• Title/Summary/Keyword: processing temperature

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Study of Growth and Temperature Dependence of SnS Thin Films Using a Rapid Thermal Processing (황화급속열처리를 이용한 SnS 박막성장 및 온도의존성 연구)

  • Shim, Ji-Hyun;Kim, Jeha
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.2
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    • pp.95-100
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    • 2016
  • We fabricated a tin sulfide (SnS) layer with Sn/Mo/glass layers followed by a RTP (rapid thermal processing), and studied the film growth and structural characteristics as a function of annealing temperature and time. The elemental sulfur (S) was cracked thermally and applied to form SnS polycrystalline film out of the Sn percursor at pre-determined pressures in the RTP tube. The sulfurization was done at the temperature from $200^{\circ}C$ to $500^{\circ}C$ for a time period of 10 to 40 min. At ${\leq}300^{\circ}C$, 20 min., p-type SnS thin films was grown and showed the best composition of at.% of [S]/[Sn] $${\sim_=}$$ 1 and [111] preferred orientation as investigated from using XRD (X-ray diffraction) analysis and EDS (energy dispersive spectroscopy) and SEM (scanning electron microscopy), and optical absorption by a UV-VIS spectrometer. In this paper, we report the details of growth characteristics of single phase SnS thin film as a function of annealing temperature and time associated with the pressure and ambient gas in the RTP tube.

Electrical Characteristics of HIS Tube Depending on Processing Parameters (공정변수에 따른 초전도 튜브의 전기적 특성)

  • Park, Chi-Wan;Jang, Gun-Eik;Ha, Dong-Woo;Seung, Tae-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.5
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    • pp.468-472
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    • 2005
  • High-temperature Superconductor(HTS) tubes were fabricated in term of different processing variables such as preheating temperature, speed of mold rotation and cooling rate by centrigugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were $1050{\circ}C{\sim}1100{\circ}C\;and\;550{\circ}C\;for\;30\; min$, respectively The mould roating speed was 1000 rpm. A tube was annealed at $840 {\circ}C$ for 72 hours in oxygen atmosphere. The plate-like grains were well developed along the loafing direction and typical grain size was about more than $40{\mu}$. It was found that Ic values increased with increasing the Preheating temperature and speed of mold rotation. While Ic decreased with increasing the cooling rate. The measured Ic in $50mm{\times}70mm{\times}2.5mm$ tube was about 896 Amp.

Design of blood temperature management system using RFID and ubiquitous sensor network (RFID와 USN을 이용한 혈액 온도관리시스템의 설계)

  • Kim, Soo-Jung;Yoo, Sun-Kook;Park, Jung-Jin;Seo, Kuk-Jin;Kim, Hyun-Ok;Bae, Ha-Suk;Chang, Byung-Chul
    • Journal of Sensor Science and Technology
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    • v.15 no.4
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    • pp.291-296
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    • 2006
  • We focus on the solutions to prevent fatal risk to patient's life caused by transfusing blood which is wrong type or has exceeded norm temperature. Also, this study gives priority to the verification of medical safety of using blood, of which management is applied advanced sensor tag technology adopted RFID(Radio Frequency Identification) temperature sensor and USN(Ubiquitous Sensor Network) for temperature management of blood. Therefore, this study can contribute to protect of health of patients who take blood transfusion through construction of basis of new process of blood management.

Actual operation characteristics to evaluate the performance of heat pump outdoor unit in the constant temperature chamber (항온챔버에서 히트펌프 실외기의 성능을 평가하는 실제 운전)

  • Jong-Ryeol Kim
    • Journal of the Institute of Convergence Signal Processing
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    • v.23 no.3
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    • pp.123-128
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    • 2022
  • A lot of research is being done to develop a high-efficiency heat pump to save energy, and research to reduce or eliminate the phenomenon of frost occurring in the outdoor unit coil is also being conducted at the same time. In order to conduct a study that does not cause frost on the outdoor unit of the heat pump regardless of the season, a constant temperature chamber like a general room that can be tested under the same conditions as in the natural state was built. The experiment was conducted by providing an environment similar to the natural state to the outdoor unit of the heat pump installed in the constant temperature chamber. As a result, the lower the outdoor temperature, the lower the efficiency of the heat pump. It wat confirmed that the lower the value, the longer it is.

Effect of Tempering Temperature on Hydrogen Embrittlement of Cr-Mo Low Alloy Steels for High-pressure Gaseous Hydrogen Storage (고압수소 저장용 Cr-Mo계 저합금강의 수소취성에 미치는 템퍼링 온도의 영향)

  • M. S. Jeong;H. C. Shin;S. G. Kim;B. Hwang
    • Transactions of Materials Processing
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    • v.33 no.3
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    • pp.185-192
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    • 2024
  • This study examined how varying tempering temperatures affect the susceptibility of Cr-Mo low alloy steels to hydrogen embrittlement. A slow strain-rate test (SSRT) was carried out on the steels electrochemically pre-charged with hydrogen in order to examine the hydrogen embrittlement behavior. The results showed that the hydrogen embrittlement resistance of the Cr-Mo low alloy steels improved with increasing tempering temperature. Thermal desorption analysis (TDA) revealed that diffusible hydrogen content decreased with increasing tempering temperature, accompanied by a slight increase in the peak temperature. This decrease in hydrogen content was likely due to a reduction in dislocation density which served as reversible hydrogen trap sites. These findings underline the significant role of tempering temperature in enhancing the hydrogen embrittlement resistance of Cr-Mo low alloy steels.

On the new mold structure with multi-point gate for filling-balance mold (다점 핀포인트 금형에서 균형충전이 가능한 사출금형 구조)

  • Kwon, Youn-Suk;Jeong, Yeong-Deug
    • Design & Manufacturing
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    • v.2 no.5
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    • pp.25-29
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    • 2008
  • Almost all injection molds have multi-cavity runner system for mass production, which are designed with geometrically balanced runner system in order to accomplish filling balance between cavity to cavity during processing. However, even though geometrically balanced runner is used, filling imbalance have been observed. Filling imbalance could be decreased by modifying processing conditions such as injections rate, mold temperature, injection pressure, melt temperature that are related to shear, viscosity. In this study, a series of experiment was conducted to investigate filling imbalance variation when modifying runner layout and ploymer and to determine which processing condition influences as the primary cause of filling imbalance in geometrically balanced runner system. The filling imbalance was desreased up to result range of $3{\leq}DFI{\leq}8(%)$ by using a new runner system for balanced filling.

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Relation of weld-quality and core shape in injection molding (사출성형 시 코어 형상과 웰드품질과의 관계)

  • Lee, Gyu-Ho;Choi, Woo-Su;Noh, Keon-Cheol;Jeong, Yeong-Deug
    • Design & Manufacturing
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    • v.8 no.1
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    • pp.23-26
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    • 2014
  • The injection molding is used in more than 70% of total production of plastic products. Weld line in injection molded part is one of the defects in injection molding process. Weld line deteriorates not only appearance quality but also mechanical property. In this study weld quality has been examined according to the injection processing temperature, materials and mold designs. We selected four different materials such as PA, PP, ABS and PS as experimental materials. Weld quality increased as injection processing temperature increases. It was more dependent on materials flow ability. As a result, weld quality incase of rectangular core is better than circular core.

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Experimental study of heat transfer in the surrounding for bubble attached at the upper cooled surface of square cavity using the Thermo-sensitive Liquid-crystal Tracer (열감응액정을 이용한 사각공동내의 상단냉각평판에 형성된 기포 주위의 열전달현상 구명)

  • Kwon, Gi-Han;Eom, Yong-Kyoon
    • Proceedings of the KSME Conference
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    • 2001.06d
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    • pp.509-515
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    • 2001
  • In a square cavity, the flow phenomena in the surrounding of the bubble attached at the upper cooled solid wall were studied by using a thermo-sensitive liquid-crystal tracer and image processing techniques. This method offers the advantage of measuring the entire flow field in a selected plane within the fluid at a given instant of time in contrast to point by point method like T/C. Quantitative data of the temperature were obtained by applying a colour-image-processing to the. visualized image. As the growing of a bubble, In a bubble size appears the flow phenomena which the direction of flow is reversed in the entire temperature and flow field. The observed phenomena are described with regard to thermocapillary convection.

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A Study on Life Assessment for In-Service High-Temperature Components Using Image Processing Technique (컴퓨터 화상처리 기법을 이용한 고온 구조물의 수명평가 연구)

  • 김효진;정재진
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.4
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    • pp.44-50
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    • 1998
  • The creep life fraction can be evaluated by the degree of grain deformation since the grain of Cr-Mo base metal deforms in the direction of stress. The grain deformation method using image processing technique is developed for life assessment of in-service high-temperature components. The new assessment model of grain deformation method is presented to apply to in-service components and is verified by interrupted creep test for ex-serviced material of 1Cr-0.5Mo steel. The proposed model, which is irrespective of stress direction, is to evaluate mean of the absolute deviation for the measured ratios which are diametrical maximum to minimum dimensions for grains.

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Synthesis and Electrical Properties of Barium Uranium Sulfides

  • Sato, Nobuaki;Nakajima, Takeshi;Yamada, Kohta;Fujino, Takeo
    • The Korean Journal of Ceramics
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    • v.5 no.4
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    • pp.348-352
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    • 1999
  • Barium uranium sulfides, $BaUS_3$ and $BaU_2B_5$, were synthesized in a single phase by the reactin of $(Ba, UO_2)(NO_3)_2$ at Ba/U=1 and 0.5 with carbon disulfide at 1273 K for 6 h. They crystallized in orthorhombic structure with space group, Pnma. The lattice parameters a, b and c are 7.493, 10.38 and 7.238$\AA$ for $BaUS_3$ and 7.525, 8.475 and 11.858$\AA$ for $BaU_2S_5$, respectively. The electrical conductivity of these compunds increased with increasing temperature above 200K, below which however, it was nearly temperature independent. The Hall coefficient suggested that they are n-type semiconductors.

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