• Title/Summary/Keyword: quartz powder

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A Study on Development of a Liner Manufactured by Mine Wastes and Polymer (광산폐기물과 폴리머를 이용한 Liner 개발에 관한 연구)

  • 진호일
    • Economic and Environmental Geology
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    • v.33 no.2
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    • pp.139-146
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    • 2000
  • Development of an effective liner by utilization of the tailings frm the Imcheon mine and polymer has been tried. The tailings piled in the Imcheon mine, whose true specific gravity is about 2.86, are composed mainly of quartz, alkali-feldspar, muscovite and pyrite, and mostly (93.7% in volume) coarser than sand grain size (50${\mu}{\textrm}{m}$). Strength, leaching and permeability tests have been performed on the test specimens of polymer concrete manufactured with various mixing proportions of tailings, unsaturated polyester resins(UPR), calcium carbonates, stone powder sludges and granite soils. Polymer concrete specimens with stone powder sludges or granite soils as fillers and aggregates indicate 2.5 to 3 fold higher flexural and compressive strengths and lower permeabilities than those with calcium carbonates, which shows their usability as a waterproof liner. Also, the polymer concrete liner with stone powder sludge fillers is more advisable in aspects of utilization of waste sludges than that with other fillers.

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Synthesis of Carbon Nanotubes by Chemical Method at Warm Temperatures (탄소나노튜브의 중저온에서의 화학적 합성)

  • Ahn, Jung-Ho;Lee, Sang-Hyun;Kim, Yong-Jin;Chung, Byung-Sik
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.305-312
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    • 2006
  • Amorphous carbon nanotubes were synthesized by a reaction of benzene, ferrocene and Na mixture in a small autoclave at temperatures as low as $400^{\circ}C$. The resulting carbon nanotubes were short and straight, but their inner hole was filled with residual products. The addition of quartz to the reacting mixture considerably promoted the formation of carbon nanotubes. A careful examination of powder structure suggested that the nanotubes in this process were mainly formed by surface diffusion of carbon atoms at the surface of solid catalytic particles, not by VLS(vapor-liquid-solid) mechanism.

An Experimental Study on the Strength Properties of Reactive Powder Concrete Using copper slag aggregate (동제련 슬래그를 골재로 사용한 반응성 분말 콘크리트(RPC)의 강도 특성에 관한 실험적 연구)

  • Park, Min-Su;Lee, Seung-Hoon;Kim, Young-Su
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.05a
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    • pp.278-279
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    • 2014
  • This study was performed an evaluation of mechanical properties of reactive powder concrete using copper slag. So, various RPC containing copper slag were made by replacement ratio of copper slag and different the curing condition and their mechanical properties were investigated. From the experimental results, slump flow using copper slag tends to increase with replacement ratio. And also, 30% of copper slag with quartz sand was found to have a compressive strength superior to that of plain.

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A study on th reaction between silicon in melt and carbon (용융상태에서의 silicon과 carbon의 반응에 관한 연구)

  • M.J. Lee;B.J. Kim;S.M. Kang;J.K. Choi;B.S. Jeon;Keun Ho Orr
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.4
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    • pp.336-346
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    • 1994
  • We studied the reaction between silicon and carbon. Silicon granules and silicon with 0.2 wt% carbon powders were prepared for sample and then they were heated up to the $1450^{\circ}C, 1550^{\circ}C, 1650^{\circ}C, 1700^{\circ}C$ and were dwelled 1 hr and 4 hrs, respectively. we studied the change of morphologies of molten silicon and the formation of SiC following the reaction withcarbon using optical microscope, SEM, and XRD. Above the melting point of silicon, oxygens are precipitated during the decomposition of quartz used crucible. SiO formed from the reaction between molten silicon and precipitated oxygen evaporated and made the surface defects. SiC were formed with the reaction between the unreacted carbon and molten silicon. Polytype of the SiC formed at the solidification interface was ${\alpha}-SiC$.

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Photoluminescence of Hexagonal Boron Nitride (h-BN) Film

  • Jin, Moon-Seog;Kim, Nam-Oh
    • Journal of Electrical Engineering and Technology
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    • v.5 no.4
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    • pp.637-639
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    • 2010
  • Hexagonal boron nitride (BN) films were prepared. The process involved, spraying BN powder-dispersed $H_3BO_4-BCl_3$-ethyl alcohol solution on quartz plates, and the drying off quartz plates before, and annealing at $1070^{\circ}C$ in a nitrogen atmosphere. The optical energy band gap of the BN films was 5.28 eV. Photoluminescence peaks with energies of 3.44, 3.16, 2.97, and 2.35 eV at 10 K were observed and analyzed. Accordingly, these have resulted from donor-acceptor pair recombinations.

Nanocomposite magnetic powder materials using mechanochemical Synthesis

  • Soh, Dae-Wha;Mofa, N.N.;Keteguenov, T.A.;Mansurov, Z.A.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.11a
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    • pp.585-587
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    • 2002
  • The materials showing high structure dispersity are developed on the quartz base and they are obtained by mechano-chemical technology. Depending on the processing conditions and subsequent applications the materials produced by mechano-chemical reaction show concurrently magnetic, dielectric and electrical properties. The obtained magnetic-electrical powders classified by aggregate complex of their features as segnetomagnetics, contain a dielectric material as a canγing nucleus, particularly the quartz on that surface one or more layers of different compounds are synthesized having thickness up to 10~50 nm and showing magnetic, electrical and other properties.

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AN EXPERIMENTAL STUDY ON COEFFICIENT OF THERMAL EXPANSION OF DENTAL INVESTMENTS (수종치과매몰재(數種齒科埋沒材)의 열팽창계수(熱膨脹係數)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.5 no.1
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    • pp.29-34
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    • 1979
  • The purpose of this study was to measure thermal expansions of dental investments, Biovest(Casting Investment. Dentsply International INC, U.S.A.), Multi-Best (Use for all dental chrome-cobalt alloys, The Ransom & Randolph Co. U.S.A.), Kerr(Inlay Investment. Sybron Kerr, U.S.A.), O. K. (Inlay Investment. Shofu Dental MFG, Co. Japan), Whip-Mix (Cristobalite Inlay Investment. Whip-Mix Corporation. U.S.A.). Thermal expansion of specimens(5mm in diameter and 50mm in length) was measured by a dilatometer at the temperature range from $20^{\circ}C$ to $700^{\circ}C$ by comparing expansion between standardized quartz and experimental specimens with heating rate about $300^{\circ}C$/hr. The following results were obtained. 1. The coefficient of thermal expansion of Biovest was $15{\times}10^{-6}/^{\circ}C$ in the water powder ratio 18/100 and $14{\times}10^{-6}/^{\circ}C$ in the water powder ratio 28/100. Those of Multi-Best were $9{\times}10^{-6}/^{\circ}C$ in the water powder ratio 14/100 and $7{\times}10^{-6}/^{\circ}C$ in the water powder ratio 24/100. 2. The coefficient of thermal expansion of Kerr were $17{\times}10^{-6}/^{\circ}C$ in the water powder ratio 38/100 and $14{\times}10^{-6}/^{\circ}c$ in the water powder ratio 48/100. Those of O. K. were $9{\times}10^{-6}/^{\circ}C$ in the water powder ratio 33/100 and $7{\times}10^{-6}/^{\circ}C$ in the water powder ratio 43/100 3. The coefficient of thermal expansion of Whip-Mix were $14{\times}10^{-6}/^{\circ}C$ in the water powder ritio 40/100 and $12{\times}10^{-6}/^{\circ}c$ Fein the water powder ratio 50/100. Those of Hi-Heat were $11{\times}10^{-6}/^{\circ}c$ in the water powder ratio 28/100 and $10{\times}10^{-6}/^{\circ}c$ in the water powder ratio 38/100.

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Microstructure of ZnO Thin Film on Nano-Scale Diamond Powder Using ALD (나노급 다이아몬드 파우더에 ALD로 제조된 ZnO 박막 연구)

  • Park, S.J.;Song, S.O.
    • Journal of the Korean Vacuum Society
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    • v.17 no.6
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    • pp.538-543
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    • 2008
  • Recently a nano-scale diamond is possible to manufacture forms of powder(below 100 nm) by new processing of explosion or deposition method. Using a sintering of nano-scale diamond is possible to manufacture of grinding tools. We have need of a processing development of coated uniformly inorganic to prevent an abnormal grain growth of nano-crystal and bonding obstacle caused by sintering process. This paper, in order to improve the sintering property of nano-scale diamond, we coated ZnO thin films(thickness: $20{\sim}30\;nm$) in a vacuum by ALD(atomic layer deposition) Economically, in order to deposit ZnO all over the surface of nano-scale diamond powder, we used a new modified fluidized bed processing replaced mechanical vibration effect or fluidized bed reactor which utilized diamond floating owing to pressure of pulse(or purge) processing after inserted diamond powders in quartz tube(L: 20 mm) then closed quartz tube by porosity glass filter. We deposited ZnO thin films by ALD in closed both sides of quartz tube by porosity glass filter by ALD(precursor: DEZn($C_4H_{10}Zn$), reaction gas: $H_2O$) at $10^{\circ}C$(in canister). Processing procedure and injection time of reaction materials set up DEZn pulse-0.1 sec, DEZn purge-20 sec, $H_2O$ pulse-0.1 sec, $H_2O$ purge-40 sec and we put in operation repetitive 100 cycles(1 cycle is 4 steps) We confirmed microstructure of diamond powder and diamond powder doped ZnO thin film by TEM(transmission electron microscope) Through TEM analysis, we confirmed that diamond powder diameter was some $70{\sim}120\;nm$ and shape was tetragonal, hexagonal, etc before ALD. We confirmed that diameter of diamond powders doped ZnO thin film was some $70{\sim}120\;nm$ and uniform ZnO(thickness: $20{\sim}30\;nm$) thin film was successfully deposited on diamond powder surface according to brightness difference between diamond powder and ZnO.

An Experimental Study on Mechanical Properties of Ultra-High Strength Powder Concrete (압축강도 300MPa 이상의 초고강도 분체콘크리트 개발을 위한 실험적 연구)

  • Jo, Byung-Wan;Yoon, Kwang-Won;Park, Jung-Hoon;Kim, Heoun
    • Journal of the Korea Concrete Institute
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    • v.22 no.3
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    • pp.287-295
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    • 2010
  • In this study, ordinary Portland cement was used and the air void was minimized by using minute quartz as the filler. In addition, steel fibers were used to mitigate the brittle failure problem associated with high strength concrete. This study is in progress to make an Ultra-high strength powdered concrete (UHSPC) which has compressive strength over 300 MPa. To increase the strength of concrete, we have compared and analyzed the compressive strengths of the concretes with different mix proportions and curing conditions by selecting quartz sand, dolomite, bauxite, ferro silicon which have diameters less than 0.6 mm and can increase the bond strength of the transition zone. Ultra-high strength powdered concrete, which is different from conventional concrete, is highly influenced by the materials in the mix. In the study, the highest compressive strength of the powdered concrete was obtained when it is prepared with ferro silicon, followed in order by Bauxite, Dolomite, and Quartz sand. The amount of ferro silicon, when the highest strength was obtained, was 110%, of the weight of the cement. SEM analysis of the UHSPC showed that significant formation of C-S-H and Tobermorite due to high temperature and pressure curing. Production of Ultrahigh strength powdered concrete which has 28-day compressive strength upto 341MPa has been successfully achieved by the following factors; steel fiber reinforcement, fine particled aggregates, and the filling powder to minimize the void space, and the reactive materials.

Effect of Microstructure on the Prooperties of High Strength Hardened Cement Paste (II) (고강도 시멘트 경화체의 특성에 미치는 미세구조의 영향 (II))

  • 김정환;최상흘;한기성
    • Journal of the Korean Ceramic Society
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    • v.27 no.8
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    • pp.1034-1042
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    • 1990
  • Investigation for the preparation of high strength hardened cement paste using ordinary portland cement, hydroxypropyl methyl cellulose(HPMC) with various admixtures was carried out. The cement paste was mixed with 0.1 of water cement ratio by twin roll mill and cured 60 days in humidity chamber. When the quartz powder or white cement was added to the paste, the flexural strength was 900∼1000kg/㎠ and the Young's modulus was 8∼9×105kg/㎠. When the silicafume was added, the flexural strength was 800kg/㎠ and the Young's modulus was 6×105kg/㎠.

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