• Journal of the Korean Crystal Growth and Crystal Technology
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• v.27 no.6
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• pp.295-302
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• 2017

In this study, the effect of pre-curing process on the enhancement of mechanical properties of IGCC-slag-based-geopolymer was studied. Pre-curing is a process in which the green geopolymer is left at room temperature for a certain period of time prior to the high-temperature curing, and it is known as increasing the strength of a specimen. Therefore, in this experiment, the compressive strength of the geopolymers was measured according to various pre-curing conditions, and microstructure and crystal phase changes were observed by SEM and XRD, respectively. The W/S ratio was determined to be 0.26, which can offer the maximum geopolymer strength with easy molding ability, and the concentration of the alkali solution was 15 M. Pre-curing was performed at room temperature for 0 to 27 days. Compressive strength of the geopolymer made with pre-curing process increased by 36~87 % compared with the specimens made with no pre-curing process. Those improved compressive strength for the pre-cured geopolymer was confirmed owing to promotion effect of pre-curing process on generation of C-S-H gel and zeolite phases, which were analyzed using by XRD and SEM measurement.

• Journal of Urban Science
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• v.12 no.1
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• pp.1-10
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• 2023

The cement industry is a major source of carbon dioxide emissions. Reduction in emissions in this sector is an important issue. Calcium silicate cement is a type of alternative to ordinary Portland cements which contributes to the reduction in carbon dioxide emissions. However, because the type of cement is a non-hydraulic material, there are limitations to its application in the field. The effects of pre-curing periods on the physical characteristics of ordinary Portland cement pastes with calcium silicate cement in the present study were investigated. The Independent variable is the pre-curing period. The pre-curing period varied from 0 to 5 hrs, considering the hydration characteristics of ordinary Portland cement. The carbonation curing of the ordinary Portland cement pastes with the calcium silicate cement after pre-curing was conducted. The concentration of gaseous CO₂ was fixed at 20 %. The test results showed that the pre-curing period led to the pore structural change of the pastes, which in turn could affect the further reaction under the long-term curing condition.

• Transactions of the Society of Information Storage Systems
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• v.3 no.3
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• pp.113-117
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• 2007

재생층이 상변화물질로 이루어진 초해상 광디스크에 있어서, 기록 전과 후에 thermal curing 을 실시하여 신호품질과 재생안정성이 크게 향상되었다. Pre-curing으로 수천 회 이하에서 나타나는 short-term stability가 향상되었고, post-curing 한 후 mid-term stability 가 향상되었다. 그리고, pre- and post-curing 후 noise level 은 전반적으로 $1{\sim}2dB$가 낮아졌고, CNR은 $2{\sim}3dB$, jitter 는 $2{\sim}3%$ 가 향상되었다.

• Applied Microscopy
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• v.43 no.4
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• pp.155-163
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• 2013

Meta-kaolin (MK) and blast furnace slag (BS) were used as raw materials with NaOH and sodium silicate as alkali activators for making geo-polymers. The compressive strength with respect to the various pre-curing conditions was investigated. In order to improve the recycling rate of BS while still obtaining high compressive strength of the geo-polymers, it was necessary to provide additional CaO to the MK by adding BS. The specimens containing greater amounts of BS can be applied to fields that require high initial compressive strength. Alkali activator(s) are inevitably required to make geo-polymers useful. High temperature pre-curing plays an important role in improving compressive strength in geo-polymers at the early stage of curing. On the other hand, long-term curing produced little to no positive effects and may have even worsened the compressive strength of the geo-polymers because of micro-structural defects through volume expansion by high temperature pre-curing. Therefore, a pre-curing process at a medium range temperature of $50^{\circ}C$ is recommended because a continuous increase in compressive strength during the entire curing period as well as good compressive strength at the early stages can be obtained.

• Journal of Urban Science
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• v.11 no.1
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• pp.21-28
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• 2022

Raman spectroscopy is effective to investigate functional groups via molecular vibration. The technique offers the structural information of compounds including subtle changes in the chemical composition of local atomic coordination without critical damage. Thus, the effect of carbonation on the hydration characteristics of Portland cement under pre-curing conditions for carbonation was investigated via Raman spectroscopy in the present study. Gaseous CO₂ was injected within 60 seconds, and the reaction time was varied from 0 minute to 90 minutes. The test results indicated that the Ca/Si ratio of C-S-H reduced immediately after mixing and then the C-S-H with a relatively high Ca/Si ratio coexisted as the reaction time increased. The calcium carbonates formed in the present study included calcite and amorphous calcium carbonates. The test results via Raman spectroscopy provide valuable information about the carbonation characteristics of OPC under pre-curing conditions for carbonation.

• Proceedings of the Korean Institute of Building Construction Conference
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• v.y2004m10
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• pp.11-14
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• 2004

The object of this study is vibrating compaction and curing method in the production process of Design concrete for precast concrete(Design-PC) product. From change of vibrating compaction time and pre-curing time. curing temperature which would be factors of product quality in Design-PC concrete production. and research of optimized steam curing condition from relations between curing condition and strength development. basic data of vibrating compaction time and concrete steam curing method for Design-PC will be presented.

• Proceedings of the Korea Concrete Institute Conference
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• 2000.10b
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• pp.939-944
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• 2000

This study examines both strength development and pore volume of high temperature curing mortar, using a blast-furnace slag powder (BFS). This study experiments with various pre-steaming period, differing curing temperature and the replacement of BFS. According to the results, the strength development of BFS mortar is stronger when higher curing temperature are used(as opposed to standard curing). Also, regardless of the curing method, pore volume decreases as the curing time increases. From these results we can identify the optimum conditions required pre-steaming period, differing curing temperature and the replacement to produce BFS mortar properties.

• Elastomers and Composites
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• v.53 no.2
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• pp.67-74
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• 2018

Magneto-rheological elastomers (MREs) are smart materials in which the inherent stiffness and damping properties can be changed by the influence of an external magnetic field. The magneto-rheological (MR) effect depends on the orientation characteristics of the dispersed magneto-responsible particles (MRPs) in the matrix. In this study, natural rubber (NR) and ethylene propylene diene rubber (EPDM) were blended and used as a matrix of an MRE. EPDM was pre-cured before blending with NR. The Mooney viscosity, curing characteristics, and mechanical properties were analyzed with various pre-curing conditions of EPDM and the NR/EPDM blend. The results show that excellent mechanical properties of the NR/EPDM blend-based MRE were obtained when the pre-curing time of EPDM was 60 min. The aging property of the NR-based MRE was improved by the introduction of pre-cured EPDM. Also, the anisotropic MRE showed a higher MR effect than that of the isotropic MRE.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.27 no.6
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• pp.319-326
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• 2017

In this study, a lightweight geopolymer was prepared using by slag discharged from IGCC (Integrated Gasification Combined Cycle) power plant and its physical properties, the density and compressive strength, were analyzed as a function of the concentration of alkali activators, W/S ratio and aging times. Also the possibility of applying it to lightweight materials by adding Si sludge as a foaming agent to the geopolymerg was investigated. In particular, a complex composition of alkali activator and a pre-curing process were applied to improve the strength properties of lightweight geopolymers. While the compressive strength of the lightweight geopolymer using a single activator was 9.5 MPa, the specimen made with a complex composition of alkali activator had compressive strength of 2~5 times higher. In addition, the lightweight geopolymer with pre-curing process showed a compressive strength value of 18~48 % higher than that of specimen made with no precuring process. In this study, by using a complex activator and a pre-curing process. the maximum compressive strength of lightweight geopolymer was obtained as 40 MPa (The specimen was aged for 3 days and had density of $1.83g/cm^3$), which is comparable to cement concrete. By analyzing the crystal phase and microstructure of geopolymers obtained in this study using by XRD and SEM, respectively, it was confirmed that the flower-bud-like zeolite crystal was homogeneously distributed on the surface of the C-S-H gel (sodium silicate hydrate gel) in the geopolymer.

• Textile Coloration and Finishing
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• v.17 no.6 s.85
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• pp.27-35
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• 2005

Conventional pad- dry-cure(thermo-fixation) process usually produces functional performance on both sides of a fabric. UV curing technique was applied to impart water- and oil-repellent finish effective only on the face of a PET knitted fabric. The preferential one-side coating, by virtue of the limited penetration of UV light, was achieved by W curing after padding of a fluorocarbon agent without special coating or printing equipments. The difference in the functional property of face and back sides was examined by measuring water and oil repellency at each side of the treated fabric. The influence of pre/post-irradiation dose and agent concentration on the performance of the finished fabrics were investigated. While increase in both resin concentration and post-irradiation did not have significant effect on the finish, UV pre-irradiation of PET fabrics caused remarkable influence presumably due to appropriate surface modification of PET fabrics required for facile wetting of the resin. The dimensional stability and color change of the UV cured fabrics measured by FAST and reflectance spectrophotometry showed significantly decreased color difference and increased percent extension compared with the samples pre-irradiated without agent application.