• 제목/요약/키워드: pre-treatment condition

검색결과 352건 처리시간 0.027초

안정화 열처리에 의한 Al-4.8Zn-1.3Mg계 합금 압출재 특성 평가 (Characterization of Extrusion Parts for after Pre-aging Treatment in an Al-4.8Zn-1.3Mg Alloy)

  • 이창연
    • 한국기계기술학회지
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    • 제20권6호
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    • pp.818-823
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    • 2018
  • In this study, the effect of pre-aging treatment for inhibition of natural aging of Al-4.8Zn-1.3Mg alloy by extrusion process was investigated. Firstly, the as-cast microstructure of Al-4.8Zn-1.3Mg alloy billet and its evolution during homogenization($460^{\circ}C$, $4h+510^{\circ}C$, 5h) were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), hardness analysis. The as-cast microstructures of Al-4.8Zn-1.3Mg alloy reveal $Mg_2Zn$, $Al_5Cu$, $Al_{13}Cu$ formed between dendrities. After homogenization, MgZn, $Al_4Cu$, $Al_{13}Cu$ phases precipitated into the matrix. In addition, standard deviation of homogenized billet was improved than as-cast billet from 2.62 to 0.99. According to pre-aging($100^{\circ}C$, 1h) Al-4.8Zn-1.3Mg alloy by extrusion process, yield strength and tensile strength deviation improved more than condition by natural aging.

명시적 교수와 암시적 교수가 요청 화행 전략 표현 학습에 미치는 효과 비교 연구 - 중국인 한국어 학습자를 대상으로 - (The effects of explicit and implicit pragmatic instruction in Korean request strategies for Chinese learners)

  • 이연경
    • 한국어교육
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    • 제25권1호
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    • pp.115-144
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    • 2014
  • The purpose of this paper is to compare the two different instruction methods for Korean learners of academic purposes in learning request expression. Participants were divided into two groups, explicit and implicit group. Both groups viewed several scenes from the drama that involved native speakers interacting in different situations. The instructional treatment for the explicit group included metapragmatic information while the treatment for the implicit group did not. On the other hand, the treatment for the implicit group followed implicit techniques, which were repetition of the video presentation and a script reading activity. This study was made up of a pre-test, a post-test, and a delayed-test. The pre-test was conducted prior to the instructional treatment. The post-test was administered a day after the last instruction and the delayed-test was conducted five weeks after the treatments. Two types of tests, speaking and writing, were used in this study to examine subjects' knowledge of Korean request. The result of this research reveals that implicit treatment was more effective than explicit treatment in Korean learners' request acquisition. This results might have been due to the operationalization of the implicit condition in this study. Implicit instruction may help language learners make rules by themselves through tasks.

무전해 Ni-P 두께와 Assembly Process가 Solder Ball Joint의 신뢰성에 미치는 영향 (Effects of the Electroless Ni-P Thickness and Assembly Process on Solder Ball Joint Reliability)

  • 이지혜;허석환;정기호;함석진
    • Journal of Welding and Joining
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    • 제32권3호
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    • pp.60-67
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    • 2014
  • The ability of electronic packages and assemblies to resist solder joint failure is becoming a growing concern. This paper reports on a study of high speed shear energy of Sn-4.0wt%Ag-0.5wt%Cu (SAC405) solder with different electroless Ni-P thickness, with $HNO_3$ vapor's status, and with various pre-conditions. A high speed shear testing of solder joints was conducted to find a relationship between the thickness of Ni-P deposit and the brittle fracture in electroless Ni-P deposit/SAC405 solder interconnection. A focused ion beam (FIB) was used to polish the cross sections to reveal details of the microstructure of the fractured pad surface with and without $HNO_3$ vapor treatment. A scanning electron microscopy (SEM) and an energy dispersive x-ray analysis (EDS) confirmed that there were three intermetallic compound (IMC) layers at the SAC405 solder joint interface: $(Ni,Cu)_3Sn_4$ layer, $(Ni,Cu)_2SnP$ layer, and $(Ni,Sn)_3P$ layer. The high speed shear energy of SAC405 solder joint with $3{\mu}m$ Ni-P deposit was found to be lower in pre-condition level#2, compared to that of $6{\mu}m$ Ni-P deposit. Results of focused ion beam and energy dispersive x-ray analysis of the fractured pad surfaces support the suggestion that the brittle fracture of $3{\mu}m$ Ni-P deposit is the result of Ni corrosion in the pre-condition level#2 and the $HNO_3$ vapor treatment.

대기압 플라즈마를 이용한 고분자 소재의 표면개질 (Surface Modification of Polymeric Material Using Atmospheric Plasma)

  • 심동현;설수덕
    • 폴리머
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    • 제32권5호
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    • pp.433-439
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    • 2008
  • 고분자 소재에 평판형 플라즈마 전처리 방식을 적용시켜 polyurethane foam(density : 0.27)과 rubber (butadiene rubber) 소재 표면의 접촉각 및 접착력을 향상시켰다. 플라즈마 반응기의 최적의 반응조건을 조사하기 위해서 전처리기류(질소, 아르곤, 산소, 공기), 기류의 유량($30{\sim}100\;mL/min$), 그리고 전처리 시간($0{\sim}30\;s$) 등을 변화시켜 전처리하고 polyurethane foam의 경우 진공식 플라즈마처리 방식과 상호 비교하였다. 분위기 기류인 $N_2$의 유량을 100 mL/min로 설정 후 polyurethane foam은 10 s, rubber는 3 s 동안 전처리 했을 때 가장 높은 접착박리강도를 나타내었다. 전처리 후 소재의 표면 변화는 SEM과 ATR-FTIR을 이용하여 측정하였다. 결과적으로 평판형 플라즈마 조작 방식에 의한 처리로 소재 표면의 젖음성과 접착박리강도가 개선되었음을 확인하였다.

GC-MS를 이용한 식물홀몬 분석 (Analysis of Plant Hormones using GC-MS)

  • 조광연
    • 한국작물학회지
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    • 제34권s01호
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    • pp.26-32
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    • 1989
  • The analytic principles of GC and MS were explained in relation to plant hormone analyses and the characteristics of two instruments were compared. The selection of column, condition of measurement and the method of ionization to get a good spectrum were also briefly described. Finally, the pre-treatment of sample by solvent extraction method to remove the unnecessary part of sample and the synthetic method, especially reagents and reaction condition, for the preparation of ether or ester derivative which can be easily vaporized in GC were explained.

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열화학적 가수분해 영향인자에 따른 물리화학적 특성 변화 및 혐기성소화 효율 평가 (Variation in Physicochemical Properties and Anaerobic Digestion Efficiency by Thermal-alkali Pre-treatment (THAP) Factors)

  • 박세용;한성국;송은혜;김충곤;이원배
    • 유기물자원화
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    • 제27권3호
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    • pp.27-39
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    • 2019
  • 본 연구에서는 음식물류 폐기물과 하수슬러지의 효과적인 병합 혐기성 처리를 위한 열화학적 가수분해 방법의 최적 조건 평가와, 열화학적 가수분해에 따른 병합 혐기성 소화 효율에 대해 평가 하였다. 열화학적 가수분해는 온도 (80, 100, 120, 140, 160, $180^{\circ}C$)와 NaOH (5, 20, 40, 60, 100 meq/L) 조건에 따른 solubilization COD, CST(Capillary Suction Time), TTF(Time to Filter), volatile fatty acids (VFAs) 등에 대해 평가를 하였으며, 병합 혐기성 소화 효율평가는 biochemical methane potential (BMP) test를 통해 평가하였다. 실험결과 음식물류폐기물과 하수슬러지의 열화학적 가수분해 시 온도 $140^{\circ}C$, NaOH 60 meq/L에서 solubilization COD 20 % 이상, CST와 TTF가 60초 이하, VFAs 농도가 12,000 mg-COD/L 이상으로 최적조건으로 규명되었다. 병합 혐기성 소화 결과도 열화학적 가수분해 조건과 동일한 조건에서 가스발생량이 가장 높았다. 따라서, 음식물류폐기물과 하수슬러지의 효과적인 병합혐기성소화를 위한 열화학적 가수분해 전처리 조건은 온도 $140^{\circ}C$, NaOH 주입농도 60 meq/L라 판단된다.

Influence of Infrared Radiationon Sowing Quality and Growth Indicators of Winter Wheat Plants

  • Chervinsky, L.;Storozhuk, L.;Pashkovska, N.
    • 식품보건융합연구
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    • 제6권1호
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    • pp.17-20
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    • 2020
  • Wheat is the most abundant crop in the world, accounting for one third of the world's population diet. In Ukraine, wheat is in fact, in addition to its nutritional value, a national symbol of the state. Therefore, the main thesis on the development of modern plant growing in Ukraine is the reduction of costs and the introduction of innovative technologies. The quality of grain and seed depends on many factors, namely: agro-climatic conditions, sowing condition of the seed material, quality characteristics of the soil, yielding properties of seeds, pre-sowing seed treatment. etc. For this purpose, the photosynthesis and intensity of photosynthesis need to be limited to the width of the leaf and the height of the leaves by a smaller cut of the stem. It is extremely important to ensure that the head and side pagons of wheat are in good condition. All parameters are often secured by the technology of grain preparation before delivery. Prior to this technology, it is possible to introduce processing of the material in the form for the development of the material. This article presents the effectiveness of the use of infrared irradiation for the pre-sowing treatment of winter wheat seeds in Sekobra Research, Germany.

공주 축산폐수공공처리장에서의 바이오가스-마이크로터빈 분산발전시스템 개발 (Biogas-Microturbine Distributed Generation Developement at Gong-Ju Public Livestock Wastewater Treatment Facility)

  • 박정극;허광범;이기철;강호;임상규
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2008년도 춘계학술대회 논문집
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    • pp.229-234
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    • 2008
  • Korea Electric Power Corporation (KEPCO) has started the nation's first biogas-microturbine project in the city of Gongju as an effort to encourage the utilization of wasted biogas containing useful energy source in the form of $CH_4$. The goal of the project is to set up the biogas microturbine co-generation system for utilizing biogas as an energy source and improving the economics of the wastewater treatment plant. Wastewater treatment processes were investigated in depth to find improvement possibility. Changes in internal recirculation ratio and pre-treatment degree are needed to optimize plant operation and biogas production. Biogas pre-treatment system satisfies Capstone's fuel condition requirement with the test result of 99.9% and 90.2% of hydrogen sulphide and ammonia is removal performance. Installation of microturbine and manufacture of heat exchanger to warm anaerobic digester has been done successfully. Expected economic profit produced by the system is coming from energy saving including electricity 115,871kWh/year and heat contained in exhaust gas 579GJ/year.

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소방의 매염 및 염색특성에 관한 연구 (A Study on the mordanting and dyeing properties of Caesalpinia Sappan, L.Dye)

  • 주영주
    • 복식
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    • 제36권
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    • pp.109-119
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    • 1998
  • For the purpose of standardization and practicability of natural dyeing, the mordanting and dyeing properties of Caseaslpinia Sappan, L. and Brazilin were studied. Appropriate extraction, dyeing and mordanting condition of Caeaslpinia Sappan, L. were determined, and the effect of mordanting method on dye up-take adn color fastness of dyed fabric was investigated. The most absorbance of Caeaslpinia Sappan, L. solution was 445nm, Brazilin was 448nm. The color of bazilin solution was affected by pH 7~9. The optimum temperature to extract Caesalpinia Sappan, L. was 10$0^{\circ}C$ adn dyeing solution for 1 hour. In case mordants concentration, the most absorbance was 0.3%. In case mordanting test, the best and proper temperature to quantities of absorbed mordants in silk was 8$0^{\circ}C$ and the most quantities of absorbed mordants in silk was mordant treatment by Cu. Effective dyeing time to silk was 60min. Effective mordanting temperature was 8$0^{\circ}C$, and its time was 30min. K/S value of dyeing fabrics was recoginazed by mordanting treat-ment, specially Fe, Sn, Al, Cu. K/S value of pre-mordanting was higher than post-mordanting. After soaping treatment K/S value of pre- and post-mordanting silk was decreased and 0.1%(W/V) quantity of mordant was sufficient for treatment. In the case of Caeaslpinia Sappan, L. fastness was increased by mordanting treatment. Mordants and mordanting treatment method affected the amount of absorption and color change of dyed silk.

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CBCT 기반 폐 종양 정위 신체 방사선 요법(SBRT)에서 치료 전·후 set up 에러의 정확도 평가 (Accuracy Evaluation of Pre- and Post-treatment Setup Errors in CBCT-based Stereotactic Body Radiation Therapy (SBRT) for Lung Tumor)

  • 장은성;최지훈
    • 한국방사선학회논문지
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    • 제15권6호
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    • pp.861-867
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    • 2021
  • SBRT는 1회나 또는 3~5회에 걸쳐 치료 Fraction이 30분에서 최대 1시간 걸리므로 치료 중 자세오차가 발생할 가능성이 있다. 이러한 set-up의 오차를 줄이고 정확한 선량을 주기위해 SBRT 환자 치료 시 치료 전 CBCT를 사용하여 보정 후 좌표 값들을 적용하여 치료한 값과 치료 후 긴 치료시간으로 인해 자세 움직임 여부를 확인하기 위해 다시 CBCT를 촬영하여 치료 전.,후 오차 값들의 유용성을 평가하고자 한다. 계통오차 범위는 평균적으로 X, Y, Z축에서 0.032~0.17 cm으로 나타나 치료 후에도 움직임의 변화가 매우 적음을 확인하였다. 호흡동조에 의한 종양 중심체 변화 (±SD)는 X, Y 및 Z 방향에서 0.11(±0.12) cm, 0.27(±0.15) cm, 0.21cm(±0.31cm)였다. 종양 에지 (±SD)은 각각 X, Y및 Z 방향에서 0.21(±0.18) cm, 0.30(±0.23) cm, 0.19cm(±0.26) cm이었다. 종양 교정된 변위의 (±SD)은 각각 RL, AP 및 SI 방향에서 0.03(±0.16) cm, 0.05(±0.26) cm, 0.02(±0.23) cm이었다. 3차원 벡터 값의 범위는 치료 전과 CBCT를 비교했을 때 평균적으로 0.11~0-.18 cm 교정된 셋업 오차는 0.3 cm 이내에 있음을 확인하였다. 따라서, 일부 나이가 많은 환자, 치료 당일 컨디션, 체형에 따라 다소 값들의 변화가 있었지만 유의 범위 내에 있음을 확인하였다.