• Title/Summary/Keyword: pretreatments

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CALIBRATION TRANSFER FROM REFLECTANCE TO INTERACTANCE-REFLECTANCE WITHOUT STANDARDS: USE OF MATHEMATICAL PRETREATMENTS

  • Fernandez Cabanas, Victor-M.;Varo, Garrido;Dardenne, Pierre
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1242-1242
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    • 2001
  • The use of fibre optic probes for NIR quality control in the industry is becoming very important, as it provides a powerful tool to reduce sample analysis time and it facilitates the implementation of on-line analyses. However, most of the applications of fibre optics and probes have been done on suspensions, clear liquids and films, chemical and pharmaceutical products and also on fruits and animal products. Traditional applications of near infrared spectroscopy in agriculture have been developed in reflectance mode and calibration transfer could be an interesting way to reduce efforts. Classical methods for calibration transfer between different instruments involve the use of sealed reference cups, but, as fibre optic analysis does not use cups, it is necessary to develop new methods for calibration transfer without standards (Blank et al., 1996). In this paper, we have studied how the most used mathematical pretreatments (three methods of Multiplicative Scatter Correction, Standard Normal Variate, Detrending and derivatives) and their combinations applied to calibration development can contribute to reduce spectral differences between instruments. Calibration equations were obtained for three sets of cereals (barley, wheat and maize) scanned in reflectance mode and then they were validated with samples analysed in reflectance and interactance-reflectance mode (fibre optic). Preliminary results show how some combination of pretreatments reduce the differences in the predicted values, measured as standard error of differences, facilitating the use of calibrations obtained in reflectance for samples analysed by interactance-reflectance. However, the application of pretreatments is not enough to satisfy the control limits for calibration transfer suggested by Shenk et al. (1992), and it should be necessary to combine them with a specific algorithm for instruments standardization.

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Effect of Kerfing and Incising Pretreatments on High-Temperature Drying Characteristics of Cedar and Larch Boxed-Heart Timbers with Less than 150 mm in Cross Section Size (배할 및 인사이징 전처리가 횡단면 크기 150 mm 이하 삼나무와 낙엽송 수심재의 고온건조특성에 미치는 영향)

  • LEE, Chang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.3
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    • pp.345-363
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    • 2020
  • This study was conducted to identify the effect of kerfing and incising pretreatments on high-temperature drying characteristics of cedar and larch boxed-heart timbers with a cross section of less than 150 mm. The result showed that the pretreatments have made a significant difference regarding surface check and shrinkage. Although the kerfing was suitable as a pretreatment to reduce the occurrence of surface check, the incising was not suitable as a pretreatment since the knives of timber joined together, causing the conversion to the surface checks. The shrinkage showed a significant result that the final moisture content was reduced in the order of incising, kerfing, and kerfing-incising after the drying process based on the pretreatment condition. Twist was more affected by the grain angle than the anisotropy of the juvenile wood, and there was no effect of pretreatments.

Preparation of Lignocellulose Nanofibers from Korean White Pine and Its Application to Polyurethane Nanocomposite (국산 잣나무 유래 리그노셀룰로오스 나노섬유 제조 및 이를 이용한 강화 폴리우레탄 나노복합재료)

  • Jang, Jae-Hyuk;Lee, Seung-Hwan;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.6
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    • pp.700-707
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    • 2014
  • The effect of steam and ozone pretreatments on fibrillation efficiency by wet disk-milling was investigated. Hemicellulose (40%) and lignin (42%) of Korean white pine were partially removed by steam and ozone pretreatments, respectively. With increasing wet disk-milling time, the diameter of fibers was significantly decreased and its size distribution became narrow. Especially, the average diameters of lignocellulose nanofibers after steam and ozone pretreatments were 19 nm and 12 nm, respectively. Thus-obtained lignocellulose nanofibers-reinforced polyurethane composite was prepared. Tensile strength and elastic modulus were drastically improved with increasing wet disk-milling time and lignocellulose nanofiber content. Nanocomposite reinforced by lignocellulose nanofibers after two pretreatments showed higher tensile properties, compared to that reinforced by lignocellulose nanofiber without pretreatment, at the similar wet disk-milling time.

Pretreatments of Softwood Sawdust for Mycelial Growth of Lentinus edodes

  • Kim, Tae-Hong;Lim, Bu-Kug;Chang, Jun-Pok;Yoon, Kab-Hee;Lee, Jong-Yoon;Yang, Jae-Kyung
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.3
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    • pp.109-115
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    • 2002
  • Mycelial growth of L. edodes by pretreatments of softwood was studied on a sawdust medium. The sawdust used was from the following softwood species : Larix leptolepis, Pinus densiflora and Pinus koraiensis. The pretreatment consisted of cold-water (48 h), hot-water (3 h) and steam extractions (3 h) at a ratio of 500 g : 3,000 mL (sawdust : distilled water). The sawdust medium was a mixture of 76% sawdust, 20% rice bran, 3% glucose, 0.4% potassium nitrate and 0.6% calcium carbonate. Following sawdust pretreatments proved most suitable : L. leptolepis (steam extraction), P. densiflora (hot-water extraction) and P. koraiensis (hot-water extraction). Mycelial growth on P. koraiensis sawdust increased in proportion to an increase in hot-water extraction time. Mycelial growth was optimum on the sawdust extracted for 12 hours, hot-water extraction beyond this period proved unsuitable. With the exception of P. densiflora at 100 ㎍/mL, antifungal activity occurred in every sample. Maximum inhibition of mycelial growth was obtained from following concentration of hot-water extractives : P. densiflora (104 ㎍/mL) and P. koraiensis (104 ㎍/mL). This study has provided useful preliminary information for the cultivation of L. edodes.

Microwave-assisted pretreatment technologies for the conversion of lignocellulosic biomass to sugars and ethanol: a review

  • Puligundla, Pradeep;Oh, Sang-Eun;Mok, Chulkyoon
    • Carbon letters
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    • v.17 no.1
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    • pp.1-10
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    • 2016
  • Lignocellulosic biomass conversion to biofuels such as ethanol and other value-added bio-products including activated carbons has attracted much attention. The development of an efficient, cost-effective, and eco-friendly pretreatment process is a major challenge in lignocellulosic biomass to biofuel conversion. Although several modern pretreatment technologies have been introduced, few promising technologies have been reported. Microwave irradiation or microwave-assisted methods (physical and chemical) for pretreatment (disintegration) of biomass have been gaining popularity over the last few years owing to their high heating efficiency, lower energy requirements, and easy operation. Acid and alkali pretreatments assisted by microwave heating meanwhile have been widely used for different types of lignocellulosic biomass conversion. Additional advantages of microwave-based pretreatments include faster treatment time, selective processing, instantaneous control, and acceleration of the reaction rate. The present review provides insights into the current research and advantages of using microwave-assisted pretreatment technologies for the conversion of lignocellulosic biomass to fermentable sugars in the process of cellulosic ethanol production.

Utilization of Osmotic Dehydration as Pretreatment prior to Drying (건조전처리로서 삼투건조의 이용)

  • 윤광섭
    • Food Science and Preservation
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    • v.5 no.3
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    • pp.305-314
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    • 1998
  • In the drying process, many undesirable physicochemical changes occur that influence dried food product qualities. Pretreatments method is used to reduce the deterioration of dried food product qualities such as color, flavor, texture, rehydration ability and retention of nutrients. The methods of pretreatments are blanching, chemical treatment and osmotic dehydration. Osmotic dehydration is a water removal process which is based on placing foods in a concentrated osmotic solution or in a dry osmotic material. A large number of process variables have a significant effect on process and final product quality. In order to improve final product quality it is necessary to know the role of each process variable and understand the mecanisms throughout the process. Osmotic dehydration is a valuable processing tool with great future in minimal processing of fruits and vegetables.

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Study on anti-allergic effects of Arctii Fructus herbal acupuncture (우방자약침(牛蒡子藥鍼)의 항(抗)알러지 효과(效果)에 대한 연구(硏究))

  • Jang, Seok-Chang;Song, Choon-Ho
    • Korean Journal of Acupuncture
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    • v.25 no.1
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    • pp.197-211
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    • 2008
  • Objectives : We studied on anti-allergic effects of Arctii Fructus Herbal Acupuncture(AFHA) and Arctii Fructus Herbal Acupuncture Solution(AF). Methods : In vivo, Animals were herbal-acupunctured AFHA at both ST36 three times for 5 days. Then, we investigated compound 48/80-induced active systemic anaphylaxis(ASA) using ICR mice and anti-DNP IgE-induced passive cutaneous anaphylaxis(PCA) using Sprague Dawley rat. In vitro, we measured cell viability, b-hexosaminidase, IL-4 and TNF-a release from RBL-2H3 cells after treatment of AF of various concentrations. Results : In vivo, AFHA pretreatments at both ST36 inhibited compound 48/80-induced ASA. PCA was inhibited by AFHA pretreatments at both ST36. In vitro, AF treatments were not affect on cell viability and inhibited b-hexosaminidase, IL-4 and TNF-a release. Conclusions : These results suggest that AFHA and AF may be beneficial in the inhibition of allergic inflammatory response.

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ffect of Semen Perillae herbal acupuncture on the type 1 hypersensitivity (소자약침(蘇子藥鍼)이 Type 1 Hypersensitivity에 미치는 영향)

  • Song, Se-Hoon;Song, Choon-Ho
    • Korean Journal of Acupuncture
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    • v.25 no.1
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    • pp.213-227
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    • 2008
  • Objectives : We studied on anti-allergic effects of Semen Perillae Herbal Acupuncture(SPHA) and Semen Perillae Herbal Acupuncture Solution(SP). Methods : In vivo, Animals were herbal-acupunctured SPHA at both ST36 three times for 5 days. Then, we investigated compound 48/80-induced active systemic anaphylaxis (ASA) using ICR mice and anti-DNP IgE-induced passive cutaneous anaphylaxis (PCA) using Sprague Dawley rat. In vitro, we measured cell viability, b-hexosaminidase release, IL-4 and TNF-a from RBL-2H3 cells after treatment of SP of various concentrations. Results : In vivo, SPHA pretreatments at both ST36 inhibited compound 48/80-induced ASA. PCA was inhibited by SPHA pretreatments at both ST36 and optional points. In vitro, SP treatments were not affect on cell viability and inhibited b-hexosaminidase release, IL-4 and TNF-a. Conclusions : These results suggest that SPHA and SP may be beneficial in the inhibition of allergic inflammatory response.

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Ultrafiltration of Oily Wastewater with Surface Pretreated Membranes

  • Kim, Kyu-Jin;Fane, Antony G.
    • Korean Membrane Journal
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    • v.1 no.1
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    • pp.43-49
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    • 1999
  • Separation of soluble oil was investigated during filtration of cutting oil emulsion using various commercial ultrafiltration membranes. The surface properties of membranes used were hydrophilic hydrophobic and modified surfaces by various surfactant pretreatments. Conditions varied include stirring speed transmeembrane pressure membrane type and surfactant type for pretreatment. The results give some indication of mechanisms occurring at the membrane surface. Surfactant pretreatments significantly improved water flux and UF flux of hydrophilic regenerated cellulose(up to 2.4x for YM100) and hydrophobic polysulfone (up to 2.2x for PTHK) membranes depending on surfactant type and operating conditions. The UF flux enhancement was attributed to membrane swelling and reduction of interfacial surface tension between oil droplets and membrane surface. unexpectedly the hydrophilic membranes revealed greater flux enhancement than the hydrophobic membranes. The results also showed a greater improvement in UF flux at lower operating pressure.

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Effect of Radix Asteris Herbal Acupuncture at $BL_{13}$ on the Type I Hypersensitivity (자울약침액(紫菀藥鍼液)의 폐유(肺兪) 처치(處置)가 Type I Hypersensitivity에 미치는 영향)

  • Kwon, Hyuk-Sang;Song, Choon-Ho
    • Journal of Acupuncture Research
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    • v.23 no.5
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    • pp.167-175
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    • 2006
  • Objectives : We studied the effects of Radix Asteris herbal acupuncture solution (RAHAS) on the type I hypersensitivity. Methods : In vivo, we measured compound 48/80 induced active systemic anaphylactic shock, anti-DNP IgE induced passive cutaneous anaphylaxis (PCA) and acetic acid induced microvascular permeability using ICR mice. In vitro, we showed effects on cytotoxicity and ${\beta}$-hexosaminidase release from RBL-2H3 cells. Results : In vivo, RAHAS pretreatments at $BL_{13}$ and optional points inhibited active systemic anaphylactic shock induced by compound 48/80 and microvascular permeability increased by acetic acid. PCA was only inhibited by RAHAS pretreatments at $BL_{13}$. In vitro, RAHAS treatments inhibited ${\beta}$-hexosaminidase release. Conclusion : These results suggest that RAHAS may be beneficial in the prevention of type I hypersensitive inflammatory response.

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