• 한국분말재료학회지
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• 제2권2호
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• pp.135-141
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• 1995

As the first step of study on fabrication of ceramic powders from phytoliths in rice, especially in rice husks, pulverization method of rice husks and the properties of milled rice husks were investigated. Impact methods, such as ball milling, were not meaningful for pulverizing elastic and thin fabric structure of rice husks. The most effective one was cutting method. In the present work, a rotating knife cutting method was applied to pulverizing rice husks. A 40-mesh screen was inserted under the rotating knives. The most portion of the milled powder was found in -50/+100 mesh section. Morphology of the milled rice husks revealed that the husks larger than 70 mesh were flake-like shape, at -70/+100 mesh section relatively equi-axed shape, at -170/+325 mesh section rod-like shape, and below 325 mesh section dust-like shape. Tap density of raw rice husks was about 0.1 $g/cm^3$, while those of milled rice husks were over $0.4 g/cm^3$. This meant that, for a given volume of reactor, raw material charge can be increased more that 4 times when using milled rice husks than unmilled one. True densities of unmilled and milled rice husks were higher than $1.4 g/cm^3$, and increased with decreasing milled sizes.

• 한국염색가공학회지
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• 제22권2호
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• pp.132-139
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• 2010

Sericin pulverization process was applied by freezing-thawing of sericin protein concentration solution and physicochemical properties of sericin/chitosan blended films were investigated. In sericin pulverization process by freezing-thawing method, the refrigeration storage at $4^{\circ}C$ maximized gelling between sericin molecules, which increased 10% of recovery ratio from sericin concentration solution that using ultrafiltration procedure. In physicochemical properties of sericin/chitosan blended films, the maximum load of chitosan (6.7kgf) had higher than that of sericin (1.2kgf), and the elongation of sericin and chitosan had 96% and 34%, respectively. Also FT-IR analysis of sericin/chitosan blended films showed that both sericin and chitosan films had amide I peak (N-H bond) in $1,521cm^{-1}$ and amide II peak (C=O bond) in $1,630cm^{-1}$. In addition, it could confirm compatibility between both materials as indicated by the decrease in the amide I peak's absorption value as chitosan content increases.

• 한국방사선학회논문지
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• 제4권1호
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• pp.11-17
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• 2010

요석은 고대 인류부터 지금 현재 인류까지 끊임없이 인간을 괴롭히고 있는 질병중의 하나이다. 하지만 딱히 예방법이 없어 문제가 생기면 비뇨기과적 치료가 절대적으로 필요한 질병이다. 이런 요석의 가장 큰문제점은 상당한 통증 과 구토, 발열등을 유발한다는 것이다. 통증은 요관을 통과 할 때나 요관이 요석으로 인한 심한 경련이 일어날 때 크게 일어난다. 이 통증은 마약성분이 강한 펜타닐 이나 페치딘 같은 강한 진통제에도 잘 잡히지 않는 경향이 있어 신속한 검사와 치료가 요구된다. 본 논문에서는 ESWL(Extracorpereal Shock Wave Lithotripsy)을 이용한 요석 치료시 특히 분쇄율은 낮고 환자의 통증은 심한 Proximal ureteral stone 과 Mid ureteral stone에 대해 각각의 여러 조건을 적용하여 최적의 치료방법과 최고의 분쇄율에 대하여 실험 과 연구를 하여 보았다. 실험결과 Proximal과 Mid ureter에 위치한 stone은 호흡에 의한 충격파의 적중률이 낮아 분쇄율이 distal ureter보다 낮았으나 방전interval을 줄임으로써 분쇄율을 높일 수 있었고, 낮은 방전 Power로 여러번 분쇄하는 것보다는 높은 방전 Power와 적절한 방전횟수로 분쇄를 하였을 때 ureter도 보호하면서 분쇄율이 높다는 것을 알 수 있었다.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2000년도 International Symposium on Magnetics The 2000 Fall Conference
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• pp.393-394
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• 2000

The magnetic alloy of $Nd_{2}Fe_{14}B$-type was synthesized by a mechano-chemical method, including the processes of spray-drying, de-binding, milling, $H_{2}$- and Ca-reduction and washing. The very fine $Nd_{2}Fe_{14}B$ particles smaller than $1\mu\textrm{m}$ could be achieved without the inevitable pulverization step in conventional processes.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 추계 학술발표회 제20권2호
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• pp.525-528
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• 2008

고에너지 소비형인 시멘트의 대체 재료로써 고로슬래그의 활용성을 높이기 위해 분쇄 방법과 입자의 분말도 그리고 알칼리 자극제의 종류에 따른 50wt.%의 고로슬래그를 치환한 고로 슬래그 시멘트의 수화 및 물리적 특성을 조사하였다. 알칼리 자극제로써 Ca(OH)$_2$, NaOH, Na$_2$SO$_4$,사용하였고 이런 특성들을 비교하기 위해 자극제를 넣지 않은 무첨가 슬래그 시멘트를 함께 실험하였다. 압축강도 실험에서의 분쇄방법에 차이로는 알칼리 자극제에 관계없이 롤러밀로 분쇄한 슬래그가 대체적으로 높은 강도를 나타내었으며 자극제에 따라서는 재령 7일 이내의 초기강도에서는 분말도와 분쇄방법에 관계없이 Na$_2$SO$_4$>Ca(OH)$_2$>None>NaOH 순으로 나왔으며 28일의 장기강도에선 Ca(OH)$_2$가 가장 높게 나타났다.

• ALGAE
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• 제19권2호
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• pp.123-127
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• 2004

A more rapid and efficient method to extract RNA from Ecklonia cava Kjellman (Laminariales, Phaeophyceae) was introduced in this study. Each step of the procedure was evaluated and the optimal concentration of each chemical in the lysis solution was determined. Tissue pulverization with PVPP and β-mercaptoethanol in the lysis solution were not essential for RNA extraction of this species. The highest yield and purity of E. cava RNA were obtained by the lysis solution containing 1% CTAB, 1 M NaCl, 0.7% PVP, 10mM EDTA and 100mM Tris-Cl (pH 9.0). Approximately 8μg of RNA was obtained from 200 mg of ground tissue. The ratios of the absorbance at 260 nm and 280 nm were from 1.6 to 1.8 and those of at 230 nm and 260 nm were from 1.8 to 2.0. The extracted RNAs obtained in this study turned out to have a sufficient quality for cDNA synthesis.

• 한국수소및신에너지학회논문집
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• 제7권1호
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• pp.71-79
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• 1996

Yttrium thin film, 580nm thick, was prepared by electron beam evaporation. Film was hydrogenated room temperature upto 40 bar hydrogen pressure, without any activation process. Hydrogen concentration was determined by a quartz-crystal microbalance(QCM) method. YH2.9 sample was made without any pulverization. Electrical resistance was measured by four-point DC method in the temperature range between room temperature and 30K for various hydrogen concentration, x=0 to 2.9 of YHx sample. Temperature dependent resistance of YH2.9 shows low temperature minimum at 105K, the metal-semiconductor transition at 260K, and a hystersis above 210K.

• ALGAE
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• 제22권2호
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• pp.125-129
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• 2007

Conventional methods for the isolation and purification of mRNA from Zygnema were unsuccessful because of its high amount of pigments and RNA interactive molecules. In particular, pigments were difficult to remove using conventional protocols because they interacted with RNA during pulverization of the materials. This resulted in total degeneration of RNA in two to three hours. To alleviate this problem, we developed an isolation method that utilized DEAE-cellulose resin. The pigments bound to DEAE anion exchange resin and separated from the RNA. Purified total RNA showed an yield of 50 μg per 100 mg of tissue with this method. The amplified 2nd strand cDNA was distributed 300 bp and over.

• 한국건설순환자원학회논문집
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• 제3권4호
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• pp.313-319
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• 2015

본 연구에서는 비가열 제조법에 의한 BP슬러지의 반건조 제조공정 개발에 관한 연구로 고함수율(50% 이상)의 BP부산물을 건설 재료로의 대량 활용하기 위하여 산업부산물과 혼합에 따른 함수율 저감에 관한 연구를 수행하였다. BP부산물에 함수저감재(1:0.5)의 투입비율에서 함수저감율을 측정결과 PA+CFA(1:0.5) 배합에서 함수율이 18.5%로 가장 낮게 나타났다. 또한, 에이징 온도조건 $20{\sim}30^{\circ}C$일 경우 에이징 기간 1~2일 사이에 약 9.2~11.4%의 함수율을 나타내 본 연구에서 건설재료로 활용하기 위한 10% 이내의 함수율 저감에 근접하였다. 에이징 공정 이후 분쇄방법에 따른 비가열 BP부산물의 물성을 비교 평가한 결과, 분쇄방식에 따라서 차이는 많이 발생하지 않았으며, 생산효율 및 경제성을 고려할 경우 연속생산이 가능한 미립자분쇄기 또는 핀밀을 사용하는 것이 적합할 것으로 나타났다.

• 보존과학연구
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• 통권29호
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• pp.199-220
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• 2008

Hobun(Oyster shell White) is a traditional material used as extender and white pigment from ancient times. The production method of it, however, has been discontinued. We have studied the traditional production method of Hobun by weathering oyster shell, which is one of the traditional ways for preparing Hobun. Reproduction study of manufacturing method of the discontinued traditional material is an important accomplishment of our research. Also this study provides solid background knowledge to stabilize the production and supply of Hobun for the cultural asset repairing materials. The result can be summarized as follows: The production process of Hobun by weathering method takes 5 steps - (1) weathering shells ${\rightarrow}$ (2) washing ${\rightarrow}$ (3) pulverization ${\rightarrow}$ (4) separating fine powder by submerging in water ${\rightarrow}$ (5) drying. The major aim in step (1) is to eliminate organic impurities. In the step (4), the fine particles smaller than $25{\mu}m$ are separated by extracting the supernatant from stirred suspension after heavy particles are submerged. Also, the soluble inorganic impurities can be eliminated through the powder submerge in 15 times water and stirring the suspension 6 hours and changing the water 3~4 times. The final products have high quality with 94.03, 0.52, 2.05 for L, a, b, less than $25{\mu}m$ particle size, fine resistance for discoloration by light and environmental pollution and good workability.