• Title/Summary/Keyword: pre-heat treatments

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A Study on the Gettering in Czochralski-grown Single Crystal Silicon Wafer (Czochralski 법으로 성장시킨 실리콘 단결정 Wafer에서의 Gettering에 관한 연구)

  • 양두영;김창은;한수갑;이희국
    • Journal of the Korean Ceramic Society
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    • v.29 no.4
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    • pp.273-282
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    • 1992
  • The effects of intrinsic and extrinsic gettering on the formation of microdefects in the wafer and on the electrical performance at near-surfaces of three different oxygen-bearing Czochralski silicon single crystal wafers were investigated by varying the combinations of the pre-heat treatments and the phosphorus diffusion through the back-surface of the wafers. The wafers which had less than 10.9 ppma of oxygen formed no gettering zones irrespective of any pre-heat treatments, while the wafers which had more than 14.1 ppma of oxygen and were treated by Low+High pre-heat treatments generated the gettering zone comprising oxygen precipitates, staking faults, and dislocation loops. The effects of extrinsic gettering by phosphorus diffusion were evident in all samples such that the minority carrier lifetimes were increased and junction leakage currents were decreased. However, the total gettering effects among the different pre-heat treatments did not necessarily correspond to the gettering structure revealed by synchrotron radiation section topograph.

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Water Absorption and Dimensional Stability of Heat-treated Fast-growing Hardwoods

  • PRIADI, Trisna;SHOLIHAH, Maratus;KARLINASARI, Lina
    • Journal of the Korean Wood Science and Technology
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    • v.47 no.5
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    • pp.567-578
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    • 2019
  • A common problem with fast-growing hardwoods is dimensional instability that limits use of their wood. In this study, we investigated the effects of pre-drying methods, temperatures, and heating duration on the specific gravity, water absorption, and dimensional stability of three tropical fast-growing hardwoods, jabon (Neolamarckia cadamba Roxb.), sengon (Falcataria moluccana Miq.), and mangium (Acacia mangium Willd.). Wood samples were pre-dried by two methods (fan and oven at $40^{\circ}C$), and heat treatments were performed at three temperatures (120, 150, and $180^{\circ}C$) for two different time periods (2 and 6 hours). The specific gravity, water absorption, dimensional stability, and structural changes of the samples were evaluated. The results revealed that heat treatments slightly reduced the specific gravity of all three wood species. In addition, the heat treatments reduced water absorption and significantly improved dimensional stability of the samples. Oven pre-drying followed by heat treatment at $180^{\circ}C$ for 6 hours resulted in good physical improvement of jabon and sengon wood. Fan pre-drying followed by heat treatment at $180^{\circ}C$ for 2 hours improved the physical properties of mangium wood. The heat treatment shows a promising technique for improving the physical characteristic of fast growing hardwoods.

Effects of pre-heat treatments on the quality of cut kimchi cabbages during short-term storage (절단배추의 단기 저장에 대한 예열처리 효과)

  • Kim, Sang-Seop;Ku, Kyung-Hyung;Jeong, Moon-Cheol;Hong, Joo-Heon;Chung, Shin-Kyo
    • Food Science and Preservation
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    • v.21 no.6
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    • pp.776-783
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    • 2014
  • Kimchi cabbages were cut ($3{\times}3cm$), and were pre-heat treated at $40^{\circ}C$, and their physicochemical qualities and browning degrees were investigated during 8 weeks storage at $5^{\circ}C$. The Cut kimchi cabbages were treated at $40^{\circ}C$ (1~8 hrs) and their protein bands profiles were determined by sodium dodecyl sulfate polyacrylamide electrophoresis (SDS-PAGE). The 60, 39, 33, and 12 kDa bands considered heat shock proteins (HSPs) were expressed in the cut kimchi cabbage, and the 4-hr pre-heat treatment (HS 4) exhibited the strongest band ratio. The weight ratios and titratable acidities of the pre-heat treated cut kimchi cabbages were not changed so much after 8 weeks storage at $5^{\circ}C$, and the soluble solid contents of HS 4 decreased less than that of any other treatments. The browning degree of HS 4 after 8 week storage was also shown to be the least among the treatments. The polyphenol oxidase (PPO) activities of all treatments slightly rose during the over all storage period, in contrast with the decrease of total phenolic contents. The expression of HSPs was identified in the pre-heat treated cut kimchi cabbages, and HS 4 exhibited the best quality and appearance after 8 weeks storage at $5^{\circ}C$.

Development of Pre-heat-treated High Strength CHQ Wires and Forming Technology for them (고강도 냉간압조용 선조철강 및 제품화 기술 개발)

  • Yoon, D.J.;Kim, E.Z.;Ahn, S.T.;Son, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.35-36
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    • 2009
  • Development trend and current status were surveyed for pre-heat-treated high strength cold heading quality (CHQ) wire and it's forming technology. Spheroidizing, quenching, and tempering heat treatments are eliminated by adapting the pre-treated wire, which could reduce energy consumption rate and green house gas emission rate during produce parts requiring high strength. There are some challenging problems to expand application area such as enhancing forming tool life, and preventing delayed failure. Domestic research movement concerning the development and application of the new high strength wire was introduced.

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A Study on the Wave Formation and Hair Damage Levels Relating to the Uses of Treatments for Heat Permanent Waves

  • Kim, Kwan-Ok;Kim, Sung-Nam
    • Journal of Fashion Business
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    • v.12 no.6
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    • pp.1-10
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    • 2008
  • Public interest in healthy hairs gets growing as damaged hairs are seen more frequently with the generalization of heat permanent waves. For this study, experiments have been conducted to understand the influences on the changes in physical and morphological features of wave forms and damaged hairs, by collecting virgin hairs from the women in their mid-20's, who had not experienced chemical applications, and by dividing the applications of heat perm hair treatments, PPT(for pre-treatment) and LPP(for post-treatment), into the pre-treatment, the post-treatment, the pre & post-treatment, and the non-treatment. For the wave formations, curl waves were investigated by the bare eyes using the pictures taken by a digital camera. For the comparison of physical features, the experiments of tensile strength and elongation were done and their mean values were found. For the observations of morphological features, the pictures were taken by SEM for comparison. As for the findings, regarding the curl wave shapes of hairs, the most even and elastic S curl was formed in the case of non-treatment. In the physical features, both of the tensile strength and elongation showed a decreasing tendency in line with the hair damage levels, and the case of the pre & post-treatment indicated the tendency most similar to the control group. In the morphological features of the cuticle, observed with an SEM, the pre-treatment showed the higher possibility of reducing the cuticle damages than the post-treatment did. LPP was found to play the role of protective membrane for the post-treatment, and the pre & post-treatment turned out to reduce most effectively the cuticle damages.

A Study on the Microstructure and Hardness of Al-Si-Mg Alloys upon Heat Treatments (Al-Si-Mg계 합금의 열처리에 의한 미세조직과 경도 변화)

  • Lee, Se-Jong;Lee, Sung-Kwan;Baik, Nam-Ik
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.2
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    • pp.108-114
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    • 2000
  • The effects of heat treatments in Al-Si-Mg alloys on the microstructure and hardness have been investigated by the optical microscope, scanning electron microscope(SEM), and Rockwell hardness tester. The materials of various compositions are melted in a vacuum induction furnace under argon atmosphere. Five different Al alloys are prepared from commercial purity aluminium, magnesium and Al-25Si alloy. Two types of aging treatments are performed: i) Isothermal aging of the specimens at $150^{\circ}C$, $170^{\circ}C$ and $190^{\circ}C$. ii) Pre-aging of the specimens at $60^{\circ}C$, $80^{\circ}C$ and $100^{\circ}C$, and followed by final-aging at $170^{\circ}C$ and $190^{\circ}C$. After the heat treatments, Rockwell hardness are measured with all the specimens.

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Effect of Pre-Aging Conditions on Bake-Hardening Response of Al-0.4 wt%Mg-1.2 wt%Si-0.1 wt%Mn Alloy Sheets

  • Lee, Kwang-jin;Woo, Kee-do
    • Korean Journal of Metals and Materials
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    • v.49 no.6
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    • pp.448-453
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    • 2011
  • Pre-aging heat treatment after solution heat treatment (SHT) of Al-0.4 wt%Mg-1.2 wt%Si-0.1 wt%Mn alloy sheets for auto-bodies was carried out to investigate the effect of pre-aging and its conditions on the bake-hardening response. Mechanical properties were evaluated by a tensile and Vickers hardness test. Microstructural observation was also performed using a transmission electron microscope (TEM). It was revealed that pre-aging treatments play a great role in the bake-hardening response. In addition, it was found that the sphere-shaped nanosized clusters that can directly transit to the needle-shaped ${\beta}$" phase during the paint-bake process, not being dissolved into the matrix, are formed at 343 K. The result, reveals that the dominant factor of the bake-hardening response is the pre-aging temperature rather than the pre-aging time.

Effect of process type and heat treatment conditions on warm hydroformability (온간액압성형특성에 미치는 압출제조공정과 열처리 조건의 영향)

  • Yi, H.K.;Kwon, S.O.;Park, H.K.;Yim, H.S.;Lee, Y.S.;Moon, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.132-135
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    • 2007
  • In this study, hydroformability and mechanical properties of pre- and post- heat treated Al6061 tubes at different extrusion type were investigated. For the investigation, as-extruded, full annealed and T6-treated Al6061 tubes at different extrusion type were prepared. To evaluate the hydroformability, uni-axial tensile test and free bulge test were performed at room temperature and $250^{\circ}C$. Also mechanical properties of hydroformed part at various pre- and post-heat treatments were estimated by tensile test. And the tensile test specimens were obtained from hexagonal prototype hydroformed tube at $250^{\circ}C$. As for the heat treatment, hydroformability of full annealed tube is 25% higher than that of extruded tube. The tensile strength and elongation were more than 330MPa and 12%, respectively, when hydroformed part was post-T6 treated after hydroforming of pre- full annealed tube. However, hydroformed part using T6 pre treated tube represents high strength and low elongation, 8%. Therefore, the T6 treatment after hydroforming for as-extruded tube is cost-effective. Hydroformability of Al6061 tube showed similar value for both extrusion types. But flow stress of seam tube showed $20{\sim}50MPa$ lower value.

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Effects of Special Heat Treatments and Alloying Elements on the Microstructures and Mechanical Charateristics of ADI (ADI의 미세조직과 기계적 특성에 미치는 특수열처리 및 합금원소의 영향)

  • Kim, Sug-Won;Han, Sang-Won;Lee, Ui-Jong;Park, Jin-Sung;Woo, Kee-Do;Lim, Dong-Keun
    • Journal of Korea Foundry Society
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    • v.22 no.2
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    • pp.69-74
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    • 2002
  • The effects of heat treatments and alloying elements on the microstructure and mechanical charaterisitics of specially austempered ADIs containing alloying elements such as Cu, Mo and Ni were investigated. To compare with the effect of conventional and normal(CN) austempering treatment, two kinds of special austempering treatments which are those with pre-quenching and pre-heating were conducted. The hardness and uniaxial fatigue tests were carried out to evaluate the mechanical charateristics. The hardness of ADI treated by CN heat cycles was higher than those of other ADIs. Cu added ADI (Cu-ADI) tempered at 400 after austenitizing exhibited the highest fatigue life cycles. While austempering after prequenching makes the austenite with high carbon stable, which resulted in transformation to highly strengthened bainites from the carbon enriched austenite phases during tempering. The high carbon enriched banites is considered to improve the fatigue strength.

Effect of Heat Treatments on Welding Residual Stresses of AISI 4130 Steel (AISI 4130강의 용접잔류응력에 미치는 열처리의 영향)

  • 양영수;나석주;김원훈;조원만
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.15 no.6
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    • pp.1982-1989
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    • 1991
  • The effect of heat treatments were considered on the residual stress fields of AISI 4130 weldments. In experiments, various heat treatments such as preheating, postheating, stress relieve annealing and hardening treatment were carried out for the GTA weldments and the residual stress was measured by using the hole drilling method. The post weld heat treatment at 230.deg.C, which aimed mainly to prevent the possible weld cracking, was found to have only a negligible effect on the welding residual stress distribution, while the annealing treatment at 600.deg.C almost completely removes the residual stress. It was also revealed that the hardening treatment causes no further residual stresses in weldments.