• 마이크로전자및패키징학회지
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• 제21권4호
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• pp.83-89
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• 2014

Solder paste plays a crucial role as the widely used joining material in surface mount technology (SMT). The understanding of its behaviour and properties is essential to ensure the proper functioning of the electronic assemblies. The composition of the solder paste is known to be directly related to its rheological behaviour. This paper provides a brief overview of the solder paste behaviour of four different solder paste formulations, stencil printing processes, and techniques to characterize solder paste behaviour adequately. The solder pastes are based on the Sn-3.0Ag-0.5Cu alloy, are different in their particle size, metal content and flux system. The solder pastes are characterized in terms of solder particle size and shape as well as the rheological characterizations such as oscillatory sweep tests, viscosity, and creep recovery behaviour of pastes.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2005년도 추계학술발표대회 논문집
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• pp.137-140
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• 2005

Exfoliated nanocomposites of polypropylene/layered silicate were prepared by a melt compounding process using maleic anhydride modified polypropylene (PP-g-MAH) and organoclay. It was found that polypropylene/layered silicate nanocomposites exhibited remarkable reinforcement compared with the pure polypropylene or conventional composite filled with agglomerated organoclay. The polypropylene /layered silicate nanocomposites showed stronger and earlier shear thinning behaviors and outstanding strain hardening behavior than pure polypropylene or other conventional composites in shear and uniaxial elongational flows, respectively. We simulated rheological modeling for the pure polymer matrix and polypropylene/layered silicate nanocomposite in shear and elongational flows using K-BKZ integral constitutive equation. The two types of K-BKZequations have been examined to describe experimental results of shear and uniaxial elongational viscosities of pure polypropylene and polypropylene/layered silicate nanocomposite.

• Korea-Australia Rheology Journal
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• 제16권4호
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• pp.201-212
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• 2004

Properties of polymer based nanocomposites depend on dispersion state of embedded fillers. In order to examine the effect of dispersion state on rheological properties, a new bi-mode FENE dumbbell model was proposed. The FENE dumbbell model includes two separate ensemble sets of dumbbells with different fric­tion coefficients, which simulate behavior of well dispersed and aggregated carbon nanotubes (CNTs). A new parameter indicating dispersion state of the CNT was proposed to account for degree of dispersion quantitatively as well as qualitatively. Rheological material functions in elongational, steady shear, and oscillatory shear flows were obtained numerically. The CNT/epoxy nanocomposites with different dis­persion state were prepared depending on whether a solvent is used for the dispersion of CNTs or not. Dis­persion state of the CNT in the epoxy nanocomposites was morphologically characterized by the field emission scanning electronic microscope and the transmission electron microscope images. It was found that the numerical prediction was in a good agreement with experimental results especially for steady state shear flow.

• 한국세라믹학회지
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• 제40권7호
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• pp.632-636
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• 2003

To prepare the alumina cement free vibrated alumina castable, $\rho$-alumina is employed as a binder material, and nano-sized clay is added to enhance the curing strength and give thixotropic behavior. The rheological behavior of matrix of castable is controlled by investigating the influences of ultrafines, $\rho$-alumina, and nano-sized clay on the viscosity of matrix. The microsilica and ultrafine alumina were added 3 wt% and 4 wt%, respectively to the matrix, which showed that the viscosities tends to be lowest values. The rheological property of the matrix is well established by adding $\rho$-alumina as 8 wt% and clay as 4 wt%. The thixotropic behavior of the $\rho$-alumina bonded castable was appeared by introducing nano-sized clay into the matrix and adjusting the pH near to the PZC of the clay suspension.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1996년도 춘계학술대회 논문집
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• pp.31-34
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• 1996

In this paper, the rheological chances in sensitive materials was investigated by using QCA(Quartz Chemical Analyzer). Langmuir-Blodgett method was used to transfer sensitive material to the quartz crystals because of its facility to control that amount, and deposited sensitive material has uniformity to compare with other methods respectively. For the gas sensor using mass loading effect of quartz crystal microbalance, generally the Sauberary equation has been believed to represent the only mass loading effect. But when the organic gas is adsorpted into sensitive material, the rheological changes are occurred with different pattern as to the kinds of gases. Thus, much simpler method to identify the organic or hazard gas will be obtained by the consideration of resonant frequency changes and resonant admittance changes simultaneously.

• 한국재료학회:학술대회논문집
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• 한국재료학회 1995년도 추계 학술발표 강연 및 논문개요집
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• pp.140-141
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• 1995

• International Journal of Industrial Entomology and Biomaterials
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• 제22권1호
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• pp.5-10
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• 2011

The effect of sample handling condition on the rheological measurement of regenerated silk fibroin formic acid solution using parallel plate geometry was investigated. In case of loading method, the loading by pouring sample solution resulted in the best reproducibility of rheological measurement. Loading with spoon showed a high variance of viscosity value at low shear rate region ($0.01{\sim}1sec^{-1}$) while loading with syringe exhibited a low reproducibility of viscosity at high shear region ($1{\sim}100sec^{-1}$) with a disappearance of shear thinning phenomenon. It was revealed that the sample loading with small extra amount lead to the most reproducible result. The sample loading with the exact amount for the measuring plate resulted in a lack of reproducibility of high shear viscosity, while the loading with large extra volume produced a limited consistency of low shear viscosity. It was turned out that 3 min. of waiting time before measurement was the optimum condition for reliable result. When the waiting time was less than 1 min., the low shear viscosity was obtained with a lack of consistency. On the other hand, the sample solution started drying when the waiting time increased up to 5 min.

• 한국세라믹학회지
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• 제42권11호
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• pp.737-742
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• 2005

Rheological properties of ordinary portland cement (OPC) containing metakaoline (MK), granulated blast furnace slag (GBS) and polycarboxylate type superplasticizer (PCA) were investigated using a mini-slump test, sedimentation test and viscometer. Fluidity of cement pastes containing MK (OPC-MK, OPC-MK-GBS systems) with PCA were higher than those of the cement pastes without MK(OPC, OPC-GBS systems). Colloid suspensions with $0.1\%$ PCA were changed from stable sedimentation behaviors to flocculation behaviors in the OPC-MK, OPC-GBS and OPC-MK-GBS systems. The colloid suspensions showed stable sedimentation behaviors with PCA greater than $0.2\%$. The OPC system showed shear thinning behavior. However, the other systems showed weak shear thinning behaviors with PCA. Rheological properties of cement pastes were improved when MK and GBS were contained together. The rheological properties of OPC-MK, OPC-GBS and OPC-MK-GBS systems were improved by PCA added greater than $0.2\%$.

• 한국유변학회:학술대회논문집
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• 한국유변학회 2006년도 춘계 학술발표회 논문집
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• pp.61-64
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• 2006

Soft materials, such as polymer solutions, gels and filamentous protein materials in cells, show complicated behavior due to their complex structures and dynamics with multiple characteristic time and length scales. Several complementary techniques have been developed to measure viscoelastic of soft materials. Especially, particle tracking microrheology, using the Brownian motion of particles in a medium to get rheological properties, has recently been improved both theoretically and experimentally. Compared to other conventional methods, video particle tracking microrheology has some advantages such as small sample volume, detecting spatial variation of local rheological properties, and less damage to sample materials. With these advantages, microrheology is more suitable to measure the properties of complex materials than other mechanical rheometries.

• 한국응용과학기술학회지
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• 제32권3호
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• pp.386-393
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• 2015

콜로이드 분산계와 같은 복잡한 물질의 유변성질은 전단 흐름이 일어날 때 비뉴톤 유동현상을 나타낸다. 이들 유변성질은 유동단위의 성질과 유동 세그먼트 사이의 상호작용에 의하여 영향을 받는다. 유동곡선을 이론적인 틱소트로피식에 적용하여 여러 틱소트로피 유동 곡선에 대한 유동파라메타, 완화시간, $({\beta}_2)_0$, 구조적인 요인, $C_2$, 전단 모듈러스, $X_2/{\alpha}_2$을 구하였다. 유변 파라메타의 변화는 비뉴톤 유동, 점도, 유동 세그먼트의 유동 활성화 에너지와 직접적인 관계가 있다.