• 한국표면공학회지
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• 제48권3호
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• pp.73-81
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• 2015

Chloride plating solution was fabricated by dissolving metal Ni powders in solution with HCl and deionized water. Effects of deposition conditions on the properties of Ni films electrodeposited from chloride baths were studied. Current efficiency of Ni films electrodeposited from the baths containing saccharin was decreased with increasing the current density. Residual stress of Ni thin films ware measured to be about 230 ~ 435 MPa in the range of current density of $10{\sim}25mA/cm^2$. Cathode current efficiency in baths without saccharin was initially increased with increasing pH, while it was decreased with increasing pH further. Cathode current efficiency in baths with saccharin (except at pH 2) exhibited less 10 ~ 20% than that in baths without saccharin. Residual stress of Ni films electrodeposited from baths without saccharin was measured to be 388 ~ 473 MPa in the range of pH 2 ~ pH 5 and then was increased to 551 MPa at pH 6. On the other hand, residual stress of Ni films electrodeposited from baths with saccharin was increased with increasing pH. Surface morphology was strongly affected by the change of current density, but slightly by solution pH and addition of saccharin.

• 한국지반환경공학회 논문집
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• 제15권8호
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• pp.13-21
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• 2014

항만 터미널 부두 지역의 연약지반 개량을 위해 PBD가 적용되었다. 본 논문은 PBD가 적용된 연약지반에서 PBD가 설치된 직후부터 상부 구조물 운용 후의 잔류침하거동에 대해서 다루고 있다. 기존의 연구는 개량공법 시공 중에 발생하는 침하, 즉 PBD 개량 효과에 대해 주로 이루어졌다. 실제 시설물의 운용 중에 발생하는 잔류침하는 시설물의 유지 및 운용을 위해서는 아주 중요한 요소이나 이 부분에 대한 연구는 매우 부족한 실정이다. 본 연구에서는 실제로 운용 중에 있는 항만 터미널 부두의 침하량 계측결과를 분석하여 운용 중에 발생한 침하량은 PBD 개량층에서 발생하는 것을 확인하였다. 또한 계측값과 수치해석 값을 비교한 결과 계측값이 수치해석에 의해 예측된 잔류침하량 내에서 수렴하는 것도 확인하였다.

• 한국지구물리탐사학회:학술대회논문집
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• 한국지구물리탐사학회 2006년도 공동학술대회 논문집
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• pp.155-160
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• 2006

이 논문에서 중력이상에서 광역이상과 잔여이상을 분리하는 문제를 다루었다. 지구통계학의 한 가지 방법인 인자크리깅 기법을 이용하여 공간필터링에 적용하였다. 이 방법은 일반적으로 광역이상은 공간적으로 큰 규모의 상관관계를 가지고 잔여이상은 좁은 지역에서 높은 상관관계를 가진다는 가정에서 출발하였다. 크리깅 방법의 하나인 인자크리깅(Factorial kriging)을 적용하기 위하여 영향 반경이 큰 지역과 작은 지역에 적합한 서로 다른 베리오그램 모델을 적용하여 각각을 광역이상과 잔여이상으로 구분하였다. 이 방법의 적용가능성을 검증하기 위하여 한 방향으로 증가하는 경향을 가정한 광역이상에 단일 이상체를 가정한 잔여이상이 더해진 합성 모델에 대하여 적용하였다. 베리오그램 모델은 각각 광역이상과 잔여이상을 나타내는 두개의 서로 다른 베리오그램 모델의 합으로 근사할 수 있었다. 따라서 서로 다른 두개의 베리오그램 모델에 대하여 인자 크리깅을 이용한 공간필터링을 적용한 결과 광역이상과 잔여이상을 구분할 수 있다. 이 방법을 폐갱도가 존재하는 지역에서의 고정밀중력탐사 자료에서 적용하여 잔여이상을 추출하였고, 다항식 접합법의 결과와도 비교하였다. 이 연구를 통하여 인자크리깅을 이용한 공간필터링 방법이 중력이상에서 광역이상과 잔여이상을 분리해 낼 수 있는 한 가지 방법이 될 수 있음 보였다.

• 한국식품위생안전성학회지
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• 제9권1호
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• pp.1-13
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• 1994

A Simultaneous determination method was improved for the determination and confirmation of zeranol, zearalenone, as well as their isomers and metabolites, in beef. The analytes were extracted from tissue by CH3CN, hydrolyzed enzymatically(for glucuronide conjugates), cleaned up by a strong basic anion exchange resin combined with a liquid/liquid partitioning, derivatized using MSTFA and confirmed, quantified by GC/MS/SIM with a internal standard, zearalane. The results were as follows : (1) all the estrogens were separated on the GC/MS chromatogram under the extraction method and the chromatographic conditions improved, the retention times of zearalane-TMS2, zearalanone-TMS2, zearalenone-TMS2, zeranol-TMS3, taleranol-TMS3, and $\alpha$-zearalenol-TMS3, $\beta$-zearalenol-TMS3, were 18.49, 19.44, 19.63, 19.71, 19.79 and 19.99, 20.08 minutes, respectively. (2) The calibration curves of residual zeranol, zearalenone and their metabolites showed constantly linear(r=0.99) in the range of 5~20 ng. The minimum detection concentration of residual zeranol, zearalenone and their metabolites was 1 ppb. (3) The total average recovery of residual zeranol, zearalenone and their metabolites from spiked beef was 60.2%(CV=29.7%) at the 1 ppb and 63.5%(CV=26.5) at the 2 ppb, 72.9%(CV=18.2%) at the 4 ppb. (4) The preservation method for 6 estrogens was improved for the fast running time(21 min) and MSTFA was utilized for derivatizing 6 estrogens for improvement of recovery, for good resolution, for characteristic mass spectra unlike Jose's method and Tina's method. The utilization of zearalane as internal standard showed good quantification result for zeranol, zearalenone, as well as their isomers and metabolites, in beef.

• 한국식품위생안전성학회지
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• 제24권4호
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• pp.338-347
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• 2009

The content of residual pesticides in commercial agricultural products in Gyeongsangbuk-Do area was investigated for 5 years extending the year 2004 through 2008. The detection rates of residual pesticides in agricultural products by year were similar in range of 11.6~16.4%. But the violation rates showed lower values in the last years from 4.5% of the year 2004 to 0% of the year 2007. The highest residual concentration of each pesticide detected in commercial agricultural products was investigated by year. That is, in the year 2004 and 2005, chlorpyrifos, chlorothalonil, diazinon, endosulfan, ethoprophos, fenarimol and procymidone were detected over the tolerance in kale, parsley, celery, chard and lettuce, and in the year 2006, permethrin in the soybean and peanut. The detection rate and violation rate of pesticides were highly increased in the order of the endosulfan, chlorpyrifos, procymidone, chlorfenapyr, fenitrothion, imazalil, isoprothiolane, methidathion and permethrin. The detection rate and violation rate of pesticides were increased after August every year.

• 한국자동차공학회논문집
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• 제16권5호
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• pp.1-7
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• 2008

A study of new materials that are light-weight, high in strength has become vital to the machinery of auto industries. But then, there are a lot of problems with developing such materials that require expensive tools, and a great deal of time and effort. Therefore, the improvement of fatigue strength and fatigue life are mainly focused on by adopting residual stress. And Influence of corrosive condition for corrosion fatigue crack was investigated, after immersing in 3.5%NaCl, $10%HNO_3$+3.5%HF, $6%FeCl_3$. The immersion period was performed for 365days. The compressive residual stress was imposed on the surface according to each shot velocity based on shot peening, which is the method of improving fatigue life and strength. Fatigue life shows more improvement in the shot peened material than in the un peened material in corrosion conditions. The threshold stress intensity factor range was decreased in corrosion environments over ambient. Compressive residual stress of surface on the Shot-peen processed operate resistance force of fatigue crack propagation. The fatigue crack growth rate of the Shot-peened material was lower than that of the un peened material. Also m, fatigue crack growth exponent and number of cycle of the shot peened material was higher than that of the un peened material. That is concluded from effect of da/dN.

• 한국재료학회지
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• 제11권9호
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• pp.769-775
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• 2001

High quality PZT piezoelectric thin films were sputter- deposited on$ RuO_2$/$SiO_2$/Si substrates by using 2-step deposition method. As the first step, PZT seed layers were fabricated at a low temperature($475^{\circ}C$ ) to form a pure perovskite phase by reducing the volatility of Pb oxide. and then, as the second step, the PZT films were deposited at high temperatures ($530^{\circ}C$~$570^{\circ}C$) to reduce the defect density in the films. By this method, the pure perovskite phase was obtained at high deposition temperature range ($530^{\circ}C$~$570^{\circ}C$) and the superior electrical properties of PZT films were obtained on $RuO_2$substrate : 2Pr : 60$\mu$C/$\textrm{cm}^2$, $E_c: 60kV/cm, \;J_t: 10^{-6}A/cm^2\; at\; 250kV/cm$. The residual stress of PZT films fabricated by the 2-step deposition method was tensile and below 150MPa. It was attempted to control the residual stress in the PZT films by applying a negative bias to the substrate. As the amplitude of the substrate bias was increased, the residual tensile stress was slightly decreased, however, the ferroelectric properties of PZT films were degraded by ion bombardment.

• Design & Manufacturing
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• 제16권1호
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• pp.27-35
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• 2022

Thermoforming is a plastic manufacturing process that applies a force to stretch a film of heated thermoplastic material over an engineered mold to create a 3-dimensional shape. After forming, the shaped part can then be trimmed and finished to specification to meet an end-user's requirements. The process and thermoplastic materials are extremely versatile and can be utilized to manufacture parts for a very wide range of applications. In this study, based on K-BKZ nonlinear viscoelastic model, thermoforming process analysis was performed for an interior room-lamp. The predicted thickness was minimum at the corner of a molded film, and maximum at the center of the bottom. By using the Taguchi method of design of experiments, the effects of process conditions on residual stresses were investigated. The dominant factors were the liner thickness and the film heating time. As the thickness of the liner increased, the residual stress decreased. And it was found that the residual stress decreased significantly when the film heating temperature was higher than the glass transition temperature. A thermoforming mold and a trimming mold were manufactured, and the spring back was investigated through experiments. The dominant factors were film heating time, liner thickness, and lower mold temperature. As the film heating time and liner thickness increased, the spring back decreased. In addition, it was found that the spring back decreased as the lower mold temperature increased.

• Nuclear Engineering and Technology
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• 제53권12호
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• pp.3879-3891
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• 2021

A heat pipe residual heat removal system is proposed to be incorporated into the reactor driven subcritical (RDS) facility, which has been proposed by MIT Nuclear Reactor Laboratory for testing and demonstrating the Fluoride-salt-cooled High-temperature Reactor (FHR). It aims to reduce the risk of the system operation after the shutdown of the facility. One of the main components of the system is an air-cooled heat pipe heat exchanger. The alkali-metal high-temperature heat pipe was designed to meet the operation temperature and residual heat removal requirement of the facility. The heat pipe model developed in the previous work was adopted to simulate the designed heat pipe and assess the heat transport capability. 3D numerical simulation of the subcritical facility active zone was performed by the commercial CFD software STAR CCM + to investigate the operation characteristics of this proposed system. The thermal resistance network of the heat pipe was built and incorporated into the CFD model. The nominal condition, partial loss of air flow accident and partial heat pipe failure accident were simulated and analyzed. The results show that the residual heat removal system can provide sufficient cooling of the subcritical facility with a remarkable safety margin. The heat pipe can work under the recommended operation temperature range and the heat flux is below all thermal limits. The facility peak temperature is also lower than the safety limits.

• 대한방사선기술학회지:방사선기술과학
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• 제46권4호
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• pp.277-285
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• 2023

In this study, pneumonia identification networks with the small number of layers were constructed by using chest X-ray images. The networks had similar trainable-parameters, and the performance of the trained models was quantitatively evaluated with the modification of the network architectures. A total of 6 networks were constructed: convolutional neural network (CNN), VGGNet, GoogleNet, residual network with identity blocks, ResNet with bottleneck blocks and ResNet with identity and bottleneck blocks. Trainable parameters for the 6 networks were set in a range of 273,921-294,817 by adjusting the output channels of convolution layers. The network training was implemented with binary cross entropy (BCE) loss function, sigmoid activation function, adaptive moment estimation (Adam) optimizer and 100 epochs. The performance of the trained models was evaluated in terms of training time, accuracy, precision, recall, specificity and F1-score. The results showed that the trained models with the small number of layers precisely detect pneumonia from chest X-ray images. In particular, the overall quantitative performance of the trained models based on the ResNets was above 0.9, and the performance levels were similar or superior to those based on the CNN, VGGNet and GoogleNet. Also, the residual blocks affected the performance of the trained models based on the ResNets. Therefore, in this study, we demonstrated that the object detection networks with the small number of layers are suitable for detecting pneumonia using chest X-ray images. And, the trained models based on the ResNets can be optimized by applying appropriate residual-blocks.