• 한국주조공학회지
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• 제16권6호
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• pp.523-536
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• 1996

This paper relates to fabrication processing analysis of metal matrix composites by the injection of liquid metal into a fibrous preforms. One dimensional heat transfer analysis during squeeze infiltration process of aluminum base composites has been studied. An analysis method was investigated for the temperature distribution, infiltration velocity and melt infiltration characteristics with the commercial preform with short fiber array. When molten metal is infiltrated in a fibrous preform with random orientation, phase transformation will be occurred in a region such as molten metal, solidified region, preform region and infiltration composites region. a mathematical modelling for a solidification phenomena in fabrication process of metal matrix composites using a squeeze infiltration technique was investigated by the basic relations for liquid metal into a fibrous preform. The temperature distribution of theoretical results was compared with experimental data.

• 한국공작기계학회논문집
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• 제17권1호
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• pp.16-20
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• 2008

This paper presents the construction of micro tool clamping device using a Ni-Ti shape memory alloy(SMA) ring. Clamping force of the device is produced by elastic force of the SMA reverted to its original shape in normal temperature. Phase transformation of the SMA was realized by temperature control using a peltier element. Prototype of the SMA tool clamping device was fabricated and examined its clamping force and clamping/unclamping operation.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2002년도 하계학술대회 논문집 C
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• pp.1413-1415
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• 2002

The Displacement current measurement system used in this experiment because detecting the dynamic behavior of monolayers at the air-water interface is possible. It basically consists of a film balance, a pair of electrodes connected to each other through a sensitive ammeter. Here, one electrode is suspended in air and the other electrode is placed in the water. PBLG phase transformation measured by Maxwell-displacement-current-measurement method in surface of the water. Measured (surfacc pressure, displacement current and dipole moment) of monolayers of PBLG on the water surface. We measured displacement current that occur when changed temperature(15, 20, 25$^{\circ}$ ) and the compression speed(30, 40, 50(mm/min)). From the result, it is known that curren generated in the range of high surface pressur compression velocity and temperature become faste.

• 한국표면공학회지
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• 제29권6호
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• pp.884-890
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• 1996

We have investigated a structural change of Si(100)-($2 \times 1$)-Sb surface caused by atomic hydrogen adsorption at room temperature using time-of-flight impact collision ion scattering spectroscopy (TOF-ICISS) and low energy electron diffraction (LEED). We found that when atomic hydrogen adsorbs on the Si(100)-($2 \times 1$)-Sb surface, (1) the partial desorption of Sb atoms from the Si(100) surface occurs even at room temperature, (2) the rest Sb atoms are displaced from their original positions and form an almost two-dimensional layer with dispersive distribution of Sb atoms, and (3) the structural transformation into the Si(100)-($1 \times 1$)-H periodicity is induced by the formation of the $1 \times 1$-H dihydride phase on the Si substrate.

• 한국진공학회지
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• 제12권S1호
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• pp.116-119
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• 2003

$Ni_2$MnGa films, deposited on mica and glass substrates, were studied by ferromagnetic resonance (FMR) technology. The temperature-dependent resonance field was measured and a martensitic phase transformation (MT) was found between 310 and 340 K, exhibiting an abnormality on the curve. The easy axis is found to be in the film plane. The line width increases as a whole with decreasing temperature, which is discussed in terms of the motional narrowing mechanism. The resonance field was also measured as a function of orientation and the results were fitted, exhibiting a good consistence.

• 한국결정성장학회지
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• 제14권6호
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• pp.267-271
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• 2004

우레아 가수분해법을 이용하여 리튬이차전지용 $LiCoO_2$ 양극 분말을 합성하였다. Li/Co 몰비가 다르고 가수분해에 의해 얻어진 전구체는 다양한 온도에서 열처리되었다. 저온상 $LiCoO_2(LT-LiCoO_2)$와 고온상 $LiCoO_2(HT-LiCoO_2)$는 $500^{\circ}C$에서 2시간 열처리 후 합성되었고, 저온상에서 고온상으로 상전이는 $700^{\circ}C$ 이상에서 완전히 일어났다. 열처리 온도가 증가함에 따라 $LiCoO_2$의 층상구조가 잘 발달하였다. 충방전 실험결과 Li/Co의 몰비가 1.2이고 $800^{\circ}C$에서 열처리한 $LiCoO_2$의 초기용량이 152 mAh/g으로 높았으며, 40회 충.방전 후에는 9.2%의 용량감소를 나타내는 상대적으로 안정한 충방전 특성을 나타내었다.

• 한국광물학회지
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• 제10권2호
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• pp.148-161
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• 1997

Based on the X-ray powder diffraction (XRD) and M ssbauer spectroscopy, the thermal behavior and phase transformations of two clays are investigated for raw and fired conditions, which are collected from Kwangryeongli and Ildo district in Cheju Island. M ssbauer spectra at room temperature and 20for two clays show that paramagnetic Fe3- is the structural iron of the layer silicate and ferrihydrite, and superparamagnetic goethite has about 50% of total iron contents. The XRD peaks of hematite for the fired clays appear from 80$0^{\circ}C$ in Kwangryeongli clay and from $600^{\circ}C$ in Ildo district clay, respectively. The structural Fe2+ was completely oxidized into Fe3- at 40$0^{\circ}C$ for Kwangryeongli clay and 50$0^{\circ}C$~$600^{\circ}C$ for Ildo district clay, respectively. The structural Fe2+ was completely oxidized into Fe3- at 40$0^{\circ}C$. For the temperature ranging from 40$0^{\circ}C$ to $700^{\circ}C$~80$0^{\circ}C$, two fired clays exhibit the dehydroxylation of the clay mineral. A disintegration of the clay mineral structure is observed from $700^{\circ}C$~80$0^{\circ}C$ to 110$0^{\circ}C$, followed by the onset and spread of vitrification process. It is also shown that well-crystallized hematite phase is formed at the temperature higher than 110$0^{\circ}C$ and the relative absorption area decreases, which might be related to the recrystallization of alluminosilicate matrix.

• 한국분말재료학회지
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• 제26권5호
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• pp.389-394
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• 2019

In the present study, we have investigated the effect of sintering process conditions on the stability of the austenite phase in the nanocrystalline Fe-5wt.%Mn-0.2wt.%C alloy. The stability and volume fraction of the austenite phase are the key factors that determine the mechanical properties of FeMnC alloys, because strain-induced austenite-martensite transformation occurs under the application of an external stress at room temperature. Nanocrystalline Fe-5wt.%Mn-0.2wt.%C samples are fabricated using the spark plasma sintering method. The stability of the austenite phase in the sintered samples is evaluated by X-ray diffraction analysis and hardness test. The volume fraction of austenite at room temperature increases as the sample is held for 10 min at the sintering temperature, because of carbon diffusion in austenite. Moreover, water quenching effectively prevents the formation of cementite during cooling, resulting in a higher volume fraction of austenite. Furthermore, it is found that the hardness is influenced by both the austenite carbon content and volume fraction.

• 한국환경과학회지
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• 제17권11호
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• pp.1273-1279
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• 2008

This study examined the catalytic destruction of 1,2-dichlorobenzene on ${V_2}{O_5}/TiO_2$ nanoparticles. The ${V_2}{O_5}/TiO_2$ nanoparticles were synthesized by the thermal decomposition of vanadium oxytripropoxide and titanium. The effects of the synthesis conditions, such as the synthesis temperature and precursor heating temperature, were investigated. The specific surface areas of ${V_2}{O_5}/TiO_2$ nanoparticles increased with increasing synthesis temperature and decreasing precursor heating temperature. In addition, the removal efficiency of 1,2-dichlorobenzene was promoted by a decrease in heating temperature. However, the removal efficiency of 1,2-dichlorobenzene was decreased by an anatase to rutile phase transformation at temperatures $1,300^{\circ}C$.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2005년도 춘계학술대회 논문집
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• pp.441-445
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• 2005

In the resent years, as the research and the development of micro and precision machinery become active, the interest of micro actuators using SMA(Shape Memory Alloy) has been increased. But, no detailed researches between the thermo-dynamic property in Nitinol alloy have been done yet. In this study, the thermal property of high temperature Nitinol shape memory alloy were evaluated using differential scanning calorimeter(DSC). The structure property was investigated using X-ray diffraction(XRD). A dynamic mechanical analyzer(DMA) with three point bending mode was used to study storage and loss modulus of shape memory alloy according to the thirteen frequencies in the temperature range between 30 and $200^{\circ}C$. The effects of the temperature heating/cooling rate, the frequency on the damping capacity have been systematically investigated. Such a frequency and temperature changes also influenced significantly to the damping behavior of the shape memory alloy. It was also found that Nitinol exhibited high damping capacity during phase transformation.