Eu phosphor particles with spherical and filled morphology

  • Roh, Hyun-Sook;Kang, Yun-Chan;Park, Hee-Dong;Park, Seung-Bin
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.253-256
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    • 2002
  • $Gd_2O_3$:Eu phosphor particles were prepared by largescale ultrasonic spray pyrolysis process. The morphological control of $Gd_2O_3$:Eu particles in spray pyrolysis was performed by adding polymeric precursors into spray solution containing nitrate salts. The effect of composition and amount of polymeric precursors on the morphology, crystallinity, and photoluminescence characteristics of $Gd_2O_3$:Eu particles was investigated. The influence of chain length of PEG on the morphology and photoluminescence intensity was investigated. $Gd_2O_3$:Eu particles prepared from aqueous solution containing no polymeric precursors had a hollow structure and rough surfaces after annealing process. The phosphor particles prepared from solution containing 0.1M CA and 0.lM PEG with high molecular weight as 1,500 had a spherical and filled morphology and the highest photoluminescence intensity, which was 48% higher than that of the $Y_2O_3$:Eu commercial product.

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Diffusion barrier characteristics of molybdenum nitride films for ultra-large-scale-integrated Cu metallization (I); Surface morphologies and characteristics of sputtered molybdenum nitride films

  • Jeon, Seok-Ryong;Lee, You-Kee;Park, Jong-Wan
    • Journal of Korean Vacuum Science & Technology
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    • v.1 no.1
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    • pp.24-29
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    • 1997
  • Surface morphologies and fundamental characteristics of molybdenum nitride films deposited by reactive dc magnetron sputtering were studied for application to Cu diffusion barrier. A phase transformation from Mo to $\gamma$-Mo$_2$N phase at 0.5$N_2$ flow ratio.($N_2$/(Ar+$N_2$)) equal to and larger than 0.2, whereas a second phase transformation to $\gamma$-MoN phase at 0.5 N2 flow ratio, With the variation of the N2 ratio the surface morphologies of the films were generally smooth except the cases of 0.2 and 0.3$N_2$ gas rations, where build-up of film stresses occurred. $\gamma$-Mo$_2$N film was found to crystallize at the deposition temperature of 40$0^{\circ}C$. The surfaces of $\gamma$-Mo$_2$N films deposited up to 40$0^{\circ}C$ were smooth, but the film deposited at 50$0^{\circ}C$ had very rough surface morphology. It seems that this was due to the building-up of thermal stresses at the high deposition temperature, which might lead to hillock formation.

Quality Characteristics of Yakpyun by Adding Brown Rice (현미의 첨가량에 따른 약편의 품질특성)

  • Lee, Seung-Min;Yoo, Seung-Seok
    • Korean journal of food and cookery science
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    • v.27 no.4
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    • pp.47-54
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    • 2011
  • This study was performed to investigate the quality characteristics of Yakpyun with added brown rice. The Yakpyun was prepared with polished rice, brown rice, Jujube paste, Makkolli, sugar and salt. The Yakpyun was made with various levels (0, 20, 40, 60 or 80%) of added brown rice. After making the Yakpyun, it was examined for the effect of adding brown rice on quality characteristics using scanning electron microscopy (SEM), a mechanical test, and a sensory evaluation. The moisture contents of Yakpyun tended to decrease with increasing amounts of added brown rice, but no significant differences were observed. As the content of brown rice increased, the lightness (L) decreased and redness (a) and yellowness (b) increased. In a texture profile analysis, hardness decreased with increasing brown rice content from the moment of production to 3 days of storage. When more brown rice was added, rough surfaces were found more often under SEM, and large holes were evident between granules. The results of the sensory evaluation showed that overall acceptability was the highest for Yakpyun containing 40% added brown rice.

Characteristics of Electroplated Sn-2.5Cu Alloy Layers for Surface Finishing (표면마무리를 위한 Sn-2.5Cu 합금 도금막의 특성)

  • Kim, Ju-Youn;Bae, Kyoo-Sik
    • Korean Journal of Materials Research
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    • v.13 no.2
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    • pp.133-136
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    • 2003
  • Sn-2.5Cu alloy layers were deposited on the Alloy 42 lead-frame substrates by the electroplating method, and their microstructures, adhesion strength, and electrical resistivity were measured to evaluate the applicability of Sn-Cu alloy as a surface finishing material of electronic parts. The Sn-2.5Cu layers were electroplated in the granular form, and composed of pure Sn and Cu$_{6}$Sn$_{5}$ intermetallic compound. Surfaces of the electroplated Sn-2.5Cu layers were rather rough and also the thickness variance was large. The adhesion strength of the Sn-2.5Cu electroplated layers was highly comparable to that of the electroplated Cu alloy layer and the electrical conductivity was about 10 times higher than the pure Sn. After the 20$0^{\circ}C$ 30 min. annealing of the electroplated Sn-2.5Cu layers, the surface roughness was reduced, and adhesion strength and conductivity were improved. These results showed the Sn-Cu alloys can be used as an excellent surface finishing material.ial.

A Study on the Improvement in Performances and Wearing Sensation of Textiles for Taekwondo Wears (태권도복 소재의 성능 및 착용감의 개선을 위한 연구)

  • 전영민;박정희;최정화
    • Journal of the Korean Society of Clothing and Textiles
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    • v.27 no.1
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    • pp.134-142
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    • 2003
  • Performances of Taekwondo fabrics were evaluated in respect of fiber component. yarn count, weave structure and wearing comfort. As a beginning step, we investigated the present situation of Taekwondo wears by questionnaire from pro and amateur Taekwondo players. Samples employed in this study were cotton/nylon blend fabric that was newly woven for this study as well as fabrics of current Taekwondo wears for sale in the market. Their fundamental properties measured were such as air permeability, water vapor transport. wickability, absorption rate, Qmax values, thermal conductivity, durability, hand value, and etc. In addition, subjective wearing sensations were evaluated using Taekwondo wears made of those fabrics. From the results of the objective measurement and the subjective wearing test, we estimated the total fitness of fabrics as a Taekwondo wear. From the questionnaire we could see that pro players and amateurs wanted highly absorbing, quick drying, and soft-tough and complained abrasive surfaces and static elasticity of current fabrics. In view of the results so far achieved, nylon blended fabrics newly woven in this study, showed better comfort-related properties from both of the objective and subjective tests. It was also represented that finer yams enhanced water absorption and touch, and fabrics with rough surface such as honeycomb weave was superior in wearing comfort as well as aesthetic appearance.

3-D Reconstruction of Human Face Using the Derivative Moiré Topography

  • Bae, Yoon Jae;Ha, Byeong Wan;Park, Ji An;Cho, Choon Sik
    • Journal of the Optical Society of Korea
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    • v.18 no.5
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    • pp.500-506
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    • 2014
  • A new 3-D reconstruction algorithm for the human face is proposed using the derivative Moir$\acute{e}$ topography which ensures fast and robust reconstruction even for rough surfaces. The Moir$\acute{e}$ interference fringe pattern is initially obtained through the projection Moir$\acute{e}$ topography based on phase shifting, and then differentiated to provide a full unwrapped phase map for a human face. $2{\pi}$ ambiguity, which has been a chronically unsolved problem with Moir$\acute{e}$ topography, is successfully surmounted by differentiating the Moir$\acute{e}$ fringe patterns both in x- and y-directions when the object is located in the x-y plane. A real human face is used for verifying the proposed derivative Moir$\acute{e}$ topography. A human face of 4 different phase-shifted images taken in the fixed plane is almost fully reconstructed in 3-D format in 0.1 mm lateral resolution.

Quantitative Analysis of Roughness of Powder Surface Using Three-Dimensional Laser Profiler and its Effect on Green Strength of Powder Compacts (분말 표면 조도의 3차원 레이저 분석기를 이용한 정량화와 압분성형체 강도에 미치는 영향 분석)

  • Lee, Dong-Jun;Yoon, Eun-Yoo;Kim, Ha-Neul;Kang, Hee-Soo;Lee, Eon-Sik;Kim, Hyoung-Seop
    • Journal of Powder Materials
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    • v.18 no.5
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    • pp.406-410
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    • 2011
  • Green strength is an important property of powders since high green strength guarantees easy and safe handling before sintering. The green strength of a powder compact is related to mainly mechanical and surface characters, governed by interlocking of the particles. In this study, the effect of powder surface roughness on the green strength of iron powders was investigated using a transverse rupture test. Three-dimensional laser profiler was employed for quantitative analyses of the surface roughness. Two different surface conditions, i.e. surface roughness, of powders were compared. The powders having rough surfaces show higher green strength than the round surface powders since higher roughness leads increasing interlocked area between the contacting powders.

Interaction of Alkali Oxide and $SO_3$ on $3CaO.SiO_2$ Formation and Microstructure ($3CaO.SiO_2$ 생성반응과 미세조직에 있어서 Alkali Oxide와 $SO_3$의 상호작용)

  • 정해문;최상흘
    • Journal of the Korean Ceramic Society
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    • v.30 no.12
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    • pp.1071-1079
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    • 1993
  • Interaction of alkali oxides and SO3 and C3S formation and microstructure was studied using K2CO3 and Na2CO3 as alkali sources and (NH4)2SO4 for SO3. When SO3/K2O=1.43 as mole ratio, K2O and SO3 react to form K2SO4, this phase is immiscible with other oxide melt and thus could not affect C3S formation as well as its microstructure. In a condition of SO3/K2O 1, C3S crystals were round and grown in a much larger size. With addition of Na2O and SO3 by only 1wt% each, C3S formation was strongly hindered. Since C2S was stabilized by Na+ and SO4-2, it could not react to give C3S formation. However in the condition of SO3/Na2O=1.43, a little amount of C3S was formed. It is considered that small amount of Na2SO4 was formed, this phase was immiscible with clinker liquid, and the C3S crystals were formed locally in the liquid part of relatively low Na2O and SO3 compositions. These crystals had irregular and rough surfaces and contained more inclusions than those grown from K2O.SO3 system.

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Fatigue and mechanical properties of laser deposited maraging steel (레이저 적층 마레이징강의 기계적 특성 및 피로 특성)

  • Hong, Seok-Kwan
    • Design & Manufacturing
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    • v.12 no.3
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    • pp.36-41
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    • 2018
  • Metal 3D printing is very useful for making the injection molds containing complex conformal cooling channels. The most important issue of the 3D printed molds is cost and life cycle. However, powder bed fusion (PBF) methods are vulnerable to fatigue loading because of the presence of pores and rough surfaces. In the present study, the fatigue test was performed to obtain fatigue analysis input data for predicting the durability of a 3D printed injection mold core. The metal 3D printer used to manufacture the specimen was OPM250L from Sodick, and the metal powder material was maraging steel. The ultrasonic fatigue testing method was adopted for the fatigue test. A key advantage of the ultrasonic fatigue method is that $10^8{\sim}10^9$ long cycle test data or more could be obtained within a relatively short period. Based on the results of the experiment, the effect of heat treatment was negligible. However, there was an apparent difference in durability depending on the presence or absence of the surface treatment.

Development of smart CAD/CAM System for Machining Center Based on B-Rep Solid Modeling Techniques(ll) (A study on the 3-D CNC Cutting Planning Method Using Solid Model) (B-Rep 솔리드모델을 이용한 머시닝센터용 CAD/CAM시스템 개발(II)(솔리드모델을 이용한 3차원 CNC가공계획에 관한 연구))

  • Yang, Hee-Goo;Kim, Seok-Il
    • Journal of the Korean Society for Precision Engineering
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    • v.13 no.3
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    • pp.158-164
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    • 1996
  • In this paper, the CNC cutting planning module for product with three dimensional solid shape is realized to develop a smart CAD/CAM system which performs systematically from the shape design of procuct by the B-Rep solid modeler to the CNC cutting of product by a machining center. The three dimensional solid shape of product can be easily designed and constructed by the Euler operators and Boolean operators of the solid modeler. And the various functions such as the automatic generation of tool path for the rough and finish cutting processes, the automatic elimination of overcut, the automatic generation of CNC code for the machining center and do on, are established. Especially, the overcut-free tool paths are obtained by splitting the CL solid which is composed of the offset surfaces of the solid shape of product.

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