• Title/Summary/Keyword: plasma spray

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Fabrication, Microstructure and Adhesive Properties of BCuP-5 Filler Metal/Ag Plate Composite by using Plasma Spray Process (Plasma spray 공정을 이용한 BCuP-5 filler 금속/Ag 기판 복합 소재의 제조, 미세조직 및 접합 특성)

  • Youn, Seong-June;Kim, Young-Kyun;Park, Jae-Sung;Park, Joo-Hyun;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.27 no.4
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    • pp.333-338
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    • 2020
  • In this study, we fabricate a thin- and dense-BCuP-5 coating layer, one of the switching device multilayers, through a plasma spray process. In addition, the microstructure and macroscopic properties of the coating layer, such as hardness and bond strength, are investigated. Both the initial powder feedstock and plasma-sprayed BCuP-5 coating layer show the main Cu phase, Cu-Ag-Cu3P ternary phases, and Ag phase. This means that microstructural degradation does not occur during plasma spraying. The Vickers hardness of the coating layer was measured as 117.0 HV, indicating that the fine distribution of the three phases enables the excellent mechanical properties of the plasma-sprayed BCuP-5 coating layer. The pull-off strength of the plasma-sprayed BCuP-5 coating layer is measured as 16.5 kg/㎠. Based on the above findings, the applicability of plasma spray for the fabrication process of low-cost multi-layered electronic contact materials is discussed and suggested.

Microstructure and Tribological Characteristics of AlSi-Al$_2$O$_3$ Composite Coating Prepared by Plasma Spray (플라즈마 용사에 의한 AlSi-Al$_2$O$_3$ 복합재료 코팅층의 미세조직 및 마찰.마모특성)

  • Min Joon-Won;Yoo Seung-Eul;Kim Young-Jung;Suhr Dong-Soo
    • Journal of Welding and Joining
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    • v.22 no.5
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    • pp.46-52
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    • 2004
  • AlSi-Al$_2$O$_3$ composite layer was prepared by plasma spray on steel substrate. The composite powder for plasma spray was prepared by simple mechanical blending. The wear resistance of the composite layers and matrix aluminum alloy were performed in terms of size distribution of ceramic particles. Friction coefficients of AlSi were decreased with incorporation of $Al_2$O$_3$. The tribological properties of coated layers were affected by the size of incorporated $Al_2$O$_3$ particle. The reinforcement of $Al_2$O$_3$ particle into aluminum alloy matrix decreased the friction coefficient as well as wear loss.

Effect of Sealing Process on the Tribological Behavior of the Plasma Spray Zirconia Based Coatings (지르코니아 충전이 지르코니아계 용사코팅층의 마모마찰에 미치는 영향)

  • 신종한;임대순;안효석
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.10a
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    • pp.265-271
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    • 1998
  • High temperature wear behavior of plasma sprayed zirconia based coating sealing with zirconia sol were investigated for high temperature wear resistance application. The zirconia powders containing 2.5, 5.0, 7.5, 10.0 mol% of MoS$_2$, $Fe_2O_3$ for plasma spray were made by spray drying method. As-sprayed coating was sealed by zirconia-sol to fill up the pore and crack in coating. wear test were performed at temperature ranges from room temperature to 600$\circ$C. The microstructural changes of before and after sealing process were examined by SEM, XRD and EPMA. After sealing process, the porosity was decreased and micro-hardness was increased. The wear properties of coating after sealing process were improved by sealing of pores and cracks. The behavior of wear amount and coefficient of friction were same tendency to before sealing process.

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Optimization of Plasma Spray Coating Parameters of Alumina Ceramic by Taguchi Experimental Method (실험계획법에 의한 알루미나 세라믹의 플라즈마 용사코팅 최적화)

  • 이형근;김대훈;윤충섭
    • Journal of Welding and Joining
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    • v.18 no.6
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    • pp.96-101
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    • 2000
  • Sintered alumina ceramic substrate has been used for the insulating substrate for thick Hybrid IC owing to its cheapness and good insulating properties. Some of thick HIC's are important to eliminate the heat emitted from the parts that are mounted on the ceramic substrate. Sintered ceramic substrate can not transfer and emit the heat efficiently. It's been tried to do plasma spray coating of alumina ceramic on the metal substrates that have a good heat emission property. The most important properties to commercialize this ceramic coated metal substrate are surface roughness and deposition efficiency. In this study, plasma spray coating parameters are optimized to minimize the surface roughness and to maximize the deposition efficiency using Taguchi experimental method. By this optimization, the deposition efficiency was greatly improved from 35% at the frist time to 75% finally.

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A Study on Manufacture of Spraying Powder for BSCCO Superconductor Formation by Plasma Spray (플라즈마 용사에 의한 BSCCO 초전도체 형성을 위한 용사 분말의 제조에 관한 연구)

  • Park, Jeong-Sik;Cho, Chang-Eun;Park, Kyung-Chae
    • Journal of Powder Materials
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    • v.15 no.6
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    • pp.477-481
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    • 2008
  • Formation and characteristics of spraying powder for BSCCO High-Tc superconductor prepared by plasma spray coating were investigated. The addition of 3% of binder gives the best flowability of the powder. Ball milling for 30h and 35h gives the best flowability of powder in the case of 2001 and 0212, respectively. The withdraw ratio increases upon binder addition from 12 to 27% in the case of 2001 and from 18 to 31% in the case of 0212 for sieving powder of $30-90{\mu}m$ in size. The built-up efficiency for $100{\mu}m$ thickness of spray coating is increased more than 30% by binder addition. The microstructure of the spray coated layers was investigated by XRD and EDS analysis.

Effect of Spray Angle the on Microstructure and Mechanical Properties of Y2O3 Coating Layer Manufactured by Atmospheric Plasma Spray Process (Atmospheric plasma spray 공정으로 제조된 Y2O3 코팅층의 미세조직 및 기계적 특성에 미치는 분사 각도의 영향)

  • Hwang, Yu-Jin;Kim, Kyoung-Wook;Lee, Ho-Young;Kwon, Sik-Chol;Lee, Kee Ahn
    • Journal of Powder Materials
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    • v.28 no.4
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    • pp.310-316
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    • 2021
  • The effects of different spray angles (90°, 85°, 80°) on the microstructure and mechanical properties of a Y2O3 coating layer prepared using the atmospheric plasma spray (APS) process were studied. The powders employed in this study had a spherical shape and included a cubic Y2O3 phase. The APS coating layer exhibited the same phase as the powders. Thickness values of the coating layers were 90°: 203.7 ± 8.5 ㎛, 85°: 196.4 ± 9.6 ㎛, and 80°: 208.8 ± 10.2 ㎛, and it was confirmed that the effect of the spray angle on the thickness was insignificant. The porosities were measured as 90°: 3.9 ± 0.85%, 85°: 11.4 ± 2.3%, and 80°: 12.7 ± 0.5%, and the surface roughness values were 90°: 5.9 ± 0.3 ㎛, 85°: 8.5 ± 1.1 ㎛, and 80°: 8.5 ± 0.4 ㎛. As the spray angle decreased, the porosity increased, but the surface roughness did not show a significant difference. Vickers hardness measurements revealed values of 90°: 369.2 ± 22.3, 85°: 315.8 ± 31.4, and 80°: 267.1 ± 45.1 HV. It was found that under the condition of a 90° angle with the lowest porosity exhibited the best hardness value. Based on the aforementioned results, an improved method for the APS Y2O3 coating layer was also discussed.

Value of spray-dried plasma as a supplement to swine diets

  • Jang, Kibeom;Kim, Junsu;Kim, Sheena;Jang, Yoontack;Lee, Jeongjae;Kim, Younghwa;Park, Juncheol;Kim, Younghoon;Song, Minho
    • Korean Journal of Agricultural Science
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    • v.43 no.1
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    • pp.14-20
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    • 2016
  • One of the most powerful health management practices is the use of antibiotics, but their use is being restricted because of health safety issues. The swine industry has been looking for various alternatives to antibiotics and increasingly considers the use of dietary factors like feed ingredients, feed additives, feed formulation practices, or feeding methods, instead of using antibiotics to improve pig health and performance. Among other alternatives to antibiotics, spray-dried plasma may be a candidate. Spray-dried plasma is a blood product that provides bioavailable nutrients and physiologically active components such as immunoglobulins, glycoproteins, growth factors, peptides, etc. It is an excellent protein source with balanced and highly digestible amino acids. Several beneficial physiological activities depend on components of spray-dried plasma, such as immune competence (antibacterial activity), modulation of microbiota and/or immune system, integrity of intestinal barrier function, etc. These beneficial effects can contribute to improvement of pig performance and health by modulation of microbiota in the digestive tract and/or immune system. Therefore, it is suggested that spray-dried plasma has great potential as an antibiotics alternative.

Friction and wear properties of plasma-sprayed $Cr_2$$O_3$/$MoO_3$ composite coatings ($MoO_3$가 첨가된 $Cr_2$$O_3$ 플라스마 용사코팅의 마찰 마멸 특성)

  • 여인웅;안효석;임대순
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.06a
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    • pp.22-29
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    • 2001
  • Plasma-sprayed coatings were prepared using by spray-dried Cr$_2$O$_3$ powder with and without MoO$_3$ addition. A reciprocal type tribe-tester was employed to examine friction and wear behavior of the specimens at room temperature. The worn surfaces of plasma spray coated specimens were observed by SEM. The results showed that friction coefficient of the MoO$_3$-added coatings were lower than those without MoO3 addition. However pure Cr$_2$O$_3$ coating showed the lowest wear loss at the self-mated test. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with MoO$_3$ addition.

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Vacuum Plasma Sprayed NiTiZrSiSn Coating (진공 열 플라즈마 용사공정을 통한 NiTiZrSiSn 벌크 비정질 코팅 형성)

  • Yoon, Sang-Hoon;Kim, June-Seob;Kim, Soo-Ki;Lee, Chang-Hee
    • Journal of Welding and Joining
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    • v.25 no.4
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    • pp.42-48
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    • 2007
  • An inert gas atomized NiTiZrSiSn bulk metallic glass feedstock was sprayed onto the copper plate using vacuum plasma spraying process. In order to change the in-flight particle energy, that is, thermal energy, the hydrogen gas flow rate in plasma gas mixture was increased at the constant flow rate of argon gas. Coating and single pass spraying bead were produced with the least feeding rate. Regardless of the plasma gas composition, fully melted through unmelted particle could be observed on the overlay coating. However, the frequency of the unmelted particle number density was increased with the decrease of the hydrogen gas flow rate. The amorphous phase fraction within coating was also affected by the number density of the unmelted particle.

Tensile Analysis of Plasma Spray Coating Material by Classification of AE Signals (Acoustic Emission 파형분류에 의한 플라즈마 용사 코팅재의 인장해석)

  • ;;K. ONO
    • Journal of Ocean Engineering and Technology
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    • v.15 no.4
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    • pp.60-65
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    • 2001
  • Thermal spray coating is formed by a process in which melted particles flying with high speed towards substrate, then crash and spread on the substrate surface cooled and solidified in a very short time, Stacking of the particles makes coating. In this study, the exfoliation of $Al_2$O$_3$ and Ni-4.5wt.%Al thermally sprayed coating which were deposited by an atmospheric plasma spray apparatus are investigated using an AE method. A tensile test is conducted on notch specimens in a stress range below the elastic limit of substrate. The wave forms of AE generated from the three coating specimens can be classified by FFT analysis into two types which low frequency(type I waveform is considered to corresponds exfoliation of coating layers and type II waveform corresponds the plastic deformation of notch tip or the resultant fracture of coating. The fracture of the coating layers can estimate by AE event and amplitude, because AE features increase when the deformation generates.

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