• Title/Summary/Keyword: powder size distribution

Search Result 526, Processing Time 0.026 seconds

The Revolution of Diamond Synthesis Technology

  • Sung, James-C.;Hu, Shao-Chung;Lin, I-Chiao;Tsai, Chia-Cheng
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1136-1137
    • /
    • 2006
  • The ultrahigh pressure process for synthesizing diamond grits is due to make a quantum leap: the raw materials will incorporate diamond seeds with a predetermined pattern. The result is doubling the diamond yield with a narrower size distribution. Moreover, the shape of diamond crystals can be precisely tuned. For example, diamond octahedra or diamond cubes, that are not available today, can be mass-produced. The new technology is now being implemented worldwide so the future diamond grits will have improved quality at reduced prices.

  • PDF

Preparation and Characterization of Stable Dispersions of Ni Nanoparticles

  • Lee, Eun-Hee;Lee, Min-Ku;Rhee, Chang-Kyu
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09a
    • /
    • pp.413-414
    • /
    • 2006
  • The effects of several experimental parameters on the formation of stable Ni nanoparticles dispersion were investigated. The suspensions of Ni nanoparticles were produced in organic solvents using Hypermer KD-2 as a dispersant. The transmission profiles, particle size distribution, zeta potential, and visual inspection results were used to discuss the stability of the dispersion. The optimal conditions for the formation of stable dispersion are evaluated.

  • PDF

Characteristics of Alumina Particles Synthesized by Microwave Heating (마이크로파 가열에 의하여 합성된 알루미나 입자의 특성)

  • Kim, Sung-Wan;Lee, Sung-Hwan;Park, Jae-Hyun;Kim, Jun-Ho;Park, Seong-Soo;Park, Hee-Chan
    • Journal of the Korean Ceramic Society
    • /
    • v.39 no.10
    • /
    • pp.1007-1010
    • /
    • 2002
  • Alpha alumina platelet particles were synthesized from the powder mixture of ${\gamma}-Al_2O_3and\;Na_2SO_4$ with the use of microwave heating. The characteristics of the particles such as particle size and particle size distribution were compared with those of particles obtained from the same mixture without the use of microwave. Sample with the use of microwave showed small particle size and narrow particle size distribution compared to that without the use of microwave.

Hydrothermal Preparation and Sintering of Fine PSZT Powder (미세 PSZT분말의 수열합성 및 소결)

  • Oh, Jung Kang;Seo, Kyung Won
    • Applied Chemistry for Engineering
    • /
    • v.9 no.5
    • /
    • pp.654-660
    • /
    • 1998
  • In preparing PSZT powder by hydrothermal synthesis, effects of reaction temperature, concentration of raw materials and mineralizer on crystallinity, particle size distribution, and dielectric constant were investigated. By varying the concentration of mineralizer and the ratio of Pb to Sr or Zr to Ti, crystalline PSZT powder, having the mean particle size of $0.3{\sim}15{\mu}m$, was prepared by hydrothermal synthesis in the temperature range of $120{\sim}200^{\circ}C$ for a 2h reaction. PSZT ceramics, having dielectric constant of 1000~3000, were prepared at $1150^{\circ}C$ for a 2h sintering reaction of the PSZT powders. Experimental results showed that the weight mean particle size of $0.5{\mu}m$ was obtained when the concentration of KOH in the solution was 10 wt % and the ratio of Pb to Sr was 0.95/0.05, that of Zr to Ti was 0.52/0.48. It also showed that the ceramics of dielectric constant of 2900 were prepared through sintering of this PSZT powder. Size of PSZT particles became smaller with its narrow distribution as the concentration of KOH increased up to 10 wt %. However, it came to be larger at this concentration and above. By adding small amount of Sr that would not affect that crystallinity of particles we can improve dielectric property of sintered materials. Addition of Zr may shift the major crystal phase of synthetic PSZT powder from tetragonal to rhombohedral phase.

  • PDF

Fabrication of the ultrafine ZnO powder through glycothermal process (Glycothermal 공정에 의한 미립 ZnO 분말의 제조)

  • Dong-Sik Bae;Kyong-Sop Han;Yong-Kap Park;Seung-Beom Cho;Sang -Heul Choi
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.7 no.4
    • /
    • pp.567-572
    • /
    • 1997
  • The ZnO powder was prepared under glycothermal conditions by precipitation from metal nitrates with aqueous potassium hydroxide. The fine powder was obtained at temperatures as low as 225 to $275^{\circ}C$, The microstructure and phase of the powder were studied by SEM and XRD. The properties of the ZnO powder were studied as a function of various parameters (reaction temperature, reaction time, solid loading, etc). The average particle size of the ZnO increased with increasing reaction temperature. After glycothermal treatment at $225^{\circ}C$ for 8 h, the average particle size of the ZnO powder was about 150 nm and the particle size distribution was narrow.

  • PDF

Martensitic Transformation Behaviors of Gas Atomized Ti50Ni30Cu20 Powders (Gas atomization으로 제조된 Ti50Ni30Cu20 합금 분말의 상변태 거동)

  • Kim, Yoen-Wook;Chung, Young-Soo;Choi, Eun-Soo;Nam, Tae-Hyun;Im, Yeon-Min
    • Journal of Korea Foundry Society
    • /
    • v.31 no.1
    • /
    • pp.26-30
    • /
    • 2011
  • For the fabrication of bulk near-net-shape Ti-Ni-Cu shape memory alloys, consolidation of Ti-Ni-Cu alloy powders are useful because of their brittle property. In the present study, $Ti_{50}Ni_{30}Cu_{20}$ shape memory alloy powders were prepared by gas atomization and martensitic transformation temperatures and microstructures of those powders were investigated as a function of powder size. The size distribution of the powders was measured by conventional sieving, and sieved powders with the specific size range of 25 to $150\;{\mu}m$ were chosen for this examination. XRD analysis showed that the B2-B19 martensitic transformation occurred in the powders. In DSC curves of the as-atomized $Ti_{50}Ni_{30}Cu_{20}$ powders as a function of powder size, only one clear peak was found on each cooling and heating curve. The martensitic transformation start temperature($M_s$) of the $25-50\;{\mu}m$ powders was $31.5^{\circ}C$. The $M_s$ increased with increasing powder size and the difference of $M_s$ between $25-50\;{\mu}m$ powders and $100-150\;{\mu}m$ powders is only $1^{\circ}C$. The typical microstructure of the rapidly solidified powders showed cellular morphology and very small pores were observed in intercellular regions.

Effect of Process-Control Agents on Characteristics of Amorphous Al-Y-Ni-Co Alloy Powder Produced by Mechanical Alloying

  • Nguyen, H.V.;Kim, J.C.;Kim, J.S.;Kwon, Y.J.;Kwon, Y.S.
    • Journal of Powder Materials
    • /
    • v.17 no.1
    • /
    • pp.7-12
    • /
    • 2010
  • In this work, effect of various process-control agents (PCAs) on the mechanical alloying of amorphous alloy of $Al_{85}Y_8Ni_5Co_2$ has been investigated. The dependence of the particle shape, size and crystallization behavior of the amorphous alloy powders on the type of PCAs and their concentrations was investigated by using X-ray diffraction, field-emission scanning electron microscopy and differential scanning calorimetry. It was found that the additive of toluene could affect positively the amorphization and thermally induced crystallization processes, as well as the size refinement, morphology and particle-size distribution of as-milled powders in comparison with alloy obtained without PCA.

Corrosion Behavior and Microstructural Evolution of Magnesium Powder with Milling Time Prepared by Mechanical Milling (기계적 밀링법으로 제조된 마그네슘 분말의 밀링시간에 따른 미세구조 변화와 부식거동)

  • Ahn, Jin Woo;Hwang, Dae Youn;Kim, Gyeung-ho;Kim, Hye-Sung
    • Korean Journal of Metals and Materials
    • /
    • v.49 no.6
    • /
    • pp.454-461
    • /
    • 2011
  • In this study, the relationship between corrosion resistance and microstructural characteristics such as grain size reduction, preferred orientation, and homogenous distribution of elements and impurity by mechanical milling of magnesium powder was investigated. Mechanical milling of pure magnesium powder exhibited a complex path to grain refinement and growth together with preferred orientation reversal with milling time. It was also found that anisotropic formation of dislocation on the basal plane of magnesium was initially the dominant mechanism for grain size reduction. After 60 hrs of milling, grain coarsening was observed and interpreted as a result of the strain relaxation process through recrystallization. In spite of the finer grain size and strong (002) texture developed in the sample prepared by spark plasma sintering at $500^{\circ}C$ for 5 min after mechanical milling for 2hrs, the sample showed a higher corrosion rate. The results from this study will be helpful for better understanding of the controlling factor for corrosion resistance and behaviors of mechanical milled magnesium powders.

Quality Characteristics of Sulgidduk added with Macadamia Powder (마카다미아 가루를 첨가한 설기떡의 품질 특성)

  • Jo, Eun-Hee;Kim, Myung-Hee
    • Journal of the East Asian Society of Dietary Life
    • /
    • v.23 no.6
    • /
    • pp.742-749
    • /
    • 2013
  • In order to find out the possible effects of steamed rice cake with varying addition of macadamia powder on quality improvement, this study applied 3%, 6%, 9% and 12% addition of macadamia powder. As a result, it found that the more addition of macadamia powder led to significantly higher crude oil content. Further it revealed that whit more addition of macadamia powder, it tended to show a lower L value. Also with more addition of macadamia powder a higher b value was shown. According to SEM, it was found that the 0% group showed an inconsistent grain size and porosity, local distribution of big lumps and rough surfaces, whereas more addition of macadamia powder tended to show a large mass formation and smoother cross-section. The 12% group showed a gradually decreasing hardness. According to the results of sensory characteristics, it was found that the 12% group showed the highest level in flavor, nutty, softness, after taste and overall quality. Conclusively, it is found that the preparation of steamed rice cake using macadamia powder is helpful to keep flavor and softness; moreover, it contributes to the overall quality of rice cake.

Quality Characteristics and Industrial Application of Yanggaeng added with Arrowroot Powder in Korea Cultivars (국내산 칡 분말을 첨가한 양갱의 품질 특성 및 산업적 응용)

  • Ho-Kyoung Kim;Hyo-Won Kim
    • Journal of the Korean Society of Industry Convergence
    • /
    • v.26 no.3
    • /
    • pp.509-515
    • /
    • 2023
  • This study examind the product quality characteristics and industrial application of arrowroot powder added Yanggaeng before its industrial application. Several preliminary experiments were conducted by applying manufacturing conditions and varying the amount of arrowroot powder(1%, 2%, 3%, 4%) added to produce Yanggaeng recipes that can be sold commercially. The moisture content of the produce Yanggaeng was low due to the manufacturing standards, but it showed a significant increase with an increase in the ratio, which was similar to the results of other studies on Yanggaeng. The solubility, particale size distribution, and pH also showed a significant increasing trend. The hardness of arrowroot powder added Yanggaeng decreased with an increase in the amount of arrowroot powder, while springiness, gumminess, and chewiness increased with the addition of arrowroot powder. In terms of color, arrowroot powder showed a dark color, which was well suited to white bean paste and could also be used with black bean paste without any problem. These results were due to the manufacturing ratio being adjusted to meet commercial sales standards, resulting in a lower amount of water being used, and the characteristics of arrowroot powder being applied as they were.