• 제목/요약/키워드: precipitation behavior

검색결과 331건 처리시간 0.026초

마찰교반 용접한 2519Al 합금 용접부의 석출거동 및 미세조직 (Precipitates Behavior and Microstructure of Friction Stir Welded 2519Al Alloy)

  • 배종모;박태원;백두현;김흥주;장웅성
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2006년 추계학술발표대회 개요집
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    • pp.109-111
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    • 2006
  • In this study, microstructure and mechanical properties for the friction stir welded 2519Al-T87 alloy of the thickness of 38.8mm were studied using DSC, OM, SEM and micro hardness tester. DSC analysis show that GP Zone, ${\theta}'$ and $\theta$ phases in upper part and ${\theta}'$ and $\theta$ phase in lower part of the FSW zone. Recrystallized large grains are observed in HAZ, and elongated small and large grain in the TMAZ. In SZ, very small grains forms by high plastic deformation and heat from friction by tool and specimen.

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Epoxidized Polybutadiene as a Thermal Stabilizer for Poly(3-hydroxybutyrate). II. Thermal Stabilization of Poly(3-hydroxybutyrate) by Epoxidized Polybutadiene

  • Choi, Ju-Yol;Lee, Jong-Keun;You, Young;Park, Won-Ho
    • Fibers and Polymers
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    • 제4권4호
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    • pp.195-198
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    • 2003
  • Epoxidized polybutadiene (EPB) was prepared by polybutadiene (PB) with m-chloroperbenzoic acid (MCPBA) in homogeneous solution. EPB was blended with poly(3-hydroxybutyrate) (PHB) up to 30 wt% by solution-precipitation procedure. The thermal decomposition of PHB/EPB blends was studied by thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) and differential thermal analysis (DTA). The thermograms of PHB/EPB blends contained a two-step degradation process, while that of pure PHB sample exhibited only one-step degradation process. This degradation behavior of PHB/EPB blends, which have a higher thermal stability as measured by maximum decomposition temperature and residual weight, is probably due to crosslinking reactions of the epoxide groups in the EPB component with the carboxyl chain ends of PHB fragments during the degradation process, and the occurrence of such reactions can be assigned to the exothermic peaks in their DTA thermograms.

The Influence of Precipitated Phase in Al-4%Cu Alloy under High Magnetic Field

  • Jun, Jiang;Lee, Hyun-Jun;Min, Qi;Park, Won-Jo
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회A
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    • pp.239-243
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    • 2008
  • Nonferrous metals have a very important position in industry. At present, parts of shipbuilding, automobile, and aircraft etc. are designed and manufactured accurately, simultaneity need light-weight and high-strength. Aluminum copper alloys are one kind of typical precipitation hardening alloy which has been widely used. It is interesting to investigate transformation behavior of precipitated phase in such kind of alloys under high magnetic field. Transformation of materials under high magnetic field is many different compared with conventional condition. The author prepared the Al-4%Cu alloy.

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퇴적물 내 비소의 지구미생물학적 거동 연구

  • 이종운;이상우;박지민;김경웅;전효택;정명채
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2006년도 총회 및 춘계학술발표회
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    • pp.111-114
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    • 2006
  • The effects of indigenous bacteria on geochemical behavior of As in As-contaminated sediments (Hwachon mine and Myoungbong mine) after biostimulation with a variety of carbon sources were investigated under anaerobic condition. In Hwachon sediment, As was dramatically extracted from nonsterile sediment with time, reaching the highest concentration of $500{\mu}g/L$. The As leaching was likely caused by microbial dissolution of Fe oxides/oxyhydroxides with which As had been coprecipitated. However, in the case of Myoungbong sediment supplied with glucose, dissolved As decreased with time likely due to production of As sulfide(s) and subsequent precipitation, which resulted from bacterial reduction of $SO_4^{2-}$. The results implied that bacterial in-situ stabilization of As In subsurface has a potential to be practically applied.

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Long-Term Aging Diagnosis of Rotor Steel Using Acoustic Nonlinearity

  • Kim, Chung-Seok;Park, Ik-Keun;Jhang, Kyung-Young;Hyun, Chang-Yong
    • 비파괴검사학회지
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    • 제31권6호
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    • pp.642-649
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    • 2011
  • The long-term aging of ferritic 2.25CrMo steel was characterized using the acoustic nonlinear effect in order to apply to diagnose the degradation behavior of structural materials. We measured the acoustic nonlinearity parameter for each thermally aged specimen by the higher harmonic-generation technique. The acoustic nonlinearity parameter increased with aging time due to equilibrium M6C carbide precipitation, and has a favorable linear relation with Rockwell hardness. This study suggests that acoustic nonlinearity testing may be applicable to diagnostics on strength degradation in rotor steels.

Thermodynamic Model for Partition Coefficients in the Two Protein Systems

  • Jung, Chang-Min;Bae, Young-Chan;Kim, Jae-Jun
    • Macromolecular Research
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    • 제15권7호
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    • pp.682-687
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    • 2007
  • The equation of state developed herein is predicated on a hard-sphere reference with perturbations introduced via a potential function to account for electrostatic forces and for attraction between protein particles. During this process, the generalized Lennard-Jones (GLJ) pair potential function is employed. The GLJ pair potential function is employed to represent the protein-protein interaction in two-protein systems. Via the use of the relation between the equation of state and the chemical potential, the phase behavior in the aqueous two-protein system can be estimated. The partition coefficients can be obtained via these processes. The calculated values of the coefficients agree fairly well with the experimental data in the given pH and ionic strength range, with no additional adjustable model parameters.

진부지역 토석류발생 사면에 대한 침투 및 사면안정 연계해석 (Seepage and Slope Stability Analysis on the Site of Debris-flow at Jinbu Area)

  • 전경재;윤찬영;서흥석
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2009년도 세계 도시지반공학 심포지엄
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    • pp.369-376
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    • 2009
  • Field investigation was performed right after the occurrence of debris flow at Jinbu area. Geomorphic and geotechnical characteristics were investigated and rain fall data were collected. Based on these data, seepage and slope stability analysis was performed to verify the behavior of ground water and factor of safety of the slope according to the rainfall intensity and time. As a results, the minimum value of factor of safety achieved in long time after the moment of maximum precipitation rate. And it is confirmed that the factor of safety is susceptible to ground water level rather than rainfall intensity.

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용융아연 도금욕에서 망간 산화물의 표면석출 거동 (Behavior of the Surface Precipitation of Manganese Oxides during Hot-dip Galvanizing)

  • 이호종;김명수
    • 한국표면공학회지
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    • 제48권1호
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    • pp.27-32
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    • 2015
  • Advanced high strength steels undergo recrystallization annealing in reducing gas atmosphere before galvanizing to improve mechanical properties. The selective oxidations of elements such as Mn, Si, Cr and Al during annealing decrease wettability of liquid zinc, resulting in bare spots and other defects. In this work, Fe-3wt%Mn steel sheet was annealed at $780^{\circ}C$ for 1200 sec. in 5% $H_2-N_2$ atmosphere and then dipped into zinc bath held at $460^{\circ}C$, which contained 0.2wt% dissolved Al. MnO crystallines in the average size of 200 nm were formed on the surface after annealing. It is estimated that MnO has been detached into bath with the formation and growth of inhibition layer with longer immersion time during galvanizing. No evidence of aluminothermic reduction of MnO has been found in this study.

Fabrication of Nano-sized Titanate Powders by an Ethylene Glycol Solution Route

  • Lee, S.J.;Lee, M.J.;Yoon, Y.S.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.440-441
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    • 2006
  • Several titanate powders ($Al_2TiO_5,\;SrTiO_3$, etc.) were synthesized by an ethylene glycol solution route. Titanium isopropoxide and nitrate salts were dissolved in stoichiometric proportions in liquid-type ethylene glycol without any precipitation. The parent precursor sols were dried to porous gels, and then the gels were calcined and crystallized. All synthesized titanate powders had stable crystallization behavior at low temperature and high specific surface area after a simple ball-milling process. A three-component PZT $(Pb(Zr_{0.52}{\cdot}Ti_{0.48})O_3)$ powder was also synthesized successfully by the ethylene glycol method. In this study, the characteristics of the multi-component titanate powders by the ethylene glycol method are examined.

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초극저탄소 Cu강화형 자동차용 강판 변형시효에 미치는 Aluminum 및 고용질소의 영향 (Effect of Aluminum and Solute N on the Strain Aging of Extremely Low-Carbon Automotive Steel Strengthened with Cu sulfide)

  • 홍문희;양혜미;송승우;한성호
    • 대한금속재료학회지
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    • 제47권2호
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    • pp.71-78
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    • 2009
  • The precipitation behavior of solute carbon and nitrogen strongly affects the mechanical properties of low-carbon automotive panel. In the present study, the effects of aluminum and solute nitrogen on the bake hardenability and strain aging of extremely low-carbon steel with carbon content below 15 ppm has been investigated. The ferrite grain size and distribution of precipitates were varied with the amount of aluminum content of 0.003 to ~ 0.100 wt% in a constant solute carbon and nitrogen. With increasing the aluminum content, the ferrite grain size is increased and strain aging is delayed. The strain aging is also delayed by increasing the annealing temperature, although the ferrite grain size is not much changed.