• 한국산업융합학회 논문집
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• 제26권4_2호
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• Restorative Dentistry and Endodontics
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• 제39권4호
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• pp.303-309
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• 2014

Objectives: Hydrogen peroxide ($H_2O_2$) surface treatment of fiber posts has been reported to increase bond strength of fiber posts to resin cements. However, residual oxygen radicals might jeopardize the bonding procedure. This study examined the effect of three antioxidant agents on the bond strength of fiber posts to conventional and self-adhesive resin cements. Materials and Methods: Post spaces were prepared in forty human maxillary second premolars. Posts were divided into five groups of 8 each: G1 (control), no pre-treatment; G2, 10% $H_2O_2$ pre-treatment; G3, G4 and G5. After $H_2O_2$ application, Hesperidin (HES), Sodium Ascorbate (SA) or Rosmarinic acid (RA) was applied on each group respectively. In each group four posts were cemented with Duo-Link conventional resin cement and the others with self-adhesive BisCem cement. Push-out test was performed and data were analyzed using 2-way ANOVA and tukey's post-hoc test (${\alpha}=0.05$). Results: There was a statistically significant interaction between the cement type and post surface treatment on push-out bond strength of fiber posts (p < 0.001, F = 16). Also it was shown that different posts' surface treatments significantly affect the push-out bond strength of fiber posts (p = 0.001). $H_2O_2$ treated posts (G2) and control posts (G1) cemented with Duo-link showed the highest ($15.96{\pm}5.07MPa$) and lowest bond strengths ($6.79{\pm}3.94$) respectively. Conclusions: It was concluded that $H_2O_2$ surface treatment might enhance the bond strength of fiber posts cemented with conventional resin cements. The effect of antioxidants as post's surface treatment agents depends on the characteristics of resin cements used for bonding procedure.

• 대한치과보철학회지
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• 제38권5호
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• pp.640-649
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• 2000

In the restoration of endodontically treated teeth, carbon fiber post was recently introduced. The purpose of this in vitro study was to investigate the fracture strength of teeth restored with a pre-fabricated carbon fiber post in comparison with teeth restored with a prefabricated titanium post & custom cast gold post after cyclic loading in the different environment. A total of 30 recently extracted human central incisors of similar dimension with crowns removed were used. All teeth were placed into acrylic blocks and every steps for post and core fabrication were made accord-ing to manufacture's instruction. The post length and core dimensions were standardizd. All teeth were divided into 6 groups: 1) carbon fiber post / atmosphere, 2) titanium post / atmosphere, 3) gold post / atmosphere, 4) carbon fiber post / wet, 5) titanium post / wet, 6) gold post / wet. Carbon fiber post and titanium post were cemented in place using resin cement and cores were fabricated with Ti-Core. Custom cast gold post was made from Duralay pattern resin and cemented using resin cement, too. All specimens were thermocycled 10,000 times. After 50,000 cyclic loading, failure strength was measured using Instron testing machine. Kruskal-Wallis test followed by Mann-Whitney test was used to compare the mean fracture strength. Results were as follows : 1. All specimens showed lower fracture strength in wet environment after cyclic loading than in atmosphere condition, but did not reveal a significant difference. 2. There was no significant difference between carbon fiber post specimen and titanium post specimen in the same environment. 3. Gold cast post specimen showed significant different greater fracture strength than those of others in the same environment. 4. Carbon fiber post specimen showed no root fracture.

• 대한치과보철학회지
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• 제31권4호
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• pp.461-467
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• 1993

The purpose of this study was to evaluate the effects of method for construction of cast post and type of dental cement on the retention of cast post. The wax patterns or Duralay resin patterns were used for construction of cast post. The dental cements used in this study were zinc phosphate cement(Fleck's zinc cement, Mizzy INc., U.S.A.), glass ionomer cement(Fuji I, G-C Co., Japan), and resin cement(Panavia-EX, Kuraray Co., Japan) and the retention of cast post was measured with Instron Universal Test Machine(Instron Engineering Co., U.S.A.). The obtained results were as follows : 1. The tensile bond strength of cast posts made by Duralay resin patterns revealed 39.13(kg) with Panavia-EX, 46.40(kg) with phosphate cement, and 37.78(kg) with glass ionomer cement. 2. The tensile bond strength of cast posts made by wax patterns revealed 39.25(kg) with Panavia, EX, 44.12(kg) with phosphate cement, and 40.23(kg) with glass ionomer cement. 3. The tensile bond strength of cast posts made by Duralay resin patterns or wax patterns were not affected by the type of dental cements(P>0.05).

• 구강회복응용과학지
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• 제27권3호
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• pp.253-265
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• 2011

근관치료된 치아의 수복에서 fiber post 크기와 포스트 공간의 직경이 일치하지 않은 경우, 포스트 공간은 두꺼운 레진 시멘트로 채워지게 된다. 레진 시멘트가 두꺼워지면 시멘트 내에 기포가 형성되어 포스트 분리가 발생되기 쉽다. 이런 문제점을 해결하기 위한 방법은 composite resin을 이용하여 fiber post를 relining하는 것이다. 이렇게 형성된 해부학적 포스트는 포스트 공간에 잘 적합하고 시멘트의 두께를 감소시킨다. 이 연구의 목적은 relining 과정과 임상 과정의 간소화를 위해 사용되고 있는 luting agents 종류에 따른 fiber post의 push-out 결합 강도를 평가하는 것이다. 42개의 발치된 치아는 6개의 그룹(n=7)으로 나누어졌다. (A1: relined fiber post를 Luxacore/all-bond 2로 합착, A2: non-relined fiber post를 Luxacore/all-bond 2로 합착. B1: relined fiber post를 Calibra/XP-bond로 합착. B2: non-relined fiber post를 Calibra/XP-bond로 합착. C1: relined fiber post를 RelyX Unicem으로 합착. C2: non-relined fiber post를 RelyX Unicem으로 합착.) Push-out 결합 강도는 relining procedure와 cement type의 상호작용에 의해 영향을 받는 것으로 나타났다. relined fiber post 그룹이 non-relined fiber post 그룹보다 더 높은 결합 강도를 가지며 fiber post relining 과정은 결합강도에 유의한 영향을 가진다.(p<0.05) Luting agent에 따라 모든 그룹에서 RelyX Unicem의 결합강도가 Luxacore/All-bond 2와 Calibra/XP bond에 의한 것보다 유의하게 더 높았다(p<0.05).

• 대한화학회지
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• 제53권4호
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• pp.422-426
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• 2009

Indion 190 수지의 존재하에서 di-tert-butoxypyrocarbonate $(Boc)_{2}O$를 이용한 아민의 N-Boc protection의 효과적인, 화학적 선택성적인, 실용적인 실험안. 수지는 반응혼합물로부터 쉽게 분리되었고 활성의 감소 없이 재사용되었다. 간단한 workup, 온화한 조건, 짧은 반응시간, 높은 수율은 이 방법의 두드러진 특색들이다.

• Restorative Dentistry and Endodontics
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• 제8권1호
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• pp.45-51
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• 1982

An endodontically treated tooth is likely to be brittle than a vital tooth. Internal structure of the tooth has been weakened due to a significant removal of dentin by coronal access, canal preparation. There are many controversies concerning with various methods of reinforcing an intact anterior tooth that has endodontic treatment. In this experiment, 128 extracted maxillary anterior teeth were endodontically treated, and prepared with 4 methods of restorations; Composite resin filling with zinc phosphate cement, composite resin filling without zinc phosphate cement, composite resin filling with post, and metal crown with post. An Instron testing machine was used to measure the fracture loads of the specimens. The means of the failure loads for the 4 groups were compared by F-test statistically and the failure modes were observed. The results were as follows; 1. There were no statistically significant difference between the failure loads of the four methods of restoration. 2. Teeth without post were fractured in a horizontal or oblique plane through upper or middle third of the root. 3. In the posted teeth, fractures were occurred around the post. 4. In the metal crowned teeth with post, the fracture were occurred around the post or coronal area.

• 대한치과보철학회지
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• 제26권1호
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• pp.23-30
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• 1988

An in vitro study was performed to compare the retentive value of cast post cemented with three commonly used cements and one composite resin. Twenty cast posts were made from twenty extracted lower premolars. The samples were randomly divided into four groups. The first group was cemented with zinc phosphate cement, the second group with polycarboxylate cement, the third group with glass-ionomer cement, and the fourth group with composite resin. The tensile load test was performed on an Instron testing machine with crosshead speed of 2 mm/min and the results were compared statistically. The results were as follows ; 1. The mean value of tensile break force of cemented cast post was 23.36Kg in case of zinc phosphate cement, 16.28Kg in case of polycarboxylate cement, 22.09Kg in case of glass-ionomer cement , and 26.88Kg in case of composite resin. 2. Retention was not significantly different among zinc phosphate cement, glass-ionomer cement and composite resin. 3. Polycarboxylate cement was found to be less retentive than zinc phosphate cement, glass-ionomer cement , and composite resin.

• Restorative Dentistry and Endodontics
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• 제12권2호
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• pp.111-116
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• 1987

The experimental study was made to evaluate the influence of retentive grooves on the canal wall upon the retention of post, using different type of cements. Ninety periodontally involved anterior teeth were extracted and divided into six groups of 15 teeth. The groups were labeled as follows: Group I: Dentatus post cemented zincphosphate cement into post hole with smooth wall. Group II: Dentatus post cemented with zincphosphate cement into post hole with retentive grooves. Group III: Dentatus post cemented with glass-ionomer cement into post hole with smooth wall. Group IV: Dentatus post cemented with glass-ionomer cement into post hole with retentive grooves. Group V: Dentatus post cemented with composite resin adhesive into post hole with smooth wall. Group VI: Dentatus post cemented with composite resin adhesive into post hole with retentive grooves. The tensile strength was tested by an Instron type tester with cross-head speed of 5mm per minute. The results were as follows: In the group without retentive grooves, three kinds of cement have little effect upon retentive capacity of Dentatus post. The Dentatus post cemented on the canal wall with retentive grooves is more retentive than Dentatus post without retentive grooves.

• Restorative Dentistry and Endodontics
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• 제35권6호
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• pp.479-485
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• 2010

연구목적: 이 연구의 목적은 레진 시멘트의 포스트 공간 내 적용 방법에 따른 포스트의 push-out접착 강도를 비교하는 것이었다. 연구 재료 및 방법: 30개의 발거된 하악소구치를 사용하여 시멘트의 적용 방법에 따라 세 그룹으로 나누었는데 lentulo-spiral을 이용하여 포스트 공간 내에 레진 시멘트를 적용하는 그룹 (group Lentulo), 직접 포스트 표면에 레진 시멘트를 도포하는 그룹 (group Direct), elongation tip을 이용하여 포스트 공간 내에 레진 시멘트를 적용하는 그룹 (group Elongation tip)으로 나누었다. 근관을 성형, 충전한 뒤 Rely-X post drill을 사용하여 포스트 공간을 형성하였고, Rely-X fiber post를 Rely-X Unicem 적용하여 광중합 하였다. 시편을 아크릴릭 레진에 포매 하고 저속 절단기로 치아 장축에 수직으로 절단하여, 하나의 치아에서 치관부, 중앙, 근단부의 세 개의 시편을 얻었다. 절단한 시편을 Universal Testing Machine으로 push-out 접착 강도를 측정하였다. 접착 실패가 일어난 시편을 수술용 현미경 하에서 관찰하여 그 실패 양상을 결정하였다. 결과: 치근의 위치에 따른 push-out 접착 강도는 유의한 차이를 보였으며, 전용의 elongation tip을 사용한 그룹이 가장 높은 push-out 접착 강도를 나타냈다. 결론: 레진 시멘트를 포스트에 직접 적용하거나 lentulo-spiral을 사용하는 기존의 방법에 비해 elongation tip을 사용하는 것이 self-adhesive 계면의 결함을 줄이고 근관치료한 치아의 수복 성공율을 높일 수 있을 것으로 생각된다.