• Title/Summary/Keyword: reference range

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Simultaneous Determination of (-)-Menthone and (-)-Menthol in Menthae Herba by Gas Chromatography and Principal Component Analysis

  • Kim, Jung-Hoon;Seo, Chang-Seob;Shin, Hyeun-Kyoo
    • Natural Product Sciences
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    • v.16 no.3
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    • pp.180-184
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    • 2010
  • The simple and accurate method was established for the simultaneous determination of (-)-menthone and (-)-menthol in Menthae herba obtained from Korea and China. A quantitative analysis was performed with a gas chromatography-flame ionization detector and reference compounds were separated on a capillary HP-Innowax column (30 m $\times$ 0.23 mm, 0.50 ${\mu}m$, Agilent, MA, USA). The correlation coefficients of the compounds showed good linearity ($r^2$ > 0.9997) over the linear range. The precision, repeatability and stability showed less than 1.7% of relative standard deviation (RSD) values for two compounds. Recovery rates were within the range of 95.72 - 103.76%. The method was applied successfully to analyze 15 samples of Menthae herba and achieved sufficient and specific separation of reference compounds. The principal component analysis (PCA) exhibited the classification of 15 samples according to their locations of origin.

A temperature and supply insensitive CMOS current reference using a square root circuit (제곱근 회로를 이용한 온도와 공급 전압에 둔감한 CMOS 정전류원)

  • 이철희;손영수;박홍준
    • Journal of the Korean Institute of Telematics and Electronics C
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    • v.34C no.12
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    • pp.37-42
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    • 1997
  • A new temperature and supply-insensitive CMOS current reference circuit was designed and tested. Te temperature insensuitivity was achieved by eliminating the mobility dependence term through the multiplication of two current components, one which is proportional to mobility and the other which is inversely proportional to mobility, by using a newly designed CMOS square root circuit. The CMOS sqare root circuit was derived from its bipolar counterpart by operating the MOS transistors in the subthreshold region. The supply insensitivity was achieved by using an internal voltage generator. Te test chip was designed ans sent out for fabrication by using a 2.mu.m double-poly double-metal n-well CMOS technology. When an external voltage source was used for the square root circuit, the maximum variation and the average temperature sensitivity were measured to be 3% and 21.4ppm/.deg.C, respectively, for the temperature range of -15~130.deg.C. The maximum current variation with supply voltage was measured to be 3% within the commerical supply voltage range of 4.5~5.5V at 30.deg. C.

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Design of Temperature Stable Pulse Width Modulation Circuit Using CMOS Process Technology (CMOS 공정을 이용하는 동작온도에 무관한 펄스폭 변조회로 설계)

  • Kim, Do-Woo;Choi, Jin-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.186-187
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    • 2007
  • In this work, a temperature stable PWM(Pulse width modulation) circuit is proposed. The designed PWM circuit has a temperature dependent current source and a temperature independent voltage to compensate electrical characteristics with operating temperature. The variation of driving current is from about 4% to -6% in the temperature range $0^{\circ}C\;to\;70^{\circ}C$ compared to the current at the room temperature. The variation of bandgap voltage reference is from about 1.3% to -0.2% with temperature when the supply voltage is 3.3 volts. From simulation results, the variation of output pulse width is less than from 0.86% to -0.38% in the temperature range $0^{\circ}C\;to\;70^{\circ}C$.

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Nonparametric Ground-Motion Evaluation of Shear-Wave Fourier Spectra (비매개변수법에 의한 주파수별 스펙트럼감쇠 평가)

  • 연관희;박동희;장천중
    • Proceedings of the Earthquake Engineering Society of Korea Conference
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    • 2003.09a
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    • pp.20-27
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    • 2003
  • The nonparametric method was employed to obtain detailed broadband attenuation characteristics of horizontal Fourier spectra without generally assigned constraint that derived path terms be zeros at a reference distance. Instead, path terms fer a reference distance were obtained based on the physical phenomenon that the seismic phase is stable over the hypocentral distance range from 200km to 400km so that the Q-values evaluated at several distances inside that region should be the same. The inverted path terms show three distinct linear regions roughly divided by hypocentral distances at 65km and 115km. Also complex behavior at the near distance range below 100km was revealed which can not be properly fitted by combination of single $Q_{0}$ $f^{η}$ model and any geometrical spreading models.s.

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Validation of Radioanalytical Techniques for Nuclear Waste Characterisation

  • Warwick, Phillip E.
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.17 no.4
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    • pp.363-373
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    • 2019
  • Waste characterisation associated with nuclear site decommissioning relies on radiochemical analysis of a diverse range of sample types, requiring extensive validation of analytical techniques using matrix-matched materials. The absence of relevant reference materials has hindered robust method development and validation. The paper discusses how method validation in support of nuclear waste characterisation can be achieved without using reference materials. The key stages in an analytical procedure are evaluated and a multi-stage approach is proposed with the ultimate aim of determining an operational envelope for an analytical procedure.

Quantitative Analysis of Chloride by Heteronuclear Electronic Reference NMR Method

  • Lee, Sueg-Geun
    • Journal of the Korean Magnetic Resonance Society
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    • v.11 no.2
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    • pp.115-121
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    • 2007
  • A new quantitative analysis of chloride by the HERETIC NMR method which does not need internal or external references was described. The results showed that the use of HERETIC peak corresponding $500\;{\mu}g/mL$ of chloride calibration showed less than 4 % standard deviations from 50 to $5000\;{\mu}g/mL$ range of chloride concentrations.

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Simultaneous Faults Detection and Isolation Using Null Space Components of Faults for INS Sensor Redundancy

  • Yang, Cheol-Kwan;Shim, Duk-Sun
    • 제어로봇시스템학회:학술대회논문집
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    • 2002.10a
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    • pp.32.4-32
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    • 2002
  • We consider inertial navigation system (INS) sensor redundancy and propose a method which uses singular value decomposition to detect and isolate faults when even two sensors have faults simultaneously. When redundant sensor configuration is given, such as symmetric configuration in INS, the range space and null space of configuration matrix are determined. We use null space of configuration matrix and define 21 reference fault vectors which include 6 one-fault vectors and 15 two-fault vectors. Measurements are projected into null space of measurement matrix and compared with 21 normalized reference fault vectors, which determines fault detection and isolation.

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A linear systolic array based architecture for full-search block matching motion estimator (선형 시스토릭 어레이를 이용한 완전탐색 블럭정합 이동 예측기의 구조)

  • 김기현;이기철
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.21 no.2
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    • pp.313-325
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    • 1996
  • This paper presents a new architecture for full-search block-matching motion estimation. The architecture is based on linear systolic arrays. High speed operation is obtained by feeding reference data, search data, and control signals into the linear systolic array in a pipelined fashion. Input data are fed into the linear systolic array at a half of the processor speed, reducing the required data bandwidth to half. The proposed architecture has a good scalability with respect to the number of processors and input bandwidth when the size of reference block and search range change.

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A Study on the Compensating System for the Acoustic Characteristics Caused by the Variation of Distance from Sound Source to Microphone (음원과 마이크로폰 사이의 거리변화에 의한 음향 특성 보정에 관한 연구)

  • Jeoung, Byung-Chul;Choe, Yoon-Sik
    • The Journal of the Acoustical Society of Korea
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    • v.31 no.3
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    • pp.197-204
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    • 2012
  • In this thesis, studied the method to minimize the changes in frequency response and level due to the variation of the distance from the source to the microphone. selecting three microphones (omni directional, cardioid, super cardioid) which are being used generally, frequency responses were measured in accordance with the distance changes. Gotten the difference from the reference as the result of measurement, changed responses for each frequency range were compensated in comparison of the original human vocal source. In low frequency range, the low frequency boost caused by the proximity effect and decrease in accordance with the distance were compensated. The variation in mid-frequency range is comparatively small, however since the mid-range is the most important part of the human vocal signal, were compensated the mid-frequency range in comparison of the reference. The human vocal signal variation in high frequency range is extremely small and the high frequency is compensated close to the original source without difficulty. Understanding the microphone characteristics and compensations, this study showed that the response can be maintain among the change of the distance from the source to the microphone.

Wide-range Speed Control Scheme of BLDC Motor Based on the Hall Sensor Signal

  • Lee, Dong-Hee
    • Journal of Power Electronics
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    • v.18 no.3
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    • pp.714-722
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    • 2018
  • This paper presents a wide-range speed control scheme of brushless DC (BLDC) motors based on a hall sensor with separated low- and normal-speed controllers. However, the use of the hall sensor signal is insufficient to detect motor speed in the low-speed region because of low sensor resolution and time delay. In the proposed method, a micro-stepping current control method according to the torque angle variation is presented. In this mode, the motor current frequency and rotating angle are determined by the reference speed without the actual speed fed by the hall sensor. The detected torque angle is used to adjust the current value in a limited band to control the current value in accordance with the load. The torque angle is detected exactly at the changing point of the hall sensor signal. The rotor can follow the rotating flux with the variable torque angle. In a normal speed range, the conventional vector control scheme is used to control the motor current with a PI speed controller using the hall sensor. The torque characteristics are analyzed on the basis of the back EMF and current shape. To adopt the vector control scheme, the continuous rotor position is estimated by the measured speed and hall sensor position. At the mode changing point between low and normal speed range, the proper initial current command and reference rotor position are calculated. The calculated current command can reduce the torque ripple during transient mode. The proposed method is simple but effective in extending the speed control range of a conventional BLDC motor with hall sensor without the need for a high-resolution encoder. The effectiveness of the proposed method is verified by various experiments on a practical BLDC motor.