• 제목/요약/키워드: psaB

검색결과 56건 처리시간 0.03초

Magnetic Nanoparticle Immobilized N-Propylsulfamic Acid as a Recyclable and Efficient Nanocatalyst for the Synthesis of 2H-indazolo[2,1-b]phthalazine-triones in Solvent-Free Conditions: Comparison with Sulfamic Acid

  • Rostami, Amin;Tahmasbi, Bahman;Yari, Ako
    • Bulletin of the Korean Chemical Society
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    • 제34권5호
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    • pp.1521-1524
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    • 2013
  • N-Propylsulfamic acid supported onto magnetic $Fe_3O_4$ nanoparticles (MNPs-PSA) was used as an efficient and magnetically recoverable catalyst for synthesis of 2H-Indazolo[2,1-b]phthalazine-1,6,11(13H)-trione derivatives from the three-component, one-pot condensation reaction of phthalhydrazide, aromatic aldehydes and cyclic 1,3-diones, in good to excellent yields at $100^{\circ}C$ under solvent-free conditions. The catalyst was easily separated with the assistance of an external magnetic field from the reaction mixture and reused for several consecutive runs without significant loss of its catalytic efficiency. In order to compare, the synthesis of 2H-Indazolo[ 2,1-b]phthalazine-1,6,11(13H)-trione derivatives in the presence of catalytic amount of sulfamic acid (SA) under same reaction condition was also reported.

A Novel Grasshopper Optimization-based Particle Swarm Algorithm for Effective Spectrum Sensing in Cognitive Radio Networks

  • Ashok, J;Sowmia, KR;Jayashree, K;Priya, Vijay
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제17권2호
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    • pp.520-541
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    • 2023
  • In CRNs, SS is of utmost significance. Every CR user generates a sensing report during the training phase beneath various circumstances, and depending on a collective process, either communicates or remains silent. In the training stage, the fusion centre combines the local judgments made by CR users by a majority vote, and then returns a final conclusion to every CR user. Enough data regarding the environment, including the activity of PU and every CR's response to that activity, is acquired and sensing classes are created during the training stage. Every CR user compares their most recent sensing report to the previous sensing classes during the classification stage, and distance vectors are generated. The posterior probability of every sensing class is derived on the basis of quantitative data, and the sensing report is then classified as either signifying the presence or absence of PU. The ISVM technique is utilized to compute the quantitative variables necessary to compute the posterior probability. Here, the iterations of SVM are tuned by novel GO-PSA by combining GOA and PSO. Novel GO-PSA is developed since it overcomes the problem of computational complexity, returns minimum error, and also saves time when compared with various state-of-the-art algorithms. The dependability of every CR user is taken into consideration as these local choices are then integrated at the fusion centre utilizing an innovative decision combination technique. Depending on the collective choice, the CR users will then communicate or remain silent.

산화붕소의 소듐아미드로부터 육방정 질화붕소의 합성 (Preparation of Hexagonal Boron Nitride from Boron Oxide and Sodium Amide)

  • 손영국;장윤식;오기동
    • 한국세라믹학회지
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    • 제27권7호
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    • pp.869-876
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    • 1990
  • Hexagonal boron nitride was synthesized from boron oxide and sodium amide in ammonia gas stream. The reaction mechanisms and characteristics of as synthesized boron nitride was investigated by means of TG, DTA, IR, XRD, SEM and PSA. The results are ; 1) hexagonal boron nitride was synthesized from reactions at temperatures above 40$0^{\circ}C$ 2) Sodium metaborate was present as by-product after reaction so that the reaction mechanism is reduced as follows : 2B2O3+3NaNH2longrightarrowBN+3NaBO2+2NH3. 3) boron nitride obtained at the reaction temperature below 40$0^{\circ}C$ is found to have random layer strudcture but the structure transits to ordered layer structure rapidly with increasing reaction temperature, showing separation of (101) differaction line from (10)band in XRD pattern of the reaction product at 50$0^{\circ}C$.

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하이드로 포밍 공정시 관재의 열처리 조건에 따른 성형성 분석 (Effect of heat treatment conditions on the tube hydroformability)

  • 박광수;강부현;김동규;문영훈
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 추계학술대회
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    • pp.1810-1815
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    • 2003
  • Tube hydroforming provides a number of advantages over conventional stamping process, including fewer secondary operation, weight reduction, assembly simplification, adaptability to forming of complex structural components and improved structural strength and stiffness. In this study, the effect of the heat treatment on the hydro-formability has been investigated. By using the mild steel tube bulging test is performed at various heat treatment conditions to evaluate the hydro-formability.

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CURRENT STATUS AND IMPORTANT ISSUES ON SEISMIC HAZARD EVALUATION METHODOLOGY IN JAPAN

  • Ebisawa, Katsumi
    • Nuclear Engineering and Technology
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    • 제41권10호
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    • pp.1223-1234
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    • 2009
  • The outlines of seismic PSA implementation standards and seismic hazard evaluation procedure were shown. An overview of the cause investigation of seismic motion amplification on the Niigata-ken Chuetsu-oki (NCO) earthquake was also shown. Then, the contents for improving the seismic hazard evaluation methodology based on the lessons learned from the NCO earthquake were described. (1) It is very important to recognize the effectiveness of a fault model on the detail seismic hazard evaluation for the near seismic source through the cause investigation of the NCO earthquake. (2) In order to perform and proceed with a seismic hazard evaluation, the Japan Nuclear Energy Safety Organization has proposed the framework of the open deliberation rule regarding the treatment of uncertainty which was made so as to be able to utilize a logic tree. (3) The b-value evaluation on the "Stress concentrating zone," which is a high seismic activity around the NCO hypocenter area, should be modified based on the Gutenberg-Richter equation.

Weight optimization of coupling with bolted rim using metaheuristics algorithms

  • Mubina Nancy;S. Elizabeth Amudhini Stephen
    • Coupled systems mechanics
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    • 제13권1호
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    • pp.1-19
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    • 2024
  • The effectiveness of coupling with a bolted rim is assessed in this research using a newly designed optimization algorithm. The current study, which is provided here, evaluates 10 contemporary metaheuristic approaches for enhancing the coupling with bolted rim design problem. The algorithms used are particle swarm optimization (PSO), crow search algorithm (CSA), enhanced honeybee mating optimization (EHBMO), Harmony search algorithm (HSA), Krill heard algorithm (KHA), Pattern search algorithm (PSA), Charged system search algorithm (CSSA), Salp swarm algorithm (SSA), Big bang big crunch optimization (B-BBBCO), Gradient based Algorithm (GBA). The contribution of the paper isto optimize the coupling with bolted rim problem by comparing these 10 algorithms and to find which algorithm gives the best optimized result. These algorithm's performance is evaluated statistically and subjectively.

Expression Analysis of ESTs Derived from the Leaf of Chunpoong (Panax ginseng C,A. Meyer)

  • In, Jun-Gyo;Lee, Bum-Soo;Yang, Deok-Chun
    • 한국자원식물학회:학술대회논문집
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    • 한국자원식물학회 2003년도 춘계 학술발표대회
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    • pp.122-122
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    • 2003
  • Expressed sequence tags (EST) are help to quickly identify functions of expressed genes and to understand the complexity of gene expression. In order to analyze gene expression of the leaf development in Panax ginseng, which is one of the most important medicinal plant, expressed sequence tags (EST) analysis was carried out. We constructed a cDNA library using the immature leaf of Chunpoong. Partial sequences were obtained from 3,170 clones. The ESTs could be clustered into 1,624 (56.1%) non-redundant groups. Similarity search of the non-redundant ESTs against public non-redundant databases of both protein and DNA indicated that 1,137 groups show similarity to genes of known function. These ESTs clones were divided into sixteen categories depending upon gene function. Most abundant transcripts in immature ginseng leaf were photosynthesis related protein, such as chlorophyll a/b binding protein LHCII type I (128), chlorophyll a/b binding protein (53), ribulose-1,5-bisphosphate carboxylase (41), and photosystem I psaH (26). The EST data from immature leaf generated in this study is useful in dissecting gene expression in leaf organ of ginseng.

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Association of Six Susceptibility Loci with Prostate Cancer in Northern Chinese Men

  • Zhang, Yu-Rong;Xu, Yong;Yang, Kuo;Liu, Ming;Wei, Dong;Zhang, Yao-Guang;Shi, Xiao-Hong;Wang, Jian-Ye;Yang, Fan;Wang, Xin;Liang, Si-Ying;Zhao, Cheng-Xiao;Wang, Fei;Chen, Xin;Sun, Liang;Zhu, Xiao-Quan;Zhu, Ling;Yang, Yi-Ge;Tang, Lei;Jiao, Hai-Yan;Huo, Zheng-Hao;Yang, Ze
    • Asian Pacific Journal of Cancer Prevention
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    • 제13권12호
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    • pp.6273-6276
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    • 2012
  • Background/Aim: Six prostate cancer (PCa) susceptibility loci were identified in a genome-wide association study (GWAS) in populations of European decent. However, the associations of these 6 single-nucleotide polymorphisms (SNPs) with PCa has remained tobe clarified in men in Northern China. This study aimed to explore the loci associated with PCa risk in a Northern Chinese population. Methods: Blood samples and clinical information of 289 PCa patients and 288 controls from Beijing and Tianjin were collected. All risk SNPs were genotyped using polymerase chain reaction (PCR)-high resolution melting curve technology and gene sequencing. Associations between PCa and clinical covariates (age at diagnosis, prostate-specific antigen [PSA], Gleason score, tumor stage, and level of aggressiveness) and frequencies of alleles and genotypes of these SNPs were analyzed using genetic statistics. Results: Among the candidate SNPs, 11p15 (rs7127900, A) was associated with PCa risk (P = 0.02, odds ratio [OR] = 1.64, 95% confidence interval [CI] = 1.09-2.46). Genotypes showed differences between cases and controls on 11p15 (rs7127900, A), 11q13 (rs7931342, T), and HNF1B (rs4430796, A) (P = 0.03, P = 0.01, and P = 0.04, respectively). The genotype TG on 11q13 (rs7931342, T) was positively associated with an increased Gleason score (P = 0.04, OR = 2.15, 95% CI = 1.02-4.55). Patients carrying TG on 17q24 (rs1859962, G) were negatively associated with an increased body mass index (BMI) (P = 0.03, OR = 0.44, 95% CI = 0.21-0.92) while those with AG on HNF1B (rs4430796, A) were more likely to have PSA increase (P = 0.002). Conclusion: Our study suggests that 11p15 (rs7127900, A) could be a susceptibility locus associated with PCa in Northern Chinese. Genotype TG on 11q13 (rs7931342, T) could be related to an increased Gleason score, AG on HNF1B (rs4430796, A) could be associated with PSA increase, and TG on 17q24 (rs1859962, G) could be negatively associated with an increased BMI in Chinese men with PCa.

디지털 컬러용 pink-red 고온발색 무기안료의 합성 및 특성평가 (Synthesis and characterization of thermally stable pink-red inorganic pigment for digital color)

  • 이원준;황해진;김진호;조우석;한규성
    • 한국결정성장학회지
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    • 제24권4호
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    • pp.169-175
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    • 2014
  • 최근 각광받고 있는 디지털 프린팅을 이용한 디자인 기법은 세밀한 표현과 다양한 이미지 구현이 가능하고, 원료의 낭비가 적어 효율성이 높은 장점을 가지고 있다. 디지털 프린팅 공정에서는 cyan, magenta, yellow, black이 기본적인 디지털 4원색으로 사용되며, 도자제품에 적용되는 세라믹 안료의 경우 $1000^{\circ}C$ 이상의 고온 소성이 가능하도록 우수한 열적, 유약 안정성과 발색 특성이 요구된다. 본 연구에서는 고상합성법을 이용하여 $CaO-SnO_2-Cr_2O_3-SiO_2$ 조성의 pink-red 고온발색 무기안료를 합성하였다. $Ca(Sn,Cr)SiO_5$ 세라믹 안료의 합성 조건에 따른 물성을 XRD, SEM, PSA, FT-IR를 이용하여 분석하였고, Cr 치환량 변화가 $Ca(Sn,Cr)SiO_5$ 무기 안료의 발색 거동에 미치는 영향을 Uv-vis.와 CIE 표색계 값($L^*a^*b^*$)을 기준으로 한 색도측정을 통해 관찰하였다.

혀인두신경 또는 혀밑신경을 절단한 흰쥐 미각샘의 형태학적 변화와 렉틴조직화학 (Lectin Histochemistry and Morphological Changes in von Ebner's Glands in Rats after Glossopharyngeal or Hypoglossal Axotomy)

  • 문용석
    • 생명과학회지
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    • 제23권12호
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    • pp.1541-1552
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    • 2013
  • 부교감신경 또는 교감신경섬유가 흰쥐 혀 미각샘의 구조와 분비기능에 미치는 영향을 조사할 목적으로 성체 흰쥐의 양쪽 혀인두신경 또는 혀밑신경을 절단한 후 혀 미각샘의 형태학적 변화를 3일부터 21일까지 관찰하였고, PSA, UEA I, GSL I $B_4$, ECL, DBA, SBA, HPA, SJA 및 sWGA의 9가지 렉틴을 이용한 렉틴조직화학을 실시하여 미각샘의 복합당질의 특성과 분비양상을 비교하였다. 혀인두신경을 절단한 혀 미각샘은 3일군부터 장액샘꽈리에서 세포질 공포가 나타났으며 10일군에서는 공포가 매우 커지고 미각샘의 구조가 급격히 퇴화되었다. 반면, 혀밑 신경을 절단한 혀 미각샘의 구조는 대조군에 비하여 형태학적 변화를 보이지 않았다. 렉틴조직화학의 결과 대조군에서 혀 미각샘은 ${\alpha}$-D-galactose, N-acetyl-D-galactosamine 및 N-acetyl-D-glucosamine oligomer 성분의 복합당질을 합성하였고, 혀인두신경을 절단한 10일군부터 그 양은 급격히 감소하였다. 그러나, 혀밑신경을 절단한 혀미각샘의 복합당질 양상은 21일군까지 대조군과 차이를 보이지 않았다. 이러한 결과들은 부교감신경섬유를 포함한 혀인두신경이 흰쥐 혀 미각샘의 구조 유지와 분비기능에 중요한 역할을 담당하고 있음을 제시한다.