• Title/Summary/Keyword: powder mixture

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Fundamental Study on the Strength and Heat Transferring Charcteristic of Cement Composite with Waste CNT (폐CNT를 혼입한 시멘트 복합체의 강도 및 열전달 특성에 대한 기초적 연구)

  • Koo, Hounchul;Kim, Woon-Hak;Oh, Hongseob
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.1
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    • pp.66-73
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    • 2022
  • The purpose of this study was to develop self-heating concrete by utilizing the conduction resistance of concrete in order to reduce the risk of occurrence of black ice in the concrete pavement in winter and to prevent damage caused by freez-thawing effect. For this purpose, it was attempted to evaluate the strength and temperature exothermic characteristics using powder and liquid waste CNTs and a waste cathode agent as a conduction promotion. It was analyzed that liquid waste CNT had an effective dispersion degree in the mortar and a small decrease in strength occurred. In addition, DC 24 V was supplied by applying steel mesh, copper foil and copper wire to the mortar as electrodes, and the temperature change characteristics according to the mixing ratio of spent CNTs, anodes and carbon fibers were evaluated. In addition, by evaluating the temperature characteristics according to the electrode spacing from the selected optimal mixture, it was confirmed that it had sufficient heating characteristics up to an electrode spacing of 100 mm up to AC 50 V.

Flvonoids and Their Glycosides from the Bark of Salix rorida (분버들(Salix rorida) 수피의 후라보노이드 및 배당체 화합물)

  • Ham, Yeon-Ho;Bae, Young-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.1
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    • pp.56-62
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    • 2002
  • The air-dried bark of Salix rorida was extracted with acetone-water(7:3, v/v) and its extractives were concentrated with a vacuum evaporator. The extractives were fractionated with a series of n-hexane, chloroform, ethylacetate(EtOAc) and water on a separatory funnel. Each fraction was freeze-dried to give some dark brown powder. The EtOAc and water soluble fractions were chromatographed on a Sephadex LH-20 column using a series of aqueous methanol and ethanol-hexane mixture as eluents. The isolated compounds were tested with a cellulose TLC developed with TBA and 6% acetic acid and then visualized on UV lamp or sprayed with vanillin-HCl-EtOH. The purified compounds were flavonoids and their glycosides as follows:(+)-catechin, naringenin, salipurposide, aromadendrin, isosalipurposide, aromadendrin-7-O-𝛽-D-glucopy- ranoside and taxifolin-7-O-𝛽-D-glucopyranoside. The structures of each compounds were confirmed by 1H-NMR, 13C-NMR and mass spectra.

Engineering characteristics of dune sand-fine marble waste mixtures

  • Qureshi, Mohsin U.;Mahmood, Zafar;Farooq, Qazi U.;Qureshi, Qadir B.I.L.;Al-Handasi, Hajar;Chang, Ilhan
    • Geomechanics and Engineering
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    • v.28 no.6
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    • pp.547-557
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    • 2022
  • Dune sands are poorly graded collapsible soils lacking fines. This experimental study explored the technical feasibility of sustainable invigoration of fine waste materials to improve the geotechnical properties of dune sand. The fine waste considered in this study is fine marble waste. The fine waste powder was mixed with dune sand at different contents (5, 10,15, 20, 25, 50%), where the gradation, void ratio, compaction, and shear strength characteristics were assessed for each fine marble waste -dune sand blend. The geotechnical properties of the dune sand-fine marble waste mix delineated in this study reveal the enhancement in compaction and gradation characteristics of dune sand. According to the results, the binary mixture of dune sand with 20% of fine marble waste gives the highest maximum dry density and results in shear strength improvement. In addition, a numerical study is conducted for the practical application of the binary mix in the field and tested for an isolated shallow foundation. The elemental analysis of the fine marble waste confirms that the material is non-contaminated and can be employed for engineering applications. Furthermore, the numerical study elucidated that the shallow surface replacement of the site with the dune sand mixed with 20% fine marble waste gives optimal performance in terms of stress generation and settlement behavior of an isolated footing. For a sustainable mechanical performance of the fine marble waste mixed sand, an optimum dose of 20% fine marble waste is recommended, and some correlations are proposed. Thus, for improving dune sand's geotechnical characteristics, the addition of fine marble waste to the dune sand is an environment-friendly solution.

Effects of nano-silica and micro-steel fiber on the engineering properties of ultra-high performance concrete

  • Hakeem, Ibrahim Y.;Amin, Mohamed;Abdelsalam, Bassam Abdelsalam;Tayeh, Bassam A.;Althoey, Fadi;Agwa, Ibrahim Saad
    • Structural Engineering and Mechanics
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    • v.82 no.3
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    • pp.295-312
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    • 2022
  • This study investigates the effects of nano silica (NS) and micro steel fiber on the properties of ultra-high-performance concrete (UHPC). The experimental consists of three groups, each one with five percentages of NS content (0%, 2%, 4%, 6% and 8%) in addition to the 20% silica fume and 20% quartz powder proportioned according to the weight of cement added to the mixtures. In addition, three percentages of micro steel fibers (0%, 1% and 2%) were considered. Different mixtures with varying percentages of NS and micro steel fibers were prepared to set the water-to-binder ratio, such as 0.16% and 1.8% superplasticizer proportioned according the weight of the binder materials. The fresh properties, mechanical properties and elevated temperatures of the mixtures were calculated. Then, the results from the microstructure analyses were compared with that of the reference mixtureand it was found that 6% replacement of cement with NS was optimum replacement level. When the NS content was increased from 0% to 6%, the air content and permeability of the mixture decreased by 35% and 39%, the compressive and tensile strength improved by 21% and 18% and the flexural strength and modulus of elasticity increased by 20% and 11.5%, respectively. However, the effect of micro steel fibres on the compressive strength was inconclusive. The overall results indicate that micro steel fibres have the potential to improve the tensile strength, flexure strength and modulus of elasticity of the UHPC. The use of 6% NS together with 1% micro-steel fiber increased the concrete strength and reduce the cost of concrete mix.

Study on preparation of a thin film type of ZnS(Ag) scintillator sheet for alpha-ray detection (얇은 필름 형태의 알파선 측정용 ZnS(Ag) 섬광 검출소재 제조 연구)

  • Seo, Bum-Kyoung;Jung, Yeon-Hee;Kim, Gye-Hong;Lee, Kune-Woo;Jung, Chong-Hun;Han, Myeong-Jin
    • Analytical Science and Technology
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    • v.19 no.5
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    • pp.389-393
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    • 2006
  • The detector consisted of ZnS(Ag) scintillator and photomultiplier tube (PMT) is widely used as contamination monitor in the nuclear facilities. Such detectors are mainly manufactured by adhering the ZnS(Ag) powder onto the transparent plastic. In this study the preparation condition for ZnS(Ag) scintillator sheet using a simple method was established. The scintillator sheet was composed with a support polymer sheet and ZnS(Ag) scintillator layer. The base sheet was prepared by casting the polymer solution after solving the polymer with solvent and the scintillator layer was manufactured by printing the mixture solution with ZnS(Ag) and paste. It was found that the polysulfone(PSf) as a polymer for the base sheet and a cyano resin as a paste for adhering the ZnS(Ag) scintillator was suitable. Also, the prepared thin scintillator sheet had a sufficient mechanical strength, a optical transparency and an alpha-ray detection performance.

Synthesis of Carbon Nano Silicon Composites for Secondary Battery Anode Materials Using RF Thermal Plasma (RF 열플라즈마를 이용한 이차전지 음극재용 탄소나노실리콘복합소재 합성)

  • Soon-Jik Lee;Dae-Shin Kim;Jeong-Mi Yeon;Won-Gyu Park;Myeong-Seon Shin;Seon-Yong Choi;Sung-Hoo Ju
    • Korean Journal of Materials Research
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    • v.33 no.6
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    • pp.257-264
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    • 2023
  • To develop a high capacity lithium secondary battery, a new approach to anode material synthesis is required, capable of producing an anode that exceeds the energy density limit of a carbon-based anode. This research synthesized carbon nano silicon composites as an anode material for a secondary battery using the RF thermal plasma method, which is an ecofriendly dry synthesis method. Prior to material synthesis, a silicon raw material was mixed at 10, 20, 30, 40, and 50 wt% based on the carbon raw material in a powder form, and the temperature change inside the reaction field depending on the applied plasma power was calculated. Information about the materials in the synthesized carbon nano silicon composites were confirmed through XRD analysis, showing carbon (86.7~52.6 %), silicon (7.2~36.2 %), and silicon carbide (6.1~11.2 %). Through FE-SEM analysis, it was confirmed that the silicon bonded to carbon was distributed at sizes of 100 nm or less. The bonding shape of the silicon nano particles bonded to carbon was observed through TEM analysis. The initial electrochemical charging/discharging test for the 40 wt% silicon mixture showed excellent electrical characteristics of 1,517 mAh/g (91.9 %) and an irreversible capacity of 133 mAh/g (8.1 %).

Shrinkage Properties of High Performance Concrete Used Expansive Additive and Shrinkage Reducing Agent (팽창재와 수축저감제를 사용한 고성능 콘크리트의 수축 특성)

  • Koh, Kyung Taek;Park, Jung Jun;Ryu, Gum Sung;Kang, Su Tae
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.4A
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    • pp.787-794
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    • 2006
  • Generally, high performance concrete has characteristics such as low water-cementitious material ratio, lots of unit binder powder, thus the heat of hydration, autogenous shrinkage are tend to be increased. This study is to investigated the effect of the expansive additive and shrinkage reducing agent on the shrinkage properties of high performance concrete as a study to develop the reduction technology of the concrete shrinkage. Test results showed that the expansive additive and shrinkage reducing agent were effective the reduction of shrinkage of high performance concrete. Especially, the using method in combination with expansive additive and shrinkage reducing agent was more effective than the separately using method of that. Also, it analyzed that the combination of expansive additive of 5% and shrinkage reducing agent of 1% was the most suitable mixture, considering to the fluidity, strength and shrinkage properties.

Mock-up Crack Reduction Performance Evaluation of Blast Furnace Slag Concrete Mixed with Expansive and Swelling Admixture (팽창재와 팽윤제가 혼입된 고로슬래그 콘크리트 Mock-up의 균열 저감 성능평가)

  • Sang-Hyuck Yoon;Won-Young Choi;Chan-Soo Jeon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.11 no.4
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    • pp.552-559
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    • 2023
  • The purpose of this study is to evaluate the crack reduction performance of blast furnace slag concrete mixed with expansive and swelling admixtures. As a basic performance test, various ingredients such as blast furnace slag fine powder (BFS), calcium sulfoaluminate (CSA), bentonite, and hydroxypropyl methyl cellulose (HPMC) were used, and the results showed that bentonite showed superior performance compared to HPMC. Afterwards, a MOCK-UP test was conducted to evaluate cracking and drying shrinkage according to the mixing ratio. As a result, when bentonite and a small amount of calcium phosphate were added, drying shrinkage was reduced and cracking was reduced. In particular, a cement mixture consisting of 30 % BFS, 1 % bentonite, and 1 % calcium phosphate showed optimal crack-free performance. It is believed that BFS concrete will contribute to compensating for shrinkage through continuous expansion activity and can be used for field applications.

Prevention of Photoaging and Wrinkle Formation in Hairless Mice Dorsal Skin by APB-03 (Hairless mice에서의 대두 홍삼 혼합 분말(APB-03)의 경구 반복 투여 시 피부 주름 생성 예방 효과)

  • Lee, Ji-Hae;Lee, Byoung-Seok;Yang, Mi-Suk;Byun, Bum-Sun;Kim, Wan-Gi;Kim, Bae-Hwan;Lee, Sang-Jun
    • Korean Journal of Food Science and Technology
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    • v.37 no.6
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    • pp.989-996
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    • 2005
  • Ultraviolet (UV) induces photo aging, erythema, sunburn, photo-toxicity, photo-allergy, and skin tumor, To investigate photo-protective effects of AmorePacific Beauty-03 (APB-03; mixture of red ginseng extract powder and soybean extract powder) on UV-induced damaged skins, 40 SKH hairless female mice were orally administered APB-03 or saline five times a week and irradiated with UV three times per week far up to 12 weeks. Visible skin changes and skin damage in dermis and epidermis by replica image analysis and histological analysis. In APB-03-treated group, better skin, negative replica appearance and less wrinkle formation were observed compared to the UV control group. These results demonstrate oral administration of APB-03 have photo-protective effects on UV-damaged hairless mouse skin.

Mechanical properties of $Al_2O_3/Mo/MnO_2$ composite ($Al_2O_3/Mo/MnO_2$ 복합재료의 기계적 특성)

  • Park, Hyun;Kim, Kyung-Nam
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.16 no.4
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    • pp.172-179
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    • 2006
  • When $Al_2O_3-MoO_3$ mixture is reduced, $MoO_3$ is only reduced to Mo at $900^{\circ}C$. But a compound between $Al_2O_3$ and Mo is not formed up to $1300^{\circ}C$. In the case of $Al_2O_3-MoO_3-MnO_2$ mixture, an intermediate compound $Mn_2Mo_3O_8$ is firstly formed at $900^{\circ}C$ and changes to $MnAl_2O_4$ at $1100^{\circ}C{\sim}1300^{\circ}C$. $Al_2O_3/Mo/MnO_2$ composite are manufactured by a selective reduction process in which Mo is only reduced in the powder mixture of $Al_2O_3,\;MoO_3\;and\;MnO_2$ oxide. For $Al_2O_3/Mo$ composite, the average grain size was not changed with increasing Mo content because of inhibition of grain growth of $Al_2O_3$ matrix in the presence of Mo particles. Fracture strength increased with increasing Mo content due to phenomenon of grain growth inhibition of $Al_2O_3$ matrix. Hardness decreased because of a lower hardness value of Mo, whereas fracture toughness increased. For $Al_2O_3,\;Mo\;and\;MnO_2$ composite, grain growth was facilitated by MnOB and it showed a lower fracture strength because of grain growth effect with increasing Mo and $MnO_2$ content. Hardness decreased because of the grain growth of matrix and coalesced Mo particles to be located in grain boundary, whereas fracture toughness increased.