• Title/Summary/Keyword: pore evolution

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Microstructural Evolution and Dielectric Response Characteristics During Crystallization of Amorphous Pb(Fe2/3W1/3)O3

  • Kim, Nam-Kyung;David A. Payne
    • The Korean Journal of Ceramics
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    • v.1 no.2
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    • pp.75-80
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    • 1995
  • Development of phases, evolution of microstructures, and dielectric response characteristics of amorphous lead iron tungstates during crystabllization were investiageted. A series of mircographs showing the evolution sequence of microstructures is presented. Crystallization was observed to initiate from inside of the amorphous material. A cubic perovskite phase developed fully at $760^{\circ}C$ from amorphous state via intermediate metastable crystalline structures. Dielectric constant of amorphous PFM was totally insensitive to the temperature change around the Curie temperature of crystalline material. Sintered pellet, with relative density of 96% and an almost pore-free dense internal microstructure, could be prepared from amorphous powder.

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Print Gloss Development of Offset Ink on Controlled Coating Structure (조절된 코팅구조상에서 옵셋인쇄광택의 발현 : Part 1)

  • Jeon, Sung-J.;Lee, Jae-S.;Shon, Chang-M.
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2003.04a
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    • pp.54-69
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    • 2003
  • Print gloss is an important attribute of the final printed product. While past work has looked at the influence of key aspects of the coating structure on print gloss, a systematic study has not been reported. The coating roughness, porosity, and pore size are changed by using various combinations of coating materials and by calendering against rough plastic sheets. The print gloss is measured every tenths of a second right after printing, a few minutes after printing, and a few days afterwards. Roughness and porosity affect the print gloss for the first two seconds: this result shows that they influence the ink-film splitting event. Once ink film starts to level, roughness and pore size influences the level of print gloss within the first ten seconds after printing. Porosity modifies the evolution of print gloss for the next few minutes. The decrease in gloss at long times is found to correlate to surface roughness.

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Pore structure evolution characteristics of sandstone uranium ore during acid leaching

  • Zeng, Sheng;Shen, Yuan;Sun, Bing;Zhang, Ni;Zhang, Shuwen;Feng, Song
    • Nuclear Engineering and Technology
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    • v.53 no.12
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    • pp.4033-4041
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    • 2021
  • To better understand the permeability of uranium sandstone, improve the leaching rate of uranium, and explore the change law of pore structure characteristics and blocking mechanism during leaching, we systematically analyzed the microstructure of acid-leaching uranium sandstone. We investigated the variable rules of pore structure characteristics based on nuclear magnetic resonance (NMR). The results showed the following: (1) The uranium concentration change followed the exponential law during uranium deposits acid leaching. After 24 h, the uranium leaching rate reached 50%. The uranium leaching slowed gradually over the next 4 days. (2) Combined with the regularity of porosity variation, Stages I and II included chemical plugging controlled by surface reaction. Stage I was the major completion phase of uranium displacement with saturation precipitation of calcium sulfate. Stage II mainly precipitated iron (III) oxide-hydroxide and aluminum hydroxide. Stage III involved physical clogging controlled by diffusion. (3) In the three stages of leaching, the permeability of the leaching solution changed with the pore structure, which first decreased, then increased, and then decreased.

Prediction of Soil-Water Characteristic Curve and Relative Permeability of Jumunjin Sand Using Pore Network Model (공극 네트워크 모델을 이용한 주문진표준사의 함수특성곡선 및 상대투수율 예측에 관한 연구)

  • Suh, Hyoung Suk;Yun, Tae Sup;Kim, Kwang Yeom
    • Journal of the Korean Geotechnical Society
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    • v.32 no.1
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    • pp.55-62
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    • 2016
  • This study presents the numerical results of soil-water characteristic curve for sandy soil by pore network model. The Jumunjin sand is subjected to the high resolution 3D X-ray computed tomographic imaging and its pore structure is constructed by the web of pore body and pore channel. The channel radius, essential to the computation of capillary pressure, is obtained based on the skeletonization and Euclidean Distance transform. The experimentally obtained soil-water characteristic curve corroborates the numerically estimated one. The pore channel radius defined by minimum radii of pore throat results in the slightly overestimation of air entry value, while the overall evolution of capillary pressure resides in the acceptable range. The relative permeability computed by a series of suggested models runs above that obtained by pore network model at high degree of saturation.

The Earthworm Fauna from Ulleungdo Island, Korea with One New Species of the Genus Amynthas (Oligochaeta: Megascolecidae) (울릉도 지렁이상 및 왕지렁이속의 1신종)

  • Hong, Yong;Kim, Tae-Heung
    • Animal Systematics, Evolution and Diversity
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    • v.21 no.2
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    • pp.129-136
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    • 2005
  • During the expedition of Uileunsdo Islands, Korea in September 2-4, 2004, a total of seven species were recognized. Of these, one species Amynthas dageletensis sp. nov. is described as new to science. Amynthas degeletensis sp. nov. lacks spermathecal pore, spermathecae, prostates, and male pore. These characteristics are systematically important and unique to the species among Korean members of Amynthas. Description of the new species is provided, including illustrations of ventral view and male pore region.

Prediction of terminal density through a two-surface plasticity model

  • Won, Jongmuk;Kim, Jongchan;Park, Junghee
    • Geomechanics and Engineering
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    • v.23 no.5
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    • pp.493-502
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    • 2020
  • The prediction of soil response under repetitive mechanical loadings remains challenging in geotechnical engineering applications. Modeling the cyclic soil response requires a robust model validation with an experimental dataset. This study proposes a unique method adopting linearity of model constant with the number of cycles. The model allows the prediction of the terminal density of sediments when subjected to repetitive changes in pore-fluid pressure based on the two-surface plasticity. Model simulations are analyzed in combination with an experimental dataset of sandy sediments when subjected to repetitive changes in pore fluid pressure under constant deviatoric stress conditions. The results show that the modified plastic moduli in the two-surface plasticity model appear to be critical for determining the terminal density. The methodology introduced in this study is expected to contribute to the prediction of the terminal density and the evolution of shear strain at given repetitive loading conditions.

One-Pot Electrochemical Synthesis of Hierarchical Porous Niobium

  • Joe, Gihwan;Shin, Heon-Cheol
    • Journal of Electrochemical Science and Technology
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    • v.12 no.2
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    • pp.257-265
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    • 2021
  • In this study, we report niobium (Nb) with hierarchical porous structure produced by a one-pot, HF-free electrochemical etching process. It is proved experimentally that a well-defined hierarchical porous structure is produced from the combination of a limited repetition of pulse etching and high concentration of aggressive anion (i.e., SO42-), which results in hierarchical pores with high order over 3. A formula is derived for the surface area of porous Nb as a function of the hierarchical order of pores while the experimental surface area is estimated on the basis of the electrochemical gas evolution rate on porous Nb. From the comparison of the theoretical and experimental surface areas, an in-depth understanding was gained about porous structure produced in this work in terms of the actual pore shape and hierarchical pore order.

Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)

  • Gargi Roy;Raj Narayan Hajra;Woo Hyeok Kim;Jongwon Lee;Sangwoo Kim;Jeoung Han Kim
    • Journal of Powder Materials
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    • v.31 no.1
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    • pp.1-7
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    • 2024
  • This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 ㎛, contrasting with the 1-1.5 ㎛ size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.