• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
• /
• 2001.06a
• /
• pp.2111-2111
• /
• 2001

A chemoinfometrical method for evaluating the quantitative determination of crystallinity one polymorphs based on fourie-transformed near-infrared (FT-NIR) spectroscopy was established. A direct comparison of the data with the ones collected from using the and compared with the conventional powder X-ray diffraction method was performed. [Method] The pPure a and g forms of indomethacin (IMC) were prepared by reportedusing published methods. Six kinds of standard samples obtained by physically mixing of a and g forms. After the powder X-ray diffraction profiles of samples have been measured, the intensity values were normalized to against the intensity of silicon powder as the as an external standard. The calibration curves for quantification of crystal content were based upon the total relative intensity of four diffraction peaks from of the form g crystal. FT-NIR spectra of six calibration sample sets were recorded 5 times with the NIR spectrometer (BRAN+LUEBBE). Chemoinfometric analysis was performed on the NIR spectral data sets by applying the principal component regression (PCR). [Results] The relation between the actual and predicted polymorphic contents of form g IMC measured using by the X-ray diffraction method shows a good straight linen linear relation., and it has slope of 0.023, an intercept of 0.131 and a correlation coefficient of 0.986. PCR analyses wereis was performed based on normalized NIR spectra sets offer standard samples of known content of IMC g form. IMC. A calibration equation was determined to minimize the root mean square error of the predictionthe prediction. Figure 1 shows a plot of the calibration data obtained by NIR method between the actual and predicted contents of form g IMC. The predicted values were reproducible and had a smaller standard deviation. Figure 2 shows that the plot for the predicted transformation rate (%) of form a IMC to form g as measured by X-ray diffractomeoy against to those as measured by NIR method. The plot has a slope of 1.296, an intercept of 1,109, and a correlation coefficient of 0.992. The line represents a satisfactory correlation between the two predicted values of form g IMC content. Thus NIR spectroscopy is an effective method for the evaluation to the pharmaceutical products of quantitative of polymorph.

• Journal of the Korean Society of Tobacco Science
• /
• v.27 no.1 s.53
• /
• pp.94-99
• /
• 2005

To correct the difference of filling volumn for various cut tobacco and puffed stem according to moisture contents, correction equation was estamated by a simple regression analysis. The $R^2$(coefficient of determination) of correction equation was above 0.95. To verify the precision of correction equation, we predicted correction equation of other samples. The filling volumns by the difference of $1\%$ moisture content were $0.018\;~\;0.022cc/g$ (cut tobacco) and 0.060cc/g (puffed stem). The precision of correction equation for various cut tobacco was very high, but that of puffed stem was low due to quality deviation of row stem according to a season.

• Proceedings of the KSR Conference
• /
• 2011.05a
• /
• pp.1074-1079
• /
• 2011

This paper describes the influence on the nonlinear critical speed results of a specific railway vehicle depending on various constraint conditions. In the roller-rig tests, proper constraints are inevitable to safely hold the test vehicles. Particularly, the test results using KRRI roller-rig are more sensitive to constraint conditions because it is a kind of semi-full car type. In this study, nonlinear critical speed of specific vehicle with regards to several constraint cases were predicted by computational analysis and these results were compared to find the suitable constraint conditions. And also the deviation of semi-full car model from actual full car model was investigated. According to the bifurcation analysis, the nonlinear critical speed are dependent with the constraint condition and car-body yaw motion should be free to achieve more accurate results. And the difference between semi-full and full car model was so small that KRRI's semi-full car model are valid as long as the stability is concerned.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.10 no.1
• /
• pp.5-13
• /
• 2007

The trajectory of an current artillery munition is subject to a variety of different error sources resulting in more or less big deviation from the nominal predicted flight path. The 1D CCM(Course Correction Munition) has appeared to solve this problem and the mechanism of 1D CCM is a simple and low cost one using the influence of drag to range behavior of an artillery munition. In the paper 1D CCM concept has been simulated using wind tunnel experiment results of the specified Korean munition with CCF(Course Correction Fuze) and calculated the performance of its rang error reduction. From the simulated results it can be numerically explained that the possibility of adaptation of 1D CCM concept to Korean artillery munitions.

• Proceedings of the KIEE Conference
• /
• 1987.07b
• /
• pp.981-985
• /
• 1987

In this paper, we predicted the quantities of ass output messages with the generalized estimation equation based on regression model. And, to know the generalization of equation, we measured the deviation of errors between the observed and the estimated values. As a result, the proposed equation applied to sample data showed linear characteristics in some cases.

• Proceedings of the Korean Society of Propulsion Engineers Conference
• /
• 2009.11a
• /
• pp.459-468
• /
• 2009

Analysis of the uncertainty to have engineering solution of gas-dynamic and hydrodynamic problems is based on the comparison the prospective engineering solution with experimental result. In this paper, the mathematical model to estimate heat flux along gas-dynamic channel wall and the solution sequence are shown. Statistical information and generalizing experimental characteristics about gas- and hydro-dynamic channels were applied to the mathematical model. As the results, it is possible to draw a conclusion that models of the integrated approach, using the averaged statistical data of generalizing characteristics for a turbulent flow, without consideration of the turbulent mechanism (characteristic pulsations), can predict a nominal operating regime for gas-dynamic and hydrodynamic systems. The probable deviation of operating regime for newly designed the gas-dynamic channel can achieve 20% from a regime predicted on a basis 1-D or 3-D modelling irrespective of a kind of used models.

• Journal of Environmental Science International
• /
• v.10 no.3
• /
• pp.187-194
• /
• 2001

For the purpose of predicting air pollutants concentration in Pusan coastal urban, we used an Eulerian model of flow and dispersion/chemistry/deposition process considering SST effects which estimate through POM. The results of air quality model including emission from various sources show that the seasonal variation pattern of respective pollutants was affected by the seasonal SST fields and local circulation. Horizontal deviation of diurnal SST was 2.5~4K, especially large gradients in coastal region. Through numerical simulation of wind fields we predicted that local circulation prevailed during daytime in summer and nighttime in winter. So high concentration distribution showed toward inland in spring and summer seasons, while high concentration distribution showed at inland near coast in autumn and winter.

• International Journal of Air-Conditioning and Refrigeration
• /
• v.9 no.3
• /
• pp.1-9
• /
• 2001

In this study, condensation heat transfer coefficients (HTCs) of nonazeotropic refrigerant mixtures of HFC32/HFC 134a and HCFC123 at various compositions were measured on a horizontal smooth tube. All data were taken at the vapor temperature of 39$^{\circ}C$ with a wall subcooling of 3~8K. Test results showed that HTCs of tested mixtures were 11.0~85.0% lowed than the ideal values calculated by the mass fraction weighting of the HTCs of the pure components. Thermal resistance due to the diffusion vapor film was partly responsible for the significant reduction of HTCs with these nonazeotropic mixtures. The measured data were compared against thc predicted ones by Colburn and Drew's film model and a good agreement was observed within a deviation of 15%.

• Proceedings of the Korean Nuclear Society Conference
• /
• 1996.05b
• /
• pp.349-355
• /
• 1996

In this study, the mechanistic critical heat flux (CHF) model and correlation for water are derived based on flow excursion (or Ledinegg instability) criterion and the simplified two-phase homogeneous model. The relationship between CHF for the water and the principal parameters such as mass flux heat of vaporization, heated length-to-diameter ratio, vapor-liquid density ratio and inlet subcooling is derived on the developed correlation. The developed CHF correlation predicts very well at the applicable ranges, 1 < P < 40 bar, 1, 300 < G 27, 00 kg/$m^2$s and inlet quality is less than -0.1. The overall mean ratio of predicted to experimental CHF value is 0.988 with standard deviation of 0.046.

• Journal of Korean Society for Quality Management
• /
• v.32 no.1
• /
• pp.144-154
• /
• 2004

The bounded adjustment is known to be more efficient than repeated adjustment when the cost is incurred for engineering process control. The procedure of the bounded adjustment is to adjust the process when the one-step predicted deviation exceeds the adjustment limit by the amount of the prediction. In this paper, two run rules are proposed and studied In order to improve the efficiency of the traditional bounded adjustment procedure. The efficiency is studied in terms of the standardized cost through Monte Carlo simulation when the procedure is operated with and without the run rules. The adjustment procedure operated with run rules turns out to be more robust for changes in the process and cost parameters.