• Journal of the Korean Ceramic Society
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• v.34 no.8
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• pp.834-842
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• 1997

Controlled Ca impurity implanted inner crack-like pore in the high purity alumina single crystal, sapphire, had been created by micro-fabrication technique, which includes ion implantation, photo-lithography, Ar ion milling, and hot press technique. The morphological change and the healing of cracklike pore in Ca doped high purity single crystal alumina, sapphire, during high temperature heat treatment in vacuum were observed using optical microscopy. The dot-like surface roughening was developed and hexagon like crystal appeared on inner surface of crack-like pore after heat treatment. Bar type crystals, probably CaO.6Al2O3, were observed on the inner surface after 1 hour heat treatment at 1, 50$0^{\circ}C$, but this bar type crystal disappeared after 1 hour heat treatment at 1, $600^{\circ}C$. This disappearance means that there should be a little increase of Ca solubility limit to alumina at this temperatures.

• Proceedings of the Membrane Society of Korea Conference
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• 1994.03a
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• pp.1-21
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• 1994

There are growing needs to produce relatively high purity (99.0% or higher) oxygen at low cost. For small scale production, both pressure swing adsorption (PSA) and membrane process are competitve and less expensive or more convient than well known crygenic fractionation technology. A continuous membrane colume (CMC) combined with a PSA oxygen generator can be employed to produce high purity oxygen continuosly. The oxygen-enriched gas generated by a PSA unit, with a concentration of 93-94%, is fed to the CMC that consists of three modules of poly(imide) hollow fibers. Several experiments were conducted by varying parameters, such feed flow rate, transmenbrane pressure drop, stage cut, and feed location in order to obtain a high oxygen concentration above 99.0%. A two-series unit mode was also employed with CMC operation to optimize the given membrane area.

• Journal of the Korean Chemical Society
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• v.9 no.2
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• pp.96-100
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• 1965

Possibility on carrier-free Fe-59 preparation by Korean TRIGA Mark Ⅱ reactor was investigated, namely average cross section on $Co^{59}$(n,p) $Fe^{59}$ reaction, separation by anion exchange resin and radiochemical purity. Radiochemical purity of Fe-59 separated was checked by the method of ${\gamma}$-ray spectrometry with 256-multichannel pulse height analyzer and of half life determination. This method permits Fe-59 preparation with radiochemical purity of > 99.9%.

• Archives of Pharmacal Research
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• v.22 no.6
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• pp.614-618
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• 1999

A reversed-phase high-performace liquid chromatographic method was developed to determine the optical purity of metoprolol enantiomers. The enantiomers were converted to diastereomeric derivatives using (-)-menthyl chloroformate reagent. Separation of the enantiomers as diastereomers was achieved by reversed-phase HPLC within 30 min using Inertsil C8 column. This method allowed determination of 0.05% of either enantiomer in the presence of its stereoisomer and method validation showed adequate linearity over the required range. Owing to the reaction condition during the derivatization with (-)-menthyl chloroformate, the possibility of racemization had to be established. Different ratios of (S)-(-)-metoprolol and (R)-(+)-metoprolol were prepared. Enantiomeric separation of these mixtures took place on a chiralcel OD column or, after derivatization with (-)-menthyl chloroformate, on a C8 column. The results form the these two independent separation systems were compared with trace racemization and were in very good agreement. No racemization was found during the experiment.

• Journal of the Korean Magnetic Resonance Society
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• v.24 no.1
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• pp.30-37
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• 2020

Quantitative nuclear magnetic resonance (qNMR) has been gaining attention as a purity assessment method. In particular, qNMR is recognized as the primary method to realize the Internal System of Units (SI) in organic analysis. The capability of quantitative analysis is recognized as the beginning of NMR development. NMR signals are proportional to the number of nuclei and qNMR has been used in various fields, such as metabolomics and food and pharmaceutical analysis. However, careful sample preparation and thorough optimization of measurement parameters are required to obtain accurate and reliable results. In this review, quantitative methods used in qNMR are discussed, and the important factors to be considered also introduced. The recent development of qNMR techniques including combination with chromatography and, multidimensional NMR are also presented.

• Proceedings of the Korea Inteligent Information System Society Conference
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• 2000.11a
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• pp.341-348
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• 2000

의사결정 나무라고 불리우기도 하는 나무모형은 결과 해석의 용이성으로 데이터마이닝의 분류예측 모형으로써 큰 각광을 받고 있다. 현재 나무모형으로 가장 많이 사용되는 Breiman et. al의 CART나 Quinlan의 C4.5 모두 생성된 노드들의 자료 구성이 목표변수를 기준으로 수준 구성비 측면에서 순수해지도록 진행된다. 그러나 CRM에 있어 가장 흔한 주제인 해지예측을 위한 모델링을 실시하는 경우 관심의 대상인 해지자가 전체 자료에 극히 일부를 차지하여, 기존의 분할 방법에서와 같이 모든 노드의 순수성을 고려하기란 불가능하다. Buja와 Lee는 이와 같이 소수의 관심에 대상이 되는 부류를 찾아내기 위한 나무모형 생성방법을 소개하였다 즉, 해지자 관리가 중요한 경우 해지자와 비해지자 구분을 진행하는 기존의 방법과는 달리 전체 자료 중 해지자를 집중적으로 찾아가는 탐색적 분할 기준인 단측 순수성(one-sided purity)을 제안하였다. 본 연구에서는 단측 순수성에 의한 나무모델링을 모 PC통신 회사의 해지자 자료에 적용하며 기존의 방법과 비교하였고 몇 가지 시뮬레이션 자료를 통해 단측 순수성의 문제점과 앞으로 해결하여야 할 과제에 대하여 살펴보았다.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.149-153
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• 2005

The electron beam machining provides very high resolution up to nanometer scale, hence the E-beam writing technology is rapidly growing in MEMS and nano-engineering areas. In the optical column of the e-beam writer, there are several lenses condensing and focusing electron beams from electron gun with fringing magnetic fields. The polepieces of these lenses are usually made with high purity iron which is hard to fabricate and very expensive. In this paper, the possibility of using polepiece of object lens composed with pure iron and low carbon steel was examined to reduce cost. The magnetic field at object lens was calculated with finite element method, and practical focusing qualities of SEM pictures were observed comparing for the object lens polepieces with pure iron and two type of composed with low carbon steel.

• Journal of the Korean Society for Precision Engineering
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• v.12 no.3
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• pp.62-72
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• 1995

The present study was undertaken to investigate the dry wear mechanism of the alumina ceramics in the purity variation for the wear of STB2. The wear test was carried out under different experimental condition various sliding speed, contact pressure and sliding distance. According as the alumina purity increased, wear volume of the STB2 decreased and minimum value of wear volume was over to high speed side. According as the sliding speed and sliding distance increased, friction coefficient decreased owing to drop of the shear strength, it decresed largely owing to decreased of elastic modulus and thermal conductivity with decrease in alumina purity. Indicative of minimum, value of wear volume, low speed side was abrasive wear, high speed side was wear of heat softening. The friction surface of ceramics protacted by oxide was transfer from STB2.

• Journal of Powder Materials
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• v.15 no.1
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• pp.6-12
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• 2008

[ $YBa_2Cu_3O_{7-y}$ ](123) powders were synthesized by the solid state reaction method using two different purity $BaCO_3$ powders (99.75% and 99.7% purity) and $Y_2O_3$ (99.9%) and CuO (99.9%) powders. The effect of $BaCO_3$ purity on the formation of a 123 phase and the superconducting properties were investigated. The mixtures of raw powders were calcined at temperature ranges of $800^{\circ}C-880^{\circ}C$ in air and finally made into a single grain samples by a melt processing with top seeding. It was found that a 123 phase was well formed at temperature above $870^{\circ}C$, but the purity effect on the 123 formation was negligible. The single-grain 123 samples prepared from the different $BaCO_3$ powders showed the same $T_c$ value of 90.5 K and similar $J_c$ values about $10^4\;A/cm^2$ at 0 T and 77 K, and $10^3\;A/cm^2$ at 2 T and 77 K. This result indicates that the low purity, cheap price $BaCO_3$ powder can be used as a raw material for the fabrication of single-grain, high-$J_c$ superconducting levitator.

• Journal of the Korean Society of Food Science and Nutrition
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• v.40 no.7
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• pp.975-980
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• 2011

1-Palmitoyl-2-oleoyl-3-oleoyl glycerol (POO) and 1-palmitoyl-2-oleoyl-3-palmitoyl glycerol (POP) were enriched from palm stearin using an acetone fractionation process. Response surface methodology was employed to optimize the purity of POO ($Y_1$, %) and POP ($Y_2$, %) along with POO+POP content ($Y_3$, g) based on independent variables such as fractionation temperature ($X_1$, 25, 30, and $35^{\circ}C$) and the ratio of palm stearin to acetone ($X_2$, 1:3, 1:6 and 1:9, w/v). Fractionation conditions were optimized to maximize $Y_1$, $Y_2$, and $Y_3$, in which fractionation temperature was $29.3^{\circ}C$ with a 1:5.7 acetone ratio. With such parameters, 60.9% of POP and 23.8% of POO purity were expected with a 75% yield (3.0 g) of POO and POP.