• Title/Summary/Keyword: relative bond strength

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A Study of the appraisal for adhesive stability classified by tile bond agent on the dry wall surface (건식벽체에서 접착제 종류에 따른 타일부착 안전성 평가에 관한 연구)

  • Um Chan-Young;Sun Yoon-Suk;Kwon Shi-Won;Oh Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.05a
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    • pp.173-178
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    • 2005
  • The tile construction methods for existing have been used materials within limit which adhesion by wet method in masonry wall and concrete structure. These existing adhesive tech can caused many problems in construction of large and reform tile, after that it can be happened loose scale, peel off, falling off tile by heat and vibration or impact. In according to, this study is to test tile for bond stability, adhesive property by impact, vibration. low property by heat and then, we have the results as below; (1) The tile adhesive stability can be effected as adhesive area between bond agent and tile, adhesive area can more wide and press enough to ensure property. (2) Existing adhesive strength and standard relative tile construction is limited to adjust performance tile on the concrete and masonry wall. In summary, It is necessary to establish standard of performance and test method to ensure tile adhesive salability in dry wall.

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A STUDY ON THE PHYSICAL PROPERTIES OF ROOT CANAL SEALERS (근관충전용 실러의 물리적 성질에 관한 연구)

  • Chang, Young-In;Choi, Ho-Young
    • Restorative Dentistry and Endodontics
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    • v.20 no.1
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    • pp.142-151
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    • 1995
  • The purpose of this study was to compare and estimate the physical properties of five root canal sealers classified Calciobiotic root canals sealer as calcium hydroxide based sealer, Apatite root sealer type II as calcium phosphate based sealer, AH-26 as resin based sealer, Canals and Pulpdent root canals sealer as zinc oxide eugenol based sealer. The author investigated dimensional change and flow rate of canal sealers, diametral tensile strength and shear bond strength of sealers to dentin to evaluate the physical properties on affect of complete obturation of root canal and performed the total 100 specimens of each 25 sealers under the condition of root temperature according to manufacturer's instructions. All specimens were stored at $37{\pm}1^{\circ}C$ in 100 % relative humidity. A microscope for measurement of micro distance is used for the dimensional change test and evacuation methods using vaccum were used for the flow rate test. The result differed by the storage time measured on the tests of diametral tensile strength and shear bond strength to dentin. The following results were obtained ; 1 On the test of dimensional change, Canals and Pulpdent expanded slightly, AH-26 and Apatite showed the severe shrinkage after 48 hours. 2. AH-26 and Apatite were the excellent with each 24.59mm, 31.19mm after 3 minutes in the aspect of flow property. 3. On the diametral tensile strength, Calciobiotic root canals sealer showed the highest strength with 27.13kg/$cm^2$ after 48 hours, Apatite root sealer type II showed highest strength with 84.57kg/$cm^2$ after 120 hours. 4. On the shear bond strength to dentin, AH-26 was most excellent with 55.73kgf/$cm^2$ after 24 hours and with 134.71kgf/$cm^2$ after 120 hours.

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A STUDY OF SHEAR BOND STRENGTH AND FAILURE PATTERNS IN LIGHT-AND SELF-CURED ORTHODONTIC RESIN (교정용 광중합형 및 화학중합형 레진접착제의 전단결합강도와 파절양상에 대한 연구)

  • Lee, Min-Ha;Yang, Kyu-Ho;Park, Yeong-Joon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.23 no.2
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    • pp.549-558
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    • 1996
  • Light-cured orthodontic composite resin has been widely advertised recently for use in bonding brackets. However, the curability of light-cured resin when light waves are diffused through metal brackets in questionable. The purposes of this study were to evaluate shear bond strength and failure patterns of visible light-cured resin(Lightbond) and chemically cured-resin(Mono-Lok 2), and to determine the relative value of light-cured resin as an alternative to conventional chemically cured resin. Each of the two resins was tested on twenty extracted human first premolars. Standard edgewise metal brackets were bonded to the teeth in accordance with the manufacturers' recommendation. After bonding, the teeth were stored for 24 hours at $37^{\circ}C$, 100% humidity. The shear bond strength was tested with a universal testing machine(Instron 4302), at 0.5mm/min crosshead speed. After debonding, brackets and enamel surfaces were examined with a scanning electron microscope and a stereoscopic microscope. The results were as follows : 1. Metal brackets bonded with Lightbond showed statistically higher shear bond strength than metal brackets bonded with Mono-Lok2. 2. The predominant failure site in Lightbond was the enamel-resin interface, and in Mono-Lok 2 it was the resin itself. 3. Enamel cracks were not found in any specimen. The above results suggest that direct bonding of metal brackets to enamel with light-cured resin bonding agent can be used effectively in clinics.

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A STUDY ON THE SHAR BOND STRENGTH OF LIGHT-CURED GLASS IONOMER CEMENTS TO DENTIN ACCORDING TO CURING TIME INDUCED BY ARGON LASER (아르곤 레이저의 조사시간에 따른 광중합형 글래스 아이오노머 시멘트의 상아질에 대한 전단결합강도에 관한 연구)

  • Cho, Young-Lin;Hwang, Ho-Keel;Cho, Young-Gon;Oh, Haeng-Jin
    • Restorative Dentistry and Endodontics
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    • v.22 no.1
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    • pp.267-277
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    • 1997
  • The purpose of this study was to evaluate the shear bond strength of light-cured glass ionomer cements to dentin surface according to curing time induced by argon laser. In this study, 160 extracted human molars with sound crown were used. The dentin surface of these teeth were exposed with high speed diamond bur under water spray and polished with 120, 320, 400, 800, 1200 grits sand paper. 160 extracted human molars were randomly assigned into four groups (control, experimental 1, 2 & 3) with 40 teeth each. Control group used a visible light curing unit, XL 1000(3M Co., U.S.A) and experimental groups used argon laser($SPECTRUM^{TM}$). And then each group subdivided into two groups (A, B) according to filling materials. Subdivided A group used Fuji II LC(GC Co., Japan), B group used Vitremer(3M Co., U.S.A). The curing units and curing time of each group were as follows : Control group : visible light, 40 seconds Experimental group 1 Experimental group 2 Experimental group 3 : argon laser, 10 seconds : argon laser, 20 seconds : argon laser, 30 seconds The glass ionomer cements were bonded to dentin surface of each specimen. The specimens were stored in 100% relative humidity at 37"c for 7days. And then, the shear bond strength were measured by universal testing machine(Shimatzu Co. Japan) at crosshead speed of 5mm/min and 100kg in full scale and analyzed statistically. The following results were obtained : 1. Experimental group 2-A showed the highest shear bond strength with $9.87{\pm}1.24$ kgf and control group B showed the lowest shear bond strength with $4.08{\pm}0.78$ kgf(P<0.01). 2. The Fuji II LC showed higher shear bond strength with $9.49{\pm}1.24$ kgf than that of the Vitremer with $4.23{\pm}1.24$ kgf. There was significant difference between Fuji II LC and Vitremer(p<0.01). 3. There was no significant differences among experimental groups according to curing time induced by argon laser. 4. There was no significant differences between control group and experimental groups according to curing units.

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Development of Hybrid Fiber Reinforced Polymer Reinforcing Bars and Evaluation of the Bond Properties (하이브리드 FRP 보강근의 형상개발과 부착성능 평가)

  • Park, Ji-Sun;Park, Young-Hwan;You, Young-Jun;Kim, Keung-Hwan
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.11a
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    • pp.629-632
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    • 2006
  • The various rib geometry of hybrid fiber reinforced polymer (FRP) reinforcing bars were analyzed by finite element method. From the analysis result, two types of hybrid FRP reinforcing bars such as spiral and cross type with the same dimension of rib geometry were fabricated in this study. To evaluate the bond properties of them, direct pull-out test was performed. All testing procedures including specimens preparation, set-up of test equipments and measuring devices were made in accordance with the recommendations of CSA Standard S806-02. From the test results, it was found that cross type hybrid FRP reinforcing bars showed the highest bond strength than that of the others due to the higher relative rib area.

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DFT Conformational Study of Calix[6]arene: Hydrogen Bond

  • Kim, Kwang-Ho;Choe, Jong-In
    • Bulletin of the Korean Chemical Society
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    • v.30 no.4
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    • pp.837-845
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    • 2009
  • We have performed DFT calculations to investigate the conformational characteristics and hydrogen bonds of the calix[6]arene (1) and p-tert-butylcalix[6]arene (2). The structures of various conformers of 1 were optimized by using the B3LYP/6-31G(d,p) and /6-31+G(d,p) methods followed by single point calculation of MPW1PW91/ 6-31G(d,p). The relative stability of the conformers of 1 is in the following order: cone (pinched: most stable) > partial-cone > cone (winged) $\sim$ 1,2-alternate $\sim$ 1,2,3-alternate > 1,4-alternate > 1,3-alternate > 1,3,5-alternate. The structures of different conformers of 2 were optimized by using the B3LYP/6-31G(d,p) method followed by single point calculation of MPW1PW91/6-31G(d,p). The relative stability of the conformers of 2 is in the following order: cone (pinched) > 1,2-alternate > cone (winged) > 1,4-alternate $\sim$ partial-cone > 1,2,3-alternate > 1,3,5alternate > 1,3-alternate. One of the important factors affecting the relative stabilities of the various conformers of the 1 and 2 is the number and strength of the intramolecular hydrogen bonds.

Experimental Study on Evaluation of Abrasion Resistance of Concrete Irrigation Facilities (콘크리트 수리구조물의 수중마모저항성 평가기술에 관한 실험적 연구)

  • Kim, Meyongwon
    • Journal of The Korean Society of Agricultural Engineers
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    • v.60 no.3
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    • pp.123-133
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    • 2018
  • The purpose of this paper is to propose an experimental method to evaluate the resistance of abrasion about 24 MPa, 27 MPa, and 30 MPa compressive strength. These strength are used in the design and construction of concrete hydraulic structures in Korea. The mixing ratios of the ready mixed concrete strengths were investigated countrywide and set the representative mixture proportion ratios of the nine mixed types of OPC, FA and BFS. After making and curing the test specimens, the underwater abrasion test was performed. ASTM C 1138 International Standard was used to fabricate the test equipment, and the surface abrasion resistance of the specimen was tested using the test equipment. In the case of OPC, the 30% abrasion resistance improvement effect was observed at 72 hours as the water-binder ratio decreased. That was reason the coated cement bond strength of the specimen was strong. In the case of BFS and FA, it was improved by 9.9% and 3.8%, respectively, at 72 hours as the water-binder ratio decreased. It was due to the characteristics of the latent hydraulic and pozzolanic reactions. Generally, the relative abrasion resistance of concrete can be evaluated at 24 hours. However, in case of low strength (under 24 MPa), the surface mortar layer wears much faster at the first 12 hours, so it can be considered to evaluate the relative abrasion loss rate at this point.

A COMPARATIVE STUDY OF THE PHYSICOCHEMICAL PROPER TIES AND BOND STRENGTH TO METAL BETWEEN THE REGULAR OPAQUE POWDER AND CORE POWDER (도재소부전장금관용 Opaque 분말과 도재전장관용 core 분말의 물리화학적 성질 및 금속과의 결합력에 대한 비교연구)

  • Lim, Jang-Seop;Chung, Chang-Mo;Jeon, Young-Chan
    • The Journal of Korean Academy of Prosthodontics
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    • v.35 no.1
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    • pp.144-164
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    • 1997
  • The purpose of this study were to investigate the chemical composition, mean particle size, linear thermal expansion coefficient and metal-bonding strength of the regular opaque powder and core powder. In this study, 4 types of ceramic powders, namely Duceram Jacket Opaque powder, Duceram Opaque powder, Vita Hi-Ceram powder, Vita VMK Paint On-88 powder were used. Chemical composition was evaluated by EDS(Energy Dispersive X-ray Spectrophotometer, Oxford QX-2000, England), particle size was measured by MALVERN Instruments(MALVERN Instruments SB. OC., U.S.A.. ad linear thermal expansion coefficient was measured by dilatometer(Motoyama, Japan). Bond strength was measured by the Universal tsting machine(Istron Co., Ltd., U.S.A.). The Results were as follows : 1. Through recognition of the relative difference in chemical composition between the core powder and the regular opaque powder, the difference in the proportion of $Al_2O_3$ in each type of material is demonstrated ; Duceram Jaket Opaque powder : 30.16%, Duceram Opaque powder : 16.60%, Vita Hi-Ceram : 63.64%, Vita VMK Paint-On 88 : 16.16%. 2. There was no significant difference in the proportion of metal-bonding materials between the core powder and the regular opaque powder. 3. In the regular opaque powder, alkaline materials were incoporated in order to increase the coefficient of thermal expansion. 4. In the particle size analysis, there was no significant difference in mean particle size or in the particle size distribution between the core powder and the regular opaque powder. 5. In the thermal expansion test for temperature range of $25-600^{\circ}C$, the regular opaque powder had higher coefficient of thermal expansion than that of core powder. 6. In the 4 point flexural bending test, there was no statistically significant difference in the mean bond strength between the core powder and the opaque powder among the Duceram products.

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A STUDY ON THE RELATIVE SHEAR BOND STRENGTHS OF SOME ADHESIVE RESTORATIVE MATERIALS TO PRIMARY ENAMEL AND DENTIN (수종 접착성 수복재의 유치 법랑질과 상아질에 대한 상대적 접착력의 비교연구)

  • Kim, Seung-Mee;Kim, Shin;Jeong, Tae-Sung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.27 no.2
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    • pp.237-245
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    • 2000
  • For the purpose of comparing the bond strengths of some tooth adhesive restoration materials on primary enamel and dentin, 4 kinds (7 brands) of restorative materials including a composite resin (Z 100), a conventional glass ionomer cement (Chem-Flex), 2 brands of resin-modified glass ionomer cements (Fuji II LC-I, Vitremer), and 3 brands of compomers(Dyract AP, F2000, Compoglass) were investigated using UTM for measuring the shear bond strengths. Additionally the failure modes were examined by histologically observing the fractured surfaces of each specimen. The following results were obtained. 1. The shear bond strengths of Z 100 to the primary enamel were higher than those of other experimental materials except Fuji II LC-I, which showed significantly higher bond strength than Chem-Flex or Vitremer (P<0.05). 2. The shear bond strengths of Z 100 to the primary dentin were higher than those of other experimental materials except Dyract AP and Fuji II LC-I, both of which showed significantly higher shear strength than Chem-Flex or Vitremer (P<0.05). 3. The shear bond strengths of all restorative materials except Dyract AP showed relatively higher values to enamel surface than to dentin surface. In Dyract AP, the reverse was true significantly. 4. All materials examined showed cohesive failures except some Chem-Flex and Vitremer, which showed adhesive failures.

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Processing of Silica-Bonded Silicon Carbide Ceramics

  • Chun, Yong-Seong;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.43 no.6 s.289
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    • pp.327-332
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    • 2006
  • The effect of the processing parameters on the sintered density and strength of silica-bonded SiC (SBSC) ceramics was investigated for three types of batches with different particle sizes. The SBSC ceramics were fabricated by an oxidation-bonding process. The process involves the sintering of powder compacts in air so that the SiC particles bond to each other by oxidation-derived $SiO_2$ glass or cristobalite. A finding of this study was that a higher flexural strength was obtained when the starting powder was smaller. When a ${\sim}0.3_{-{\mu}m}$ SiC powder was used as a starting powder, a high strength of $257{\pm}42\;MPa$ was achieved at a relative density of ${\sim}80%$.