• Design & Manufacturing
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• 제14권1호
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• pp.1-7
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• 2020

In this study, the variation of the shrinkage in the thickness direction of the molded parts according to the gate size of the polymer core fabricated through the 3D printer using the SLS method was studied. The polymer cores are laser sintered and the powder material is nylon base PA2200. The polymer cores have lower heat transfer rate and rigidity than the metal core due to the characteristics of the material. Therefore, the injection molding test conditions are set to minimize the deformation of the core during the injection process. The resin used in the injection molding test is a PP material. The packing condition was set to 80, 90 and 100% of the maximum injection pressure for each gate size. The runner diameter used was ∅3mm, and the gates were fabricated in semicircle shapes with cross sections 1, 2, and 3 ㎟, respectively. Thickness measurement was performed for 10 points at 2.5 mm intervals from the point 2.5 mm away from the gate, and the shrinkage to thickness was measured for each point. The shrinkage rate according to the gate size tends to decrease as the cross-sectional area decreases as the maximum injection pressure increases. The average thickness shrinkage rate was close to 0% when the packing pressure was 90% for the gate area of 1mm2. When the holding pressure was set to 100%, the shrinkage was found to decrease by 3% from the standard dimension due to the over-packing phenomenon. Therefore, the smaller the gate, the more closely the molded dimensions can be molded due to the high pressure generation. It was confirmed that precise packing process control is necessary because over-packing phenomenon may occur.

• 센서학회지
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• 제18권6호
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• pp.467-474
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• 2009

In this study, we describe the feasibility of developing a fiber-optic temperature sensor using a thermochromic material such as 2,4,5-triphenylimidazole or also called Lophine. A sensor-tip is fabricated by mixing of a Lophine powder, which has a non-toxic and hydrophobic characteristics, and an epoxy resin. The temperature change in the sensor-tip gives rise to a change in the optical absorbance of the Lophine, and the transmittance of a light through the Lophine is also changed. We have measured the intensities of modulated lights due to the change of optical absorbance of the Lophine by using of a photo-multiplier tube(PMT). The relationships between the temperatures and the output voltages of PMT are determined to measure the temperature of water. The measurable temperature range of the fiber-optic sensor is from 5 to $30^{\circ}C$.

• Journal of Ginseng Research
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• 제43권1호
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• pp.105-115
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• 2019

Background: Ginsenosides with less sugar moieties may exhibit the better adsorptive capacity and more pharmacological activities. Methods: An efficient method for the separation of four minor saponins, including gypenoside XVII, notoginsenoside Fe, ginsenoside Rd2, and notoginsenoside Fd, from Panax notoginseng leaves (PNL) was established using biotransformation, macroporous resins, and subsequent preparative high-performance liquid chromatography. Results: The dried PNL powder was immersed in the distilled water at $50^{\circ}C$ for 30 min for converting the major saponins, ginsenosides Rb1, Rc, Rb2, and Rb3, to minor saponins, gypenoside XVII, notoginsenoside Fe, ginsenoside Rd2, and notoginsenoside Fd, respectively, by the enzymes present in PNL. The adsorption characteristics of these minor saponins on five types of macroporous resins, D-101, DA-201, DM-301, X-5, and S-8, were evaluated and compared. Among them, D-101 was selected due to the best adsorption and desorption properties. Under the optimized conditions, the fraction containing the four target saponins was separated by D-101 resin. Subsequently, the target minor saponins were individually separated and purified by preparative high-performance liquid chromatography with a reversed-phase column. Conclusion: Our study provides a simple and efficient method for the preparation of these four minor saponins from PNL, which will be potential for industrial applications.

• 보존과학회지
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• 제30권4호
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• pp.383-393
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• 2014

석조문화재 균열부분과 표면 마무리를 위한 보존처리는 현재까지 에폭시수지에 다양한 충전제를 혼합하여 사용하게 된다. 장기적 보존을 위해 이와 같은 보존처리는 필요하다. 하지만 보존처리 된 54건에 대한 현장조사와 임상실험 결과 충전제 중 활석이 포함된 경우 표면변색과 균열 등 재 손상이 확인되었다. 현장조사는 수리보고서와 처리 담당자 인터뷰, 현미경조사, 현장에서 수습한 처리 시편의 ICP 분석을 병행하여 활석 사용여부를 확인하였다. 임상실험은 현장조사에서 확인된 활석에 의한 영향평가를 위해 촉진내후성시험 후 색차와 초음파측정을 실시하였으며 그 결과 활석이 포함된 시편에서의 물성저하가 두드러졌다. 따라서 향후 균열부분 보존처리는 활석의 사용은 자제하고 동질 석분만을 충전제로 선택하여 처리할 것을 제안한다.

• 한국재료학회지
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• 제19권7호
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• pp.403-406
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• 2009

The friction characteristics of automotive brake friction materials that contained different ceramic content were investigated. Several kinds of raw materials, such as resin-based binder, reinforcing fiber, friction restraint, abrasive, and filling materials were mixed, pressed, and heated in order to make the brake friction materials. The contents of SiC and $BaSO_4$ changed from 5 vol% to 20 vol%, respectively. In addition to this, the content of $Al_2O_3$ adjusted from 1 vol% to 16 vol%. The surface morphology of the SiC containing sample appeared rough while more debris was observed when the contents of SiC increased. This implies that the SiC containing brake composite was not adequate for the automobile. However, the relatively smooth surface was observed in samples that contained the $Al_2O_3$. But the roughness was low with a content of 11 vol% $Al_2O_3$ compared to the other samples. This is consistent with the abrasive properties of the samples. In the case of $BaSO_4$ containing samples, the smoothes surface was observed in the contents of 15 vol% $BaSO_4$. Thus, it was concluded that the 11 vol% $Al_2O_3$ and 15 vol% $BaSO_4$ containing composite would be the optimum content for the brake composite. Similar to the results of the surface morphology, the abrasion resistance consistently decreased when the content of SiC increased. On the contrary, the sample that contained 11 vol% $Al_2O_3$ and 15 vol% $BaSO_4$ showed the highest abrasion resistance compared to the other samples.

• The Journal of Advanced Prosthodontics
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• 제10권4호
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• pp.321-327
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• 2018

PURPOSE. The purpose of this study was to compare the cutting method and the lamination method to investigate whether the CAD data of the proposed inlay shape are machined correctly. MATERIALS AND METHODS. The Mesial-Occlusal shape of the inlay was modeled by changing the stereolithography (STL). Each group used SLS (metal powder) or SLA (photocurable resin) in the additive method, and wax or zirconia in the subtractive method (n=10 per group, total n=40). Three-dimensional (3D) analysis program (Geomagic Control X inspection software; 3D systems) was used for the alignment and analysis. The root mean square (RMS) in the 2D plane state was measured within $50{\mu}m$ radius of eight comparison measuring points (CMP). Differences were analyzed using one-way analysis of variance and post-hoc Tukey's test were used (${\alpha}=.05$). RESULTS. There was a significant difference in RMS only in SLA and SLS of 2D section (P<.05). In CMP mean, CMP 4 ($-5.3{\pm}46.7{\mu}m$) had a value closest to 0, while CMP 6 ($20.1{\pm}42.4{\mu}m$) and CMP 1 ($-89.2{\pm}61.4{\mu}m$) had the greatest positive value and the greatest negative value, respectively. CONCLUSION. Since the errors obtained from the study do not exceed the clinically acceptable values, the lamination method and the cutting method can be used clinically.

• 마이크로전자및패키징학회지
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• 제23권4호
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• pp.125-133
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• 2016

도전 페이스트의 필러로 사용되기 위한 미세 Cu 입자를 제조하기 위하여 아산화동 분말과 황산간의 고속 화학 반응을 이용한 증류수 기반의 습식 공정으로 Cu 입자의 합성을 실시하였다. $7^{\circ}C$에서 48%의 황산과 30 g의 $Cu_2O$를 사용한 조건에서 미반응 $Cu_2O$ 입자들이 제거되면서 입자들간의 응집이 개선된 순수 Cu 나노입자들이 제조되었다. 이후 최적 첨가제의 선택을 통하여 입자들간의 응집이 가장 억제된 224 nm 크기의 Cu 입자들을 제조할 수 있었다. 이러한 미세 Cu 입자 시료에서는 응집된 형태의 조대 입자들이 다소 존재하였고 입자들간의 연결부도 일부 관찰되었으나, 삼본밀을 사용한 레진 포물레이션과의 혼합 후에는 응집된 형태의 조대 입자들이 파괴되고 입자들간의 연결부들이 탈착되어 입자들의 응집이 풀리는 거동을 관찰할 수 있었다.

• Elastomers and Composites
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• 제47권2호
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• pp.121-128
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• 2012

제대로 재활용되지 못하고 있는 폐 EPDM 즉, 자동차 Weather strip이나 세탁기 가스켓 등에서 재생한 폐EPDM 분말을 적합하고 경제성있는 Polyolefin계 Elastomer와 수지(Binder), 그리고 Filler 및 기타 첨가제를 선정하여, 다양한 배합조건으로 고무 복합소재를 압출 제조하였다. 본 실험에 유익한 기초 실험으로서, 폐 EPDM의 초음파처리 효과, 폐 EPDM복합소재의 폐타이어 복합소재와의 물성 비교, Virgin EPDM과 Devulcanized EPDM과의 비교, 그리고 12 축압출기로 압출한 재료의 물성에의 영향을 고찰하였다. 폐 EPDM을 이용하여 인조잔디 충전재와 카매트용 복합소재를 2 축압출기를 사용하여 압출한 후, 인장시편을 사출하여 인장강도, 신율, 경도의 세가지 물성을 주요 평가지표로 삼고 경제적인 배합처방을 개발하였다.

• 한국세라믹학회지
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• 제50권6호
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• pp.402-409
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• 2013

The objective of this study was to develop a synthesis process for ${\beta}$-SiC powders to reduce the synthesis temperature and to control the particle size and to prevent particle agglomeration of the synthesized ${\beta}$-SiC powders. A phenol resin and TEOS were used as the starting materials for the carbon and Si sources, respectively. $SiO_2$-C hybrid precursors with various C/Si mole ratios were fabricated using a conventional sol-gel process. ${\beta}$-SiC powders were synthesized by a carbothermal reduction process using $SiO_2$-C hybrid precursors with various C/Si mole ratios (1.6 ~ 2.5) fabricated using a sol-gel process. In this study, the effects of excess carbon and the addition of Si powders to the $SiO_2$-C hybrid precursor on the synthesis temperature and particle size of ${\beta}$-SiC were examined. It was found that the addition of metallic Si powders to the $SiO_2$/C hybrid precursor with excess carbon reduced the synthesis temperature of the ${\beta}$-SiC powders to as low as $1300^{\circ}C$. The synthesis temperature for ${\beta}$-SiC appeared to be reduced with an increase of the C/Si mole ratio in the $SiO_2$-C hybrid precursor by a direct carburization reaction between Si and excess carbon.

• 한국항행학회논문지
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• 제13권6호
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• pp.838-845
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• 2009

유전체 기판을 대신하여 안테나 기판으로 사용되어질 다양한 유전율과 투자율을 가지는 자성유전체를 얻기 위하여 유전체 재료로는 실리콘 레진과 에폭시 레진을 그리고 자성재료로는 카보닐 아이언, 바륨 및 스트론튬을 사용하여 다양한 합성물로 제조하였고, 이러한 자성유전체들의 비유전율 및 비투자율을 HP4291B 임피던스 분석기를 사용하여 측정하였다. 본 논문에서 필름형태로 제조된 자성유전체를 안테나 기판으로 사용했을 때 공진주파수, 임피던스 대역폭과 같은 안테나 특성 변화의 차이점을 유전체 기판 사용과 비교하여 알아보기 위해 측정된 비유전율 및 비투자율에 근거하여 IFA형태의 미앤더 모노폴 안테나 설계 및 제작을 하였고, 모의실험 결과 및 측정 결과를 제시하였다. 본 논문에서는 이러한 결과를 토대로 자성재료의 종류 선택 및 자성재료와 유전체 재료의 혼합비 변화에 따른 자성유전체의 특성 변화들을 논의한다.