• Title/Summary/Keyword: rapid solidification

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Characterization of the structural defects in the dendritic web-grown silicon ribbon (Dendritic web으로 성장된 규소 결정속의 결함 규명)

  • Kim, Young-Kwan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.3
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    • pp.276-283
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    • 1994
  • The dislocation configuration in web-grown silicon ribbon was investigated using chemical etching techniques. The presence of dislocation loops on twin planes is observed and acounted for by self-interstitial condensation. The interstitials were either quenched in, due to the rapid cooling of the ribbon from the solidification temperatures, or produced by oxide precipitation on the twin plane. Very large faulted loops of mm size were also observed.

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Automatic Support Structure Generation for Stereolithographic Rapid Prototyping (SLA를 이용한 신속시작작업을 위한 지지대 자동생성 시스템의 개발)

  • Hur, Junghoon;Lee, Kunwoo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.10
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    • pp.3068-3078
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    • 1996
  • stereolithography is a process used to rapidly produce polymer components directly from a computer representation of the part. There are several considerations to be made for the efficient use of the process. Especially, the necessity of support structures, which prevent the part from warping, sagging, or parachuting and toppling as the elevator moves up and down in the resin, is one concern. After solidification, the support structures must by removed in the end. Bacause this post-treatment process is often performed manually, the more the support structures, the more it increases the finishing operations. Especially for a complicated part, the removal operations may be difficult, take so much time, and even reduce the accuracy of the product. Thus it is important to efficiently generate the efficient support structure for each part geometry. This paper proposes a procedure to automatically generate the supprot structures focused on accuracy, efficiency, convenience, and generation speed.

Fabrication of Graded-Boundary Ni/Steel Material by Laser Beam (레이저빔에 의한 조성구배계면 Ni/Steel 재료의 제조)

  • 안재모;김도훈
    • Laser Solutions
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    • v.2 no.1
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    • pp.22-29
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    • 1999
  • This work was carried out as a fundamental experiment to fabricate a Graded-Boundary Ni/Steel material using a laser beam. A Ni sheet was placed on a steel substrate, and then a series of high power $CO_2$ laser beams were irradiated on the surface in order to produce a homogeneous alloyed layer. The processing parameters were : 4 ㎾ laser power, 2m/min traverse speeds, -2mm defocuing, 17 l/min sheiding gas flow rates. The sequential repetition of the laser surface alloying treatment up to 4 times, resulted in about 5mm thick of fair compositional gradient systems. In order to determine the microstructure, phase and compositional profiles in this material, optical microscopy, XRD and EDS were used. The compositions varied from 66% to 0% for Ni and 34% to 100% for Fe in this material The microstructures were typical morphologies of rapid solidification and solid-state cooling. Since compressive stress was formed in the heat affected region due to martensitic transformation, while relative tensile stress was developed in the alloyed region, cracks were formed between the alloyed region and the substrate region.

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High Temperature Deformation Behavior of Rapid-Solidification Processed Al-18Si Alloy (급냉응고된 과공정 Al-Si합금의 고온변형특성에 관한 연구)

  • 김성일
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2000.04a
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    • pp.183-186
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    • 2000
  • The high temperature deformation behavior of spray-formed Al-19wt%Si-1.87wt%Mg-0.085wt.%Fe alloy was studied by torsion testing in the strain rate range of 0.001-1 sec-1 and in the temperature range of 300-500 $^{\circ}C$. The relationship between stress temperature and strain rate is expressed using the Power law. the behavior of dynamic recrystallization is showed in 300-35$0^{\circ}C$, 1-0.1sec-1 and the behavior of dynamic recovery is showed in 450-50$0^{\circ}C$, 0.01-0.001sec-1 The size of Si particles is mall when the temperature is low and the strain rate is high. The strain rate sensitivity(m) and the apparent activation energy(Q) indicate the dependence on strain rate and temperature for flow stress respectively. The hot ductility is high when m is high and Q is low. The maps of strain rate sensitivity and apparent activation energy suggest the optimum processing conditions.

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Materials Properties of Gas Atomized and Extruded Mg-Zn-Y Alloys (가스분무 Mg-Zn-Y 합금분말 및 압출재의 특성)

  • Chae, Hong-Jun;Lee, Jin-Kyu;Bae, Jung-Chan;Kim, Taek-Soo
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.427-431
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    • 2006
  • Mg-4.3Zn-0.7Y (at%) alloy powders were prepared using an industrial scale gas atomizer, followed by warm extrusion. The powders were almost spherical in shape. The microstructure of atomized powders and those extruded bars was examined using Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscope (EDS) and X-ray Diffractometer (XRD). The grain size of the powders was coarsen as the initial powder size increased. After the extrusion, the grain size became fine due to the severe plastic deformation during the extrusion with the ratio of 10:1. Both the ultimate strength and elongation were enhanced with the decrease of initial particle size.

The Application of Computer Simulation, Industrial CT and DLS RP for the rapid development of casting pilot models (신속한 주물 시제품 개발을 위한 전산모사 기술과 산업용 단층촬영기 및 쾌속표형기의 적용)

  • Yoo S.M.;Lim C.H.;Cho I.S.;Choi J.K.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.195-196
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    • 2006
  • Direct laser sintering (DLS) technology for the resign coated sand is one of attractive technologies to produce molds and cores for the foundry industry rapidly and cost effectively. The objective of this case study is to develop casting pilot models using computer simulation technology, DLS RP machine and industrial computed tomography. The proposed casting design was verified by the Z-Cast software in the fields of fluid flow and solidification during the casting process. Casting parts with aluminum alloy using the post-curing treated sand moulds and cores are accurate to dimension and defect free.

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ELA Poly-Si과 SLS Poly-Si에서 Boron Activation에 관한 연구

  • Hong, Won-Ui;No, Jae-Sang
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.376-376
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    • 2012
  • 본 연구는 Poly-Si에 이온 주입된 Boron의 Activation 거동을 연구하고자 SLS (Sequential Lateral Solidification) Poly-Si과 ELA (Excimer Laser Annealing) Poly-Si의 활성화 거동을 비교 분석하였다. SLS 및 ELA 결정화 방법으로 제조된 Poly-Si을 모재로 비 질량 분리 방식의 ISD (Ion Shower Doping) System을 사용하여 2.5~7.0 kV까지 이온주입 하였다. 이온주입 후 두 가지의 열처리 방법, 즉, FA 열처리(Furnace Annealing)와 RTA 열처리(Rapid Thermal Annealing)를 사용하여 도펀트 활성화 열처리를 수행하고 이온주입 조건 및 활성화 열처리 방법에 따른 결함 회복 및 도펀트 활성화 거동의 변화를 관찰하였다. TRIM-code Simulation 결과 가속 이온 에너지와 조사량이 증가 할수록 이온주입 시 발생하는 결함의 양이 증가하는 것을 정량적으로 계산하였다. 실험 결과 결함의 양이 증가 할수록 Activation이 잘되는 것을 관찰할 수 있었다. SLS Poly-Si에 비하여 ELA Poly-Si의 경우 도펀트 활성화 열처리 후 활성화 효율이 높게 나타났다. 본 결과는 Grain Boundary의 역할과 밀접한 관계가 있으며 간단한 정성적인 Model을 제시하였다. 활성화 효율의 경우 RTA 열처리 시편이 FA 시편에 비하여 높은 것이 관찰되었다. 본 결과는 열처리 온도 및 시간에 따라 변화하는 Boron의 특이한 활성화 거동인 Reverse Annealing 효과에 기인하는 것으로 규명되었다.

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Development of thermoelectric semiconductor material by rapid solidification process (급속응고법에 의한 열전반도체 재료 개발)

  • 홍순직;천병선;이윤석
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2002.11a
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    • pp.80-80
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    • 2002
  • Bi-Te게 열전재료는 200~400K 정도의 저온에서 에너지 변환 효율이 가장 높은 재료로써 열전냉각, 발전재료 등에 응용하기 위하여 제조방법 및 특성에 관한 많은 역구가 진행되어 왔다. 현재 산업화에 응용되고 있는 일방향응고법은 기계적 강도가 약하여 회수 율이 낮으며, 결정을 성장시키는데 비교적 장시간을 필요로 하기 때문에 제조 단가가 비싸다. 따라서 이와 같은 문제점을 보완하기 위하여 합금설계 및 가공공정에 대한 연구가 활발히 진행되고 있다. 이에 본 연구에서는 가스분사법을 이용하여 용질원자 편석감소, 고용도의 증가, 균일고용체 형성, 결정립 미세화 등 급속응고 장점을 이용하여 화학적으로 균일한 BI-TerP열전재료 분말을 제조하고, 열간압출 가공을 통하여 이방성의 향상과 함께 미세한 결정립으로 우수한 기계적 강도를 얻을 수 있도록 제조된 분말을 압출 가공하여 열전소자의 기계적 성질과 열전특성을 연구하였다. 그 결과 급속응고 및 압출 공정을 이용한 본 연구에서는 $10\mu\textrm{m}$이하의 미세한 조직과 함께 압출공정을 통하여 이방성을 향상시켰으며, 열전소자는 $2.5{\times}10^{-3}/K$이상의 Figure of merit값을 나타내는 우수한 열전특성을 나타냈다.

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Formation and Thermal Decomposition of a Quasicrystalline Phase in Al-Fe-Mo Alloys (Al-Fe-Mo 합금에서 준결정상의 생성 및 열분해에 관한 연구)

  • Kim, Suk Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.6
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    • pp.362-368
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    • 2005
  • Formation and thermal stability of a quasicrystalline phases in Al-Fe-Mo alloys were investigated by means of melt-spinning process and subsequent heat treatment test. Thermal decomposition and phase transformation process of the as-spun alloys were studied using X-ray diffraction and electron microscopy. The melt-spun Al-Fe-Mo alloys contained an icosahedral quasicrystalline phase with a quasilattice constant of 0.457 nm. Icosahedral phase formed at a composition of $Al_{82.5}Fe_{14}Mo_{3.5}$ as a metastable phase during rapid solidification was transformed into the stable crystalline phases, cubic 1/0 approximant and monoclinic ${\lambda}$-phase, upon heating. A metastable icosahedral and cubic(a = 0.93 nm) phases in as-spun $Al_{65}Fe_{20}Mo_{15}$ alloy were decomposed into two cubic(a = 0.62, 0.31 nm) phases by heat treatment.

Cu-based Bulk Amorphous Alloys in the Cu-Zr-Ti-Ni-Pd System (Cu-Zr-Ti-Ni-Pd계 비정질 벌크합금의 형성과 성질)

  • Kim, Sung-Gyoo;Bae, Cha-Hurn
    • Journal of Korea Foundry Society
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    • v.22 no.6
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    • pp.304-308
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    • 2002
  • The new Cu-Zr-Ti-Ni-Pd amorphous alloy system has been introduced and manufactured using melt-spinning and Cu-mold die casting methods. Amorphous formability, the supercooled liquid region before crystallization and mechanical properties of the alloys were examined. The reduced glass transition temperature(Trg = Tg/Tm) and the supercooled liquid region(${\Delta}$Tx = Tx-Tg) of $Cu_{49}Zr_{30}Ti_{10}Ni_5Pb_6$ alloy were 0.620 and 57 K respectively. $Cu_{49}Zr_{30}Ti_{10}Ni_5Pb_6$ amorphous alloy was produced in the rod shape with 2mm diameter using the Cu-mold die casting. The hardness value of the amorphous bulk alloy was 432 DPN.