• 제목/요약/키워드: reference calibration

검색결과 458건 처리시간 0.026초

Building Calibration Curve for Py-GC/MS Analysis of SBR/BR Blend Rubber Compounds

  • Chae, Eunji;Choi, Sung-Seen
    • Elastomers and Composites
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    • 제55권4호
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    • pp.281-288
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    • 2020
  • A calibration curve is needed to determine the SBR and BR blend ratio of SBR/BR blend rubber compounds using pyrolysis-gas chromatography/mass chromatography (Py-GC/MS) or Py-GC. In general, a calibration curve is obtained using reference SBR/BR vulcanizates with various blend ratios. In this study, the calibration curves were obtained using reference samples made of rubber solutions and were compared to those plotted using the reference SBR/BR vulcanizates. Calibration curves using variations of 1,3-butadiene/styrene, 4-vinylcyclohexene (VCH)/styrene, 2-phenylpropene (PhP)/butadiene, PhP/VCH, 4-phenylcyclohexene (PhCH)/butadiene, and PhCH/VCH ratios with the BR content were examined for the suitability. We found that the calibration curves obtained using the mixed rubber solution references (1,3-butadiene/styrene and PhP/butadiene) could replace those constructed using the reference SBR/BR vulcanizates. The calibration curves of 1,3-butadiene/styrene and PhP/butadiene obtained using the raw references can be used for the determination of the SBR/BR blend ratios by applying some correction factors.

백금저항온도센서를 이용한 국가교정기관의 교정능력 평가 및 실험방법 (Experimental method and evaluation of the calibration capability for the national calibration centers using the platinum resistance temperature sensors)

  • 감기술;유성호;김성민;이인식
    • 센서학회지
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    • 제14권4호
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    • pp.231-236
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    • 2005
  • Calibration capability was evaluated using the reference-grade platinum resistance thermometer (PRT) in the temperature range of $-50^{\circ}C$ to $250^{\circ}C$ for the national calibration centers. The reference-grade PRT was calibrated at the several fixed points, which was composed by the freezing points of Sn, In, the melting point of Ga and the triple point of water and Hg, before and after the round-robin test (RRT) experiments. The temperature scale of reference-grade PRT was compared to the local standard PRT's using the system of the national calibration centers. $E_{n}$ values was calculated by the temperature difference between the reference-grade PRT and the local standard PRT, and the best measurement capability. Finally, the capability of the national calibration centers was evaluated by the $E_{n}$ values.

Calibration of digital wide-range neutron power measurement channel for open-pool type research reactor

  • Joo, Sungmoon;Lee, Jong Bok;Seo, Sang Mun
    • Nuclear Engineering and Technology
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    • 제50권1호
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    • pp.203-210
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    • 2018
  • As the modernization of the nuclear instrumentation system progresses, research reactors have adopted digital wide-range neutron power measurement (DWRNPM) systems. These systems typically monitor the neutron flux across a range of over 10 decades. Because neutron detectors only measure the local neutron flux at their position, the local neutron flux must be converted to total reactor power through calibration, which involves mapping the local neutron flux level to a reference reactor power. Conventionally, the neutron power range is divided into smaller subranges because the neutron detector signal characteristics and the reference reactor power estimation methods are different for each subrange. Therefore, many factors should be considered when preparing the calibration procedure for DWRNPM channels. The main purpose of this work is to serve as a reference for performing the calibration of DWRNPM systems in research reactors. This work provides a comprehensive overview of the calibration of DWRNPM channels by describing the configuration of the DWRNPM system and by summarizing the theories of operation and the reference power estimation methods with their associated calibration procedure. The calibration procedure was actually performed during the commissioning of an open-pool type research reactor, and the results and experience are documented herein.

풍력발전기 성능실증을 위한 단지교정 방법 (Site Calibration for the Wind Turbine Performance Evaluation)

  • 남윤수;유능수;이정완
    • 산업기술연구
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    • 제22권A호
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    • pp.49-57
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    • 2002
  • The accurate wind speed information at the hub height of a wind turbine is very essential to the exact estimation of the wind turbine power performance testing. Several methods on the site calibration, which is a technique to estimate the wind speed at the wind turbine's hub height based on the measured wind data using a reference meteorological mast, are introduced. A site calibration result and the wind resource assessment for the Taekwanryung test site are presented using a one-month wind data from a reference meteorological mast and a temporal mast installed at the site of wind turbine. From this analysis, it turns out that the current location of the reference meteorological mast is wrongly determined, and the self-developed codes for the site calibration are working properly. Besides, an analysis on the uncertainty allocation for the wind speed correction using site calibration is performed.

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표준준기에 의한 일사계 교정 (Thermopile Radiometer Calibration Using Reference Instrument)

  • 조덕기;윤창열;김광득;강용혁
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2010년도 춘계학술대회 초록집
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    • pp.199.2-199.2
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    • 2010
  • The main purpose of the calibration procedure is to perform a one to one comparison of the reference pyranometer and the test pyranometer. In order to achieve this, both pyranometers need to be exposed to exactly the same irradiance, under the same circumstances. There are a number of error sources that could result in a wrong measurement. Most importantly Lamp instability, pyranometer offsets, thermal offsets of junctions, voltmeter offset, voltmeter instability, reference pyranometer instability, tilting of the pyranometers and differences in sensor height. Another sun-disc calibration procedure compares the computed vertical component of the direct irradiance as measured by a pyranometer with that measured by the pyranometer to be calibrated. Readings are taken with the levelled pyranometer on a clear day. Firstly the global irradiance and then the diffuse component are measured. Simultaneously measurement of direct irradiance is made with the pyrheliometer. The ways of performing the calibration and the subsequent calculation have been chosen such that the effect all these error sources has been eliminated as much as possible.

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CHARACTERISTICS OF THE KAERI NEUTRON REFERENCE FIELDS FOR THE CALIBRATION OF NEUTRON MONITORING INSTRUMENTS

  • Kim, Bong-Hwan;Kim, Jang-Lyul;Chang, Si-Young;Cho, Gyu-Seong
    • Journal of Radiation Protection and Research
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    • 제26권3호
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    • pp.243-248
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    • 2001
  • Neutron reference fields of Korea Atomic Energy Research Institute (KAERI) for calibrating neutron measuring devices to be used in radiation workplace monitoring consist of two kinds of neutron spectra, the direct and the scattered neutron fields, which are produced by using radionuclide neutron sources, 252Cf and 241AmBe sources. Necessary parameters for calibration such as the anisotropy factor of each neutron source and the room-scattered fraction of some neutron surveymeters in the KAERI calibration facility were determined by calculation or measurement. Spectral measurement of scattered neutron fields were performed at each reference calibration point using a Bonner Multi-sphere Spectrometer (BMS) and the dosimetric quantities for calibration also estimated from the neutron energy spectra which were unfolded using the BUNKI code.

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검량보정 검증의 실험적 적합성에 대한 연구 -치료적 약물검사를 중심으로- (An Empirical Validation Study for Calibration Verification in TDM Test)

  • 장상우;김남용;최호성;박용원;추경복;윤근영;박병옥
    • 대한임상검사과학회지
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    • 제37권1호
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    • pp.1-7
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    • 2005
  • The purpose of this study was to verify (i) a consistent calibration verification for the assessment of method linearity and (ii) calibration agreement with calibration settings. We validated calibration verification through method linearity with different lot number of individual calibrators that span the working range for 9 tests except salicylate with control sample in test. We evaluated that it covered broad analyte range to assay from near zero to the top of the measuring range with 5 or 6 points every three times for 10 analytes in TDM test. Target values were plotted on X-axis with assigned or observed values on the Y-axis. Working range were as follows. Calibration verification of the measuring range (maximum to minimum values) has been validated asetaminophen 0.1 to $304.6_{\mu}g/mL$, salicylate 0 to $1005_{\mu}g/mL$, valproic acid 3.2 to $154.19_{\mu}g/mL$, digoxin 0.17 to 5.65 ng/mL, vancomycine 1.3 to $80.51_{\mu}g/mL$, carbarmazepine 0.1 to $22.3_{\mu}g/mL$, phenytonin 0.6 to $40.21_{\mu}g/mL$, theophyline 0.2 to $40.21_{\mu}g/mL$, primidone 0 to $24.07_{\mu}g/mL$, phenobarbital 0.6 to $60.0_{\mu}g/mL$. Drawing a straight line through five or six points of these data showed good linearity. We are sure that it is important to assess the calibration verification of a test method to ascertain the lowest and highest test results that are reliable.

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Calibration for Color Measurement of Lean Tissue and Fat of the Beef

  • Lee, S.H.;Hwang, H.
    • Agricultural and Biosystems Engineering
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    • 제4권1호
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    • pp.16-21
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    • 2003
  • In the agricultural field, a machine vision system has been widely used to automate most inspection processes especially in quality grading. Though machine vision system was very effective in quantifying geometrical quality factors, it had a deficiency in quantifying color information. This study was conducted to evaluate color of beef using machine vision system. Though measuring color of a beef using machine vision system had an advantage of covering whole lean tissue area at a time compared to a colorimeter, it revealed the problem of sensitivity depending on the system components such as types of camera, lighting conditions, and so on. The effect of color balancing control of a camera was investigated and multi-layer BP neural network based color calibration process was developed. Color calibration network model was trained using reference color patches and showed the high correlation with L*a*b* coordinates of a colorimeter. The proposed calibration process showed the successful adaptability to various measurement environments such as different types of cameras and light sources. Compared results with the proposed calibration process and MLR based calibration were also presented. Color calibration network was also successfully applied to measure the color of the beef. However, it was suggested that reflectance properties of reference materials for calibration and test materials should be considered to achieve more accurate color measurement.

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다른 선폭들로 구성된 격자형 교정판을 이용한 간단한 카메라 교정 시스템의 개발 (A development of the simple camera calibration system using the grid type frame with different line widths)

  • 정준익;최성구;노도환
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 1997년도 한국자동제어학술회의논문집; 한국전력공사 서울연수원; 17-18 Oct. 1997
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    • pp.371-374
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    • 1997
  • Recently, the development of computer achieves a system which is similar to the mechanics of human visual system. The 3-dimensional measurement using monocular vision system must be achieved a camera calibration. So far, the camera calibration technique required reference target in a scene. But, these methods are inefficient because they have many calculation procedures and difficulties in analysis. Therefore, this paper proposes a native method that without reference target in a scene. We use the grid type frame with different line widths. This method uses vanishing point concept that possess a rotation parameter of the camera and perspective ration that perspect each line widths into a image. We confirmed accuracy of calibration parameter estimation through experiment on the algorithm with a grid paper with different line widths.

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