• Title/Summary/Keyword: preparation process

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Preparation of β-FeSi2 Thermoelectric Materials by MA/SPS Process -Formation ofβ-FeSi2Phase- (MA/SPS 공정에 의한 β-FeSi2 열전재료의 제조(I) -β-FeSi2상의 형성-)

  • Kim, Hwan-Tae;Gwon, Yeong-Sun;Lee, Chung-Hyo
    • Korean Journal of Materials Research
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    • v.12 no.3
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    • pp.176-181
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    • 2002
  • Fabrication of ${\beta}-FeSi_2$ was attempted by making use of the combined process of mechanical alloying (MA) and spark plasma sintering (SPS). MA was performed under the Ar gas atmosphere using mixed powders of pure iron and silicon having the mole fraction of 1:2. SPS process was performed at 800-85$0^{\circ}C$ with the applied pressure of 50MPa and the holding time was ranging from 0 to 30min. The mechanically alloyed powder by cyclic operation of rotor for 15hrs consisted of $\varepsilon$-FeSi and Si phases. When this mechanically alloyed powder was sintered by SPS process above 85$0^{\circ}C$, $\varepsilon$-FeSi and ${\alpha}-Fe_2Si_5$ phase were formed. Bulk product sintered at 82$0^{\circ}C$ for 30min consisted of ${beta}-FeSi_2$ phase with a small fraction of $\varepsilon$-FeSi and the density of sintered specimen was 75.3% theoretical density. It was considered that the MA/SPS combined process was effective for the preparation of ${\beta}-FeSi_2$ without heat treatment process after sintering.

Optimization of Slurry Preparation Process for Soft Magnetic Green Sheet (연자성 복합체 후막용 슬러리 제조공정의 최적화)

  • Oh, Sea Moon;Lee, Chang Hyun;Shin, Hyo Soon;Yeo, Dong Hun;Kim, Jin Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.28 no.12
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    • pp.792-796
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    • 2015
  • With high integration of electronic components, power inductors are also miniaturized. Recently, thick film processes for small size power inductors were developed and commercialized. However, the thick film process to prepare soft magnetic green sheets was not reported enough. In this study, we used Fe-Si magnetic and CIP (carbonyl iron powders) as starting materials to lead to a bimodal particle size distribution in the sheet. We proposed a newly developed 'Modified slurry preparation process' to get well dispersed condition even at high solid contents. Using the new process, it was possible to prepare a well dispersed slurry over 70 vol% of solid. BYK-103 was better than BYK-111 as dispersant in this slurry and the optimum amount was 0.6 wt%. The optimized slurry was formed into a sheet by tape casting process and then the sheet was laminated. We conformed that small size powder, large size powder, and epoxy resin were well dispersed in the green sheet.

Real-Time Batch Size Determination in The Production Line (생산 라인에서의 실시간 배치 크기 결정)

  • Na, Kihyun;Kim, Minje;Lee, Jonghwan
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.42 no.1
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    • pp.55-63
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    • 2019
  • This paper develops an algorithm to determine the batch size of the batch process in real time for improving production and efficient control of production system with multiple processes and batch processes. It is so important to find the batch size of the batch process, because the variability arising from the batch process in the production system affects the capacity of the production. Specifically, batch size could change system efficiency such as throughput, WIP (Work In Process) in production system, batch formation time and so on. In order to improve the system variability and productivity, real time batch size determined by considering the preparation time and batch formation time according to the number of operation of the batch process. The purpose of the study is to control the WIP by applying CONWIP production system method in the production line and implements an algorithm for a real time batch size decision in a batch process that requires long work preparation time and affects system efficiency. In order to verify the efficiency of the developed algorithm that determine the batch size in a real time, an existed production system with fixed the batch size will be implemented first and determines that batch size in real time considering WIP in queue and average lead time in the current system. To comparing the efficiency of a system with a fixed batch size and a system that determines a batch size in real time, the results are analyzed using three evaluation indexes of lead time, throughput, and average WIP of the queue.

Preparation and Sinterability of Nano-Size $TiO_2$ Powders Using Supercritical Fluids (초임계 유체를 이용한 나노크기 $TiO_2$ 분말제조 및 소결특성)

  • 송정환;이정석;박인석;임대영
    • Journal of the Korean Ceramic Society
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    • v.37 no.7
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    • pp.625-631
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    • 2000
  • In this study, the characteristics and sinterablities of TiO2 powders which were fabricated on sol-gel process and supercritical fluid process were examined. The powders fabricated on sol-gel process were amorphous. The particle size and shape were changed with the amount of water used for hydrolysis of titanium ethoxide. The powders were changed from amorphous to crystalline by heating at 400℃. The crystalline anatase TiO2 powders were directly prepared in ethanol supercritical fluid condition that temperature was 270±3℃ and pressure was 7.3 MPa. It's primary crystalline size was 20 nm and agglomerated as spherical shape whose size was 0.7∼1㎛. The powders prepared on sol-gel process were not sintered densely at 900℃ because of abnormal grain growth. However, the powders which prepared on supercritical fluid process were sintered densely at the comparatively low temperature of 800℃ by ideal growth of grain, which are fired at 900℃.

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Application of CMP Process to Improving Thickness-Uniformity of Sputtering-deposited CdTe Thin Film for Improvement of Optical Properties (스퍼터링 증확 CdTe 박막의 두께 불균일 현상 개선을 위한 화학적기계적연마 공정 적용 및 광특성 향상)

  • Park, Ju-Sun;Lim, Chae-Hyun;Ryu, Seung-Han;Myung, Kuk-Do;Kim, Nam-Hoon;Lee, Woo-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.375-375
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    • 2010
  • CdTe as an absorber material is widely used in thin film solar cells with the heterostructure due to its almost ideal band gap energy of 1.45 eV, high photovoltaic conversion efficiency, low cost and stable performance. The deposition methods and preparation conditions for the fabrication of CdTe are very important for the achievement of high solar cell conversion efficiency. There are some rearranged reports about the deposition methods available for the preparation of CdTe thin films such as close spaced sublimation (CSS), physical vapor deposition (PVD), vacuum evaporation, vapor transport deposition (VTD), closed space vapor transport, electrodeposition, screen printing, spray pyrolysis, metalorganic chemical vapor deposition (MOCVD), and RF sputtering. The RF sputtering method for the preparation of CdTe thin films has important advantages in that the thin films can be prepared at low growth temperatures with large-area deposition suitable for mass-production. The authors reported that the optical and electrical properties of CdTe thin film were closely connected by the thickness-uniformity of the film in the previous study [1], which means that the better optical absorbance and the higher carrier concentration could be obtained in the better condition of thickness-uniformity for CdTe thin film. The thickness-uniformity could be controlled and improved by the some process parameters such as vacuum level and RF power in the sputtering process of CdTe thin films. However, there is a limitation to improve the thickness-uniformity only in the preparation process [1]. So it is necessary to introduce the external or additional method for improving the thickness-uniformity of CdTe thin film because the cell size of thin film solar cell will be enlarged. Therefore, the authors firstly applied the chemical mechanical polishing (CMP) process to improving the thickness-uniformity of CdTe thin films with a G&P POLI-450 CMP polisher [2]. CMP process is the most important process in semiconductor manufacturing processes in order to planarize the surface of the wafer even over 300 mm and to form the copper interconnects with damascene process. Some important CMP characteristics for CdTe were obtained including removal rate (RR), WIWNU%, RMS roughness, and peak-to-valley roughness [2]. With these important results, the CMP process for CdTe thin films was performed to improve the thickness-uniformity of the sputtering-deposited CdTe thin film which had the worst two thickness-uniformities of them. Some optical properties including optical transmittance and absorbance of the CdTe thin films were measured by using a UV-Visible spectrophotometer (Varian Techtron, Cary500scan) in the range of 400 - 800 nm. After CMP process, the thickness-uniformities became better than that of the best condition in the previous sputtering process of CdTe thin films. Consequently, the optical properties were directly affected by the thickness-uniformity of CdTe thin film. The absorbance of CdTe thin films was improved although the thickness of CdTe thin film was not changed.

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Preparation of Y2O2:Eu Red Phosphor by Sol-Gel and Calcination Process (솔-젤 및 소성공정에 의한 이트륨-유로퓸계 적색형광체 제조)

  • Yoon, Ho-Sung;Kim, Chul-Joo;Jang, Hee Dong
    • Korean Chemical Engineering Research
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    • v.46 no.3
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    • pp.506-511
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    • 2008
  • In this study sol-gel and combustion process was surveyed for the preparation of the red $Y_2O_3$: Eu phosphor, and the properties of phosphor was considered. Chelation and hydrolysis in amorphous citrate sol-gel process were completed in initial reaction stage, and water-forming condensation was superior to organic acid-forming condensation. The mole ratio of citric acid to metal ion had to be above to for the progress of sol-gel process. The dried gel powders are mostly amorphous, and crystallize completely at $700^{\circ}C$, and the crystallinity increases with increasing calcining temperature. The luminescence property of the phosphor was analyzed by measuring the emission spectra. The luminescence intensity increases when the calcination temperature and concentration of metal ions in solution increase.

A Study on the Production of Stage Costume of Musical 'Christmas Carol' (뮤지컬 '크리스마스 캐롤'의 무대의상 제작에 관한 연구)

  • Choi, Young-Ro;Lim, Young-Ja
    • Journal of the Korean Society of Costume
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    • v.57 no.3 s.112
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    • pp.136-149
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    • 2007
  • This study researched the costume manufacture process by having the musical 'Christmas Carol' as an example and specifically presented the costume manufacture process of an actually performance work, thus it aimed to be helpful theoretically and realistically, by allowing theatrical costume manufacturers and majors in theatrical costume to be informed of the systematically practical affair process of the theatrical costume manufacture and by exhibiting the research work of costume composition aiming at reproducing a silhouette in the process such as costume composition and sewing, and the effectively manufacturing methods such as the costume composition application and the sewing method development aiming at the activity of performers. In the empirical research, it analyzed the features of characters and arranged the manufacture points while actually manufacturing the performance costume, and clarified the systematically performance costume manufacture process such as a manufacture meeting${\rightarrow}$costume list preparation$\rightarrow$work-instruction sheet preparation$\rightarrow$pattern manufacture$\rightarrow$sewing$\rightarrow$performance and inspection. Through performing the manufacture of the really performance work, it is hoped that this study contributes to the development of performance art circles, by presenting a step and a method of professionally theatrical costume to the performance manufacturers and the theatrical costume manufacturers at present when the theatrical costume is solidifying its position as a professional sphere, in the performance and an, has a meaning as the initially empirical research, which can exhibit as a guide of realistically and empirically educational contents for theatrical costume aiming to bring up professional staff for theatrical costume, and becomes help in the efficiently theatrical costume manufacture realistically.

Preparation of Metal Injection Molded Dental Components using Spheroidized Ti Powders by Plasma Process (플라즈마 공정으로 구상화된 티타늄 분말과 금속사출성형 공정을 이용한 치과용 부품 제조)

  • Gwak, Ji-Na;Yang, Sangsun;Yun, Jung-Yeul;Kim, Ju-Yong;Park, Seongjin;Kim, Hyun-Seung;Kim, Yong-Jin;Park, Yong-Ho
    • Journal of Powder Materials
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    • v.20 no.6
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    • pp.467-473
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    • 2013
  • This research presents a preparation method of dental components by metal injection molding process (MIM process) using titanium scrap. About $20{\mu}m$ sized spherical titanium powders for MIM process were successfully prepared by a novel dehydrogenation and spheroidization method using in-situ radio frequency thermal plasma treatment. The effects of MIM process parameters on the mechanical and biological properties of dental components were investigated and the optimum condition was obtained. After sintering at $1250^{\circ}C$ for 1 hour in vacuum, the hardness and the tensile strength of MIMed titanium components were 289 Hv and 584 MPa, respectively. Prepared titanium dental components were not cytotoxic and they showed a good cell proliferation property.

Preparation and Characterization of (La, Sr)$MnO_3$ Electrode for High Temperature Steam Electrolysis by Glycine-Nitrate Process (Glycine-Nitrate Process를 이용한 고온 수증기 전해용 (La, Sr)$MnO_3$ 전극의 합성 및 특성 연구)

  • Choi, Ho-Sang;Kim, Hyun-Jin;Ryu, Si-Ok;Hwang, Gab-Jin
    • Transactions of the Korean hydrogen and new energy society
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    • v.18 no.1
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    • pp.46-51
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    • 2007
  • LSM powder material for an oxygen-electrode(anode) of High Temperature Steam Electrolysis (RISE) was synthesized by a Modified-Glycine nitrate process(GNP). Amount of nitric acid and its concentration was varied to find out an appropriate composition for the oxygen-electrode(anode). In order to optimize the amount of Glycine used as an oxidant of self-combustion process, the ratio of Glycine to Anion was varied. $La_{0.8}Sr_{0.2}MnO_3$, $La_{0.5}Sr_{0.5}MnO_3$, and $La_{0.2}Sr_{0.8}MnO_3$ were synthesized in this study. Those LSM were dried for overnight to remove moisture from the material at $110^{\circ}C$ and were calcined 2 hours at $650^{\circ}C$ and were sintered in a furnace for 5 hours at $1400^{\circ}C$. Their structures, surface morphologies, surface areas, and weight changes were investigated with XRD, SEM, BET, and TG/DTA. The best perovskite phase for the oxygen-electrode of HTSE was obtained with $La_{0.8}Sr_{0.2}MnO_3$ formula in which 100 ml of 3M nitric acid was used in the preparation of its formula. The optimized ratio of Glycine to Anion was 2.

A Proposal for Partial Automation Preparation System of BIM-based Energy Conservation Plan - Case Study on Automation Process Using BIM Software and Excel VBA - (BIM기반 에너지절약계획서 건축부문 부분자동화 작성 시스템 제안 - BIM 소프트웨어와 EXCEL VBA를 이용한 자동화과정을 중심으로 -)

  • Ryu, Jea-Ho;Hwang, Jong-Min;Kim, Sol-Yee;Seo, Hwa-Yeong;Lee, Ji-Hyun
    • Journal of KIBIM
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    • v.12 no.2
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    • pp.49-59
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    • 2022
  • The main idea of this study is to propose a BIM-based automation system drawing up a report of energy conservation plan in the architecture division. In order to obtain a building permit, an energy conservation plan must be prepared for buildings with a total floor area of 500m2 or more under the current law. Currently, it is adopted as a general method to complete a report by obtaining data and drawings necessary for an energy conservation plan through manual work and input them directly into the verification system. This method takes a lot of effort and time in the design phase which ultimately increases the initial cost of the business, including the services of companies specialized in the environmental field. However, in preparation for mandatory BIM work process in the future, it is necessary to introduce BIM-based automatic creation system that has an advantage for shortening the whole process to enable rapid permission of energy-saving designs for buildings. There may be many methods of automation, but this study introduces how to build an application using Dynamo of Revit, in terms of utilizing BIM, and write an energy conservation plan by automatic completion of report through Dynamo and Excel's VBA algorithm, which can save time and cost in preparing the report of energy conservation plan compared with the manual process. Also we have insisted that the digital transformation of architectural process is a necessary for an efficient use of our automation system in the current energy conservation plan workflow.