• 한국세라믹학회지
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• 제31권6호
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• pp.637-642
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• 1994

Using SHS(Self-propagating High-temperature Synthesis) method, the optimum synthetic condition of titanium carbonitride was established by controlling the parameters such as relative density of mixture (Ti+C), nitrogen pressure, additive amounts of titanium hydride(TiH1.924) and protecting heat loss. Under 1 atm nitrogen pressure, nitridation ratio with changing relative density of the sample compacts has a maximum (87.2%) at about 55%, and in the case of enveloping the pellet with a quartz tube, the highest nitridation ratio of 90% was obtained at about 68%. At relative density of 55%, nitridation ratio with the nitrogen pressure has a miximum (87.3%) at 7 atm. As the amounts of additive titanium hydride increased, nitridation ratio decreased at below 7 atm nitrogen pressure and, increased at above this pressure until percent of addition percent reached 15 wt% and decreased abruptly upon futher increases in titanium hydride. In the synthesis of TiCxNy by combustion reaction, heat transfer from combustion zone to preheating zone and nitrogen gas penetration into the compact were found to be important factors affecting the TiCxNy formation. It was difficult to obtain high nitridation ratio when the conbustion temperature was either too high or too low, and it seems that the retention of high temperature after a combustion wave sweeped through the reactant mixture pellet is critical to obtain a satisfactory nitridation ratio.

• 한국추진공학회지
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• 제9권4호
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• pp.1-8
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• 2005

과산화수소를 단일추진제로 사용하는 마이크로 추력기를 위한 실험적 연구를 수행하였다. 연구에서 은 촉매 활성화 방법과 메조스케일 반응기의 성능평가에 관한 실험을 하였다. 시도한 여러 가지 활성 방법 중, $500^{\circ}C$의 수소 환원법의 경우 가장 좋은 반응성을 가짐을 확인 하였다. 추진제의 완전한 분해 조건을 찾기 위해 메조스케일 반응기가 제작되었다. 촉매 베드를 위해 지지체로 20 mm 길이의 유리 웨이퍼를 준비하여 은 촉매를 스퍼터링 하였다. 과산화수소 공급 유량에 따라 반응기내 공간시간이 변하므로 유량을 변화시키며 반웅기 실험을 수행하였고 전환율을 측정 하였다. 20 mm 베드 길이에서 추진제의 완전한 분해를 위해 480초 이상의 공간시간이 요구된다.

• 대한수의학회지
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• 제38권3호
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• pp.565-573
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• 1998

To study the specific tools for the diagnosis of Newcastle disease virus (NDV) in chicken, polymerase chain reaction (PCR) and its presumable conditions were evaluated for the detection of hemagglutinin-neuraminidase (HN) gene of NDV RNA. For these purposes, Kyojeongwon strain of the NDV was propagated in allantoic cavity of SPF embryonating chicken eggs, and viral RNA was extracted from fractionated virus after the allantoic fluids were ultracentrifuged with sucrose gradient. The first-strand cDNA was then made for the HN gene of NDV RNA by reverse transcription at $42^{\circ}C$ for 1 hour using specific primer complementary to the HN gene. The single-stranded cDNA was used as template in the PCR of the HN-DNA, and various conditions of the PCR were evaluated to set up method for the specific detection of the HN-DNA. The PCR conditions promising for the detection of HN gene consist of preheating at $94^{\circ}C$, 5 min, 30 cycles of denaturation at $94^{\circ}C$, 1 min, annealing at $55^{\circ}C$, 1 min and polymerization at $72^{\circ}C$, 2 min, and a cycle of extension at $72^{\circ}C$, 5 min. when NDVs of allantoic fluids without fractionation were applied to the above PCR condition, the HN genes were detected effectively not only from Kyojeongwon but from other velogenic strains such as Herts and a field isolate.

• 한국축산식품학회지
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• 제34권2호
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• pp.151-157
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• 2014

This study investigated the effects of three proteases (trypsin, pepsin and chymotrypsin) on the hydrolysis efficiency of porcine placenta and the molecular weight (Mw) distributions of the placental hydrolysates. Because placenta was made up of insoluble collagen, the placenta was gelatinized by applying thermal treatment at $90^{\circ}C$ for 1 h and used as the sample. The placental hydrolyzing activities of the enzymes at varying concentrations and incubation times were determined by sodium dodecyl sulfate polyacrylamide gel electrophoresis (SDS-PAGE) and gel permeation chromatography (GPC). Based on the SDS-PAGE, the best placental hydrolysis efficiency was observed in trypsin treatments where all peptide bands disappeared after 1 h of incubation as compared to 6 h of chymotrypsin. Pepsin hardly hydrolyzed the placenta as compared to the other two enzymes. The Mw distribution revealed that the trypsin produced placental peptides with Mw of 106 and 500 Da. Peptides produced by chymotrypsin exhibited broad ranges of Mw distribution (1-20 kDa), while the pepsin treatment showed Mw greater than 7 kDa. For comparisons of pre-treatments, the subcritical water processing (37.5 MPa and $200^{\circ}C$) of raw placenta improved the efficiency of tryptic digestions to a greater level than that of a preheating treatment ($90^{\circ}C$ for 1 h). Consequently, subcritical water processing followed by enzymatic digestions has the potential of an advanced collagen hydrolysis technique.

• 한국가스학회지
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• 제18권2호
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• pp.28-34
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• 2014

일반적인 천연가스 정압기지에서는 압력제어밸브를 이용하여 고압으로 수송되는 천연가스를 감압하여 내보낸다. 이 과정에서 버려지는 폐압에너지는 터보팽창기를 도입하여 추가적인 전력생산이 가능하나 터보팽창기를 통과하는 유체에서는 감압에 의한 Joule Thompson 효과에 의하여 온도가 급격히 떨어져 파이프라인 외부에 동결을 일으키거나 파이프라인 내부에 메탄하이드레이트와 같은 고체 물질이 형성될 위험이 있다. 현재 터보팽창기를 채용한 천연가스 정압기지에서는 냉열발생에 따른 부작용을 방지하기 위하여 터보팽창기의 전단에 보일러를 설치하여 팽창 전 천연가스를 예열하고 있다. 용융탄산염연료전지와 같은 고온 연료전지는 천연가스를 연료로 사용할 수 있고 친환경적인 고온 배출가스를 방출하며 동시에 추가적인 전력을 생산하여 시스템의 효율을 높일 수 있다. 이 논문에서는 천연가스 정압기지에 용융탄산염연료전지와 터보팽창기를 설치하여 얻을 수 있는 열역학적 이득에 대해서 연구하였다. 연료전지를 기저부하로 사용함에 따라서 얻을 수 있는 이익에 대하여 분석하였다.

• 대한한의학회지
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• 제15권2호
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• pp.241-252
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• 1994

It is known that the pattern of combustion temperature can be classified into preheating, heating. retaining and cooling periods. In this experiment. the authors have studied the heating mechanism by the density of moxa material during the heating and retaining periods. The starting point. the point at which it begins to reach the maximum gradient temperature. the ending point of the heating period. and the ending point of the retaining period were measured in order to get effective stmulation by repetition of moxa-combustion. For the experiment. samples of 300mg. 400mg, and 500mg of moxa material were molded into conical molds with each 10mm in diameter and height resulting in the volume of $0.26cm^3$. The following results were obtained: The $300mg/0.26cm^3$ denstiy sample reached al1 points tested faster than the samples of $400mg/0.26cm^3$ and $500mg/0.26cm^3$ It dose not reveal any statistical differences between $400mg/0.26cm^3$ and $500mg/0.26cm^3$ in the ending point. the point at which it begins to reach the maximum gradient temperature of the heating period or the ending point of the reataining period The only difference shown was in the starting point of the heating period. According to the above results. it is concluded that the lower density moxa material reached each point of the the respective period faster than the high density moxa material.

• 한국정보통신학회논문지
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• 제20권8호
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• pp.1546-1552
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• 2016

일반적으로 치과용 주조기는 불때를 이용하여 합금을 용해하기 때문에 합금의 적절한 용융온도 및 주조시간을 조절하기 어렵고 이로 인해 가스공이나 핀홀과 같은 주조결함을 발생시키며 과열로 인한 보철물의 결함을 보이고 있다. 또한 합금이 용융된 후 주조 시 대부분 투시창이나 비접촉식 온도센서를 부착하여 적절한 주조온도가 되면 작업자가 원심력을 발생하는 버튼을 눌러 도가니에 용융된 합금을 주조링에 주입한다. 이러한 결과로 대부분 주조온도가 너무 높거나 낮아서 주조결함을 많이 발생하고 있으며 균일한 주조체를 얻지 못하고 있는 실정이다. 본 논문에서는 외부의 비접촉식 온도 센서를 이용한 온도계측이 아닌 실제 합금의 사용 온도를 계측할 수 있는 단일 온도센서를 이용한 치과용 고주파 주조기를 개발하였다.

• Journal of Advanced Marine Engineering and Technology
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• 제35권2호
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• pp.244-251
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• 2011

유한요소법을 통하여 유성압연기에 의한 스테인리스 강관 압연공정을 연구하였다. 3개의 롤에 의한 만네스만 공법을 압연공정에 적용하였다. 보통 유성압연은 냉간가공으로 시작하여 열간가공으로 종료되며, 기존의 압출공정에 비해 공정단축과 생산비절감의 장점을 갖고 있다. 압연공정은 다양하고 복합적인 공정변수를 가지고 있으며, 각각의 변수들은 성형결과에 영향을 미친다. 따라서 유성압연의 다양한 공정변수가 해석에 고려되어야 한다. 본 연구에서는 스테인리스 강관성형의 가능성과 생산성을 검토하였고, 소재예열 및 자전속도, 제품두께 변화를 해석에 반영하였다. 스테인리스 강관 압연공정은 성공적으로 시뮬레이션 되었고 최적의 압연조건을 결정하는데 유용할 것이다.

• 한국주조공학회지
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• 제23권3호
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• pp.137-146
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• 2003

The main purpose of this study is to investigate the effects of process parameter on alpha-case formation of Ti and TiAl castings. The previous studies showed that the molten titanium is excessively reactive to the refractory oxide mold, resulting in alpha-caes of the titanium castings regardless of composition of titanium alloys. However, the behavior of the alpha-case formation of TiAl alloy is not consistent with conventional titanium alloy. In order to investigate the alpha-case formation of Ti and TiAl castings with process parameter, especially the associated factors of investment mold such as mold material, binder and mold preheating temperature. An attempt has been made to characterize the alpha-case of titanium casting by using optical microscope, EDS, XRD, EMPA and hardness profiles. The formation of the alpha-case on the surface of pure titanium during investment casting was rather by that of solid solution with metallic element from mold material. The required mold strength was obtained with $CaZrO_3$ because of the possibility of using water soluble binder. However, the separation phenomenon between facing and back-up mold materials should be considered. The interfacial reaction of TiAl alloy showed different behavior from that of pure titanium and $Al_2O_3$ was best mold materials. The effect of binder as well as mold material on the formation of alpha-case was significant.

• 한국분말재료학회지
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• 제18권3호
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• pp.226-237
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• 2011

W-ZrC and W-HfC composite powders were fabricated by the Plasma Alloying & Spheroidization (PAS) method and the powders were sprayed into hybrid coating layers by using Low Vacuum Plasma Spray (LVPS) process, respectively. Microstructure, mechanical properties, and ablation characteristics of the fabricated coating layers were investigated. The LVPS process led to successful production of W-Carbide hybrid coatings, approximately 400 ${\mu}M$ or above in thickness. As the substrate preheating temperature increased from $870^{\circ}C$ to $917^{\circ}C$, the hardness of the W-ZrC coating layer increased due to decreased porosity. Vickers hardness showed higher value (about 108.4 HV) in W-ZrC hybrid coating material compared to that of W-HfC while adhesive strength was found to be similar in both coating layers. The plasma torch test revealed good ablation resistance of the W-Carbide hybrid coating layers. The relatively high performance W-ZrC coating layer at the elevated temperature is thought to be attributed to both the strengthening effect of ZrC particle remained in the layer and the formation of ZrO2 phase with high temperature stability.